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Secobarbital

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-1DB-1BP-1BP-1
Column length (m)  10.15.12.12.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm)  0.530.250.220.22
Phase thickness (mum)  2.650.250.250.25
Tstart (C) 100.130.130.120.50.
Tend (C) 300.230.290.280.300.
Heat rate (K/min)  5.10.8.20.
Initial hold (min)   1.  
Final hold (min)   10.  
I 1770.1757.1766.1769.1763.
ReferenceMHA, 9999Anderson and Fuller, 1987Sharp, 1987Stowell and Wilson, 1985Stowell and Wilson, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPacked
Active phase OV-1SE-30SE-30SE-30
Column length (m) 2.2.2.2.
Carrier gas   NitrogenN2
Substrate Gas Chrom PGas Chrom PChromosorb W AW DMS (80-100 mesh)Chromosorb W AW DMS
Column diameter (mm)     
Phase thickness (mum)     
Tstart (C) 120.120.130.130.
Tend (C) 200.200.290.290.
Heat rate (K/min) 2.52.58.8.
Initial hold (min)   2.2.
Final hold (min)   8.8.
I 1770.1770.1788.1788.
ReferenceMarozzi, Gambaro, et al., 1982Marozzi, Gambaro, et al., 1982Peel and Perrigo, 1976Peel and Perrigo, 1975
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

MHA, 9999
MHA, Directorate of ForensicScience., Forensic Toxicology, 9999. [all data]

Anderson and Fuller, 1987
Anderson, W.H.; Fuller, D.C., A simplified procedure for the isolation, characterization, and identification of weak acid and neutral drugs from whole blood, J. Anal. Toxicol., 1987, 11, 5, 198-204, https://doi.org/10.1093/jat/11.5.198 . [all data]

Sharp, 1987
Sharp, M.E., A rapid screening procedure for acidic and neutral drugs in blood by high resolution gas chromatography, J. Anal. Toxicol., 1987, 11, 1, 8-11, https://doi.org/10.1093/jat/11.1.8 . [all data]

Stowell and Wilson, 1985
Stowell, A.; Wilson, L., Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]

Marozzi, Gambaro, et al., 1982
Marozzi, E.; Gambaro, V.; Saligari, E.; Mariani, R.; Lodi, F., Use of the retention index in gas chromatographic studies of drugs, J. Anal. Toxicol., 1982, 6, 4, 185-192, https://doi.org/10.1093/jat/6.4.185 . [all data]

Peel and Perrigo, 1976
Peel, H.W.; Perrigo, B., A practical gas chromatographic screening procedure for toxicological analysis, Can. Soc. Forens. Sci. J., 1976, 9, 2, 69-74, https://doi.org/10.1080/00085030.1976.10757247 . [all data]

Peel and Perrigo, 1975
Peel, H.W.; Perrigo, B., A practical gas chromatographic screening procedure for toxicological analysis, Can.Soc.Forens.Sci.J., 1975, 9, 2, 69-74, https://doi.org/10.1080/00085030.1976.10757247 . [all data]


Notes

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