Bornyl acetate

Formula: C₁₂H₂₀O₂
Molecular weight: 196.2860
IUPAC Standard InChI: InChI=1S/C12H20O2/c1-8(13)14-10-7-9-5-6-12(10,4)11(9,2)3/h9-10H,5-7H2,1-4H3/t9?,10-,12?/m0/s1
IUPAC Standard InChIKey: KGEKLUUHTZCSIP-YZRBJQDESA-N
CAS Registry Number: 76-49-3
Chemical structure:
This structure is also available as a 2d Mol file
Stereoisomers:
Other names: Bicyclo[2.2.1]heptan-2-ol, 1,7,7-trimethyl-, acetate, endo-; Borneol, acetate; Bornyl acetic ether; 2-Camphanol acetate; endo-2-Camphanyl ethanoate; 1,7,7-Trimethylbicyclo(2.2.1)heptan-2-ol acetate; 1,7,7-Trimethylbicyclo[2.2.1]hept-2-yl acetate; bornyl aceate; borneyl acetate; endo-1,7,7-trimethylbicyclo[2.2.1]hept-2-yl acetate
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Normal alkane RI, non-polar column, temperature ramp

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Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	RTX-1	RTX-1	HP-5	HP-5
Column length (m)	60.	60.	60.	25.	25.
Carrier gas	Helium	Helium	Helium	Hydrogen	Hydrogen
Substrate
Column diameter (mm)	0.25	0.22	0.22	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.52	0.52
T_start (C)	40.	60.	60.	40.	40.
T_end (C)	250.	230.	230.	280.	280.
Heat rate (K/min)	3.	2.	2.	4.	4.
Initial hold (min)	1.
Final hold (min)	20.	5.	5.	10.	10.
I	1287.	1270.	1270.	1281.	1281.
Reference	Sardashti, Valizadeh, et al., 2013	Bendiabdellah, El Amine Dib, et al., 2012	Bendiabdellah, El Amine Dib, et al., 2012	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RTX-1	HP-5 MS	CP-Sil 5 CB	CP-Sil 5 CB
Column length (m)	25.	60.	30.	25.	25.
Carrier gas	Hydrogen	Helium	Helium	Helium	Hydrogen
Substrate
Column diameter (mm)	0.32	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.52	0.25	0.25	0.15	0.15
T_start (C)	40.	60.	50.	50.	50.
T_end (C)	280.	230.	250.	220.	230.
Heat rate (K/min)	4.	2.	7.		3.
Initial hold (min)			1.
Final hold (min)	10.	45.	5.
I	1281.	1265.	1286.	1284.	1275.
Reference	Velickovic, Ristic, et al., 2012	Yapi, Boti, et al., 2012	Zouari, Ayadi, et al., 2012	Ameen, Usman, et al., 2011	Esseien, Aboaba, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	VF-5 MS	VF-5 MS	CP-Sil 5 CB	Methylsiloxane + 5 % Ph-groups
Column length (m)	30.	60.	60.	30.	30.
Carrier gas	Helium	Helium	Helium	Nitrogen	Helium
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.26	0.25
T_start (C)	60.	30.	30.	45.	60.
T_end (C)	240.	260.	260.	280.	230.
Heat rate (K/min)	3.	2.	2.	3.	7.
Initial hold (min)	2.				2.
Final hold (min)		28.	28.	22.	20.
I	1286.	1289.	1290.	1270.	1273.
Reference	Kahriman, Tosun, et al., 2011	Leffingwell and Alford, 2011	Leffingwell and Alford, 2011	Mothana, Hasson, et al., 2011	Nadim, Malik, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5	ZB-5 MS	ZB-5 MS	BP-1
Column length (m)	30.	30.	30.	30.
Carrier gas	Helium	Nitrogen	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.32	0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	60.
T_end (C)	210.	280.	290.	290.	220.
Heat rate (K/min)	6.	5.	5.	5.	5.
Initial hold (min)	3.	1.			10.
Final hold (min)	2.	1.			30.
I	1236.	1270.	1280.	1286.	1267.
Reference	Taherpour, Maroofi, et al., 2011	Tekaya-Karoui, Boughalleb, et al., 2011	Boix, Victorio, et al., 2010	Boix, Victorio, et al., 2010	Mishra, Chaudhary, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	HP-5 MS	DB-1-MS	DB-5	HP-5MS
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.20	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.20	0.25	0.25	0.25	0.25
T_start (C)	70.	60.	30.	40.	50.
T_end (C)	220.	220.	200.	250.	250.
Heat rate (K/min)	3.	6.	2.	10.	7.
Initial hold (min)		3.	4.	1.	1.
Final hold (min)	15.		35.	3.	5.
I	1264.	1263.	1265.	1289.	1291.
Reference	Neves, Rosa, et al., 2010	Safaei-Ghomi and Batooli, 2010	Takeoka, Hobbs, et al., 2010	Yang, Zhang, et al., 2010	Zouari, Zouari, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-54	SPB-5	DB-5	RTX-1	RTX-1
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	Helium	Nitrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.53	0.25	0.22	0.22
Phase thickness (μm)	0.25	0.50	0.25	0.25	0.25
T_start (C)	60.	50.	50.	60.	60.
T_end (C)	260.	210.	250.	230.	230.
Heat rate (K/min)	2.	3.	5.	2.	2.
Initial hold (min)	5.	5.	2.
Final hold (min)	999.	45.		30.	30.
I	1282.	1297.	1289.	1270.	1271.
Reference	Dayisoylu and Alma, 2009	Gilani, Shah, et al., 2009	Ho, Wang, et al., 2009	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-1	DB-5	HP-5MS	HP-5 MS	Ultra 2
Column length (m)	30.	50.	30.	30.	50.
Carrier gas	Helium	Nitrogen	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.20	0.25	0.25	0.20
Phase thickness (μm)	0.25	0.32	0.25	0.25	0.11
T_start (C)	40.	60.	50.	50.	60.
T_end (C)	300.	220.	240.	280.	230.
Heat rate (K/min)	4.	5.	5.	4.	2.
Initial hold (min)	2.	3.			5.
Final hold (min)	10.	5.			30.
I	1262.	1289.	1295.	1288.	1291.
Reference	Nibret and Wink, 2009	Shafaghat and Sadeghi, 2009	Wannes, Mhamdi, et al., 2009	Zhao, Zeng, et al., 2009	Byun and Shin, 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	VF-5MS	SLB-5 MS	ZB-1	DB-5	Elite-1
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	Helium	Helium	Nitrogen	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	240.	50.	45.	60.	60.
T_end (C)	320.	250.	230.	250.	246.
Heat rate (K/min)	20.	3.	3.	5.	3.
Initial hold (min)	1.	2.
Final hold (min)		10.		10.
I	1290.	1284.	1266.	1293.	1284.
Reference	Kowalski, 2008	Lo Presti, Sciarrone, et al., 2008	Mierendorff, Stahl-Biskup, et al., 2008	Mosayebi, Amin, et al., 2008	Raj, Baby, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	RTX-5	DB-5 MS	OV-1	HP-5
Column length (m)	30.	20.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.18	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.20	0.25	0.25	0.32
T_start (C)	60.	50.	60.	65.	60.
T_end (C)	250.	280.	270.	260.	250.
Heat rate (K/min)	2.	4.	3.	6.	5.
Initial hold (min)	8.	1.			30.
Final hold (min)	15.
I	1284.	1295.	1288.	1318.	1282.
Reference	Sahraoui, Vian, et al., 2008	Skalicka-Wozniak, Los, et al., 2008	Victorio, Alviano, et al., 2008	Wang, Yi, et al., 2008	Yassa and Akhani, 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-5	CP Sil 5 CB	SE-52	HP-5MS
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	Helium	Nitrogen	N2		He
Substrate
Column diameter (mm)	0.25	0.20	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.32	0.25	0.25	0.25
T_start (C)	50.	60.	60.	50.	60.
T_end (C)	230.	220.	300.	220.	280.
Heat rate (K/min)	3.	5.	4.	3.	3.
Initial hold (min)	10.	3.		1.
Final hold (min)	10.	5.		5.
I	1285.	1285.	1274.	1264.	1288.
Reference	Adams, Beauchamp, et al., 2007	Amiri, 2007	Baran, von Reuss, et al., 2007	Bicchi, Cordero, et al., 2007	Bozin B., Mlmica-Dukic N., et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	DB-1	Col-Elite 5MS	DBP-5	SE-30
Column length (m)	30.	60.	30.	25.	30.
Carrier gas	Helium	Nitrogen	He	Helium	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.22	0.25
T_start (C)	60.	60.	30.	40.	40.
T_end (C)	280.	250.	246.	250.	250.
Heat rate (K/min)	4.	4.	3.	3.	5.
Initial hold (min)	5.	1.		1.	5.
Final hold (min)		10.		10.	10.
I	1288.	1275.	1269.	1255.	1291.
Reference	Capetanos, Saroglou, et al., 2007	Ghasempour, Shirinpour, et al., 2007	Gudaityte and Venskutonis R.P., 2007	Heravi and Sereshti, 2007	Loizzo, Tundis, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	DB-5	HP-5 MS	SPB-1
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	Helium	He	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.32	0.25	0.2
T_start (C)	40.	50.	50.	100.	70.
T_end (C)	250.	260.	250.	280.	220.
Heat rate (K/min)	5.	2.5	5.	4.	3.
Initial hold (min)	5.	1.		3.
Final hold (min)	10.	20.		5.	15.
I	1285.	1262.	1267.	1291.	1266.
Reference	Loizzo, Tundis, et al., 2007	Monser-Esfahani, Karamkhani, et al., 2007	Nori-Shargh, Raftari, et al., 2007	Phutdhawong, Kawaree, et al., 2007	Pinto, Salgueiro, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-1	HP-5	DB-1	DBP-5
Column length (m)	30.	60.	30.	60.	25.
Carrier gas	He	Nitrogen	Helium	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.22
T_start (C)	50.	60.	40.	60.	40.
T_end (C)	250.	250.	260.	250.	250.
Heat rate (K/min)	2.	4.	4.	5.	3.
Initial hold (min)		1.			1.
Final hold (min)		10.			10.
I	1285.	1275.	1282.	1276.	1255.
Reference	Raal, Orav, et al., 2007	Reza, Ebrahim, et al., 2007	Ristic, Krivokuca-Dokic, et al., 2007	Salehi, Fakhari, et al., 2007	Sereshti and Samadi, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5MS	HP-5 MS	HP-5MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He	Helium	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	40.	40.
T_end (C)	280.	280.	280.	250.	260.
Heat rate (K/min)	3.	3.	3.	3.	4.
Initial hold (min)				5.
Final hold (min)				10.
I	1287.	1249.	1289.	1282.	1283.1
Reference	Tsokou, Georgopoulos, et al., 2007	Tzakou, Bazos, et al., 2007	Vagionas, Graikou, et al., 2007	Vichi, Riu-Aumatell, et al., 2007	Zizovic, Stamenic, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	DB-5	ZB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	N2	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	50.	50.	40.	60.
T_end (C)	280.	280.	265.	300.	280.
Heat rate (K/min)	9.	9.	2.5	2.	3.
Initial hold (min)	3.	3.	1.
Final hold (min)	3.	3.	20.
I	1270.	1275.	1290.	1289.	1288.
Reference	Abdelwahed, Hayder, et al., 2006	Abdelwahed, Hayder, et al., 2006	Bazargani, Almasirad, et al., 2006	Biondi, Sari, et al., 2006	Bozin, Mimicá-Dukic, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	HP-5	DB-5	HP-5MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	He			He
Substrate
Column diameter (mm)	0.20	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.20	0.25	0.25	0.25	0.25
T_start (C)	70.	60.	60.	60.	50.
T_end (C)	220.	246.	230.	280.	250.
Heat rate (K/min)	3.	3.	3.	4.	2.
Initial hold (min)
Final hold (min)	15.		15.
I	1264.	1288.	1285.	1288.	1295.
Reference	Cavaleiro, Pinto, et al., 2006	Coronel, Cerda-Garcia-Rojas, et al., 2006	Damjanovic, Skala, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006	Farah, Afifi, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-1	DB-5	Methyl Silicone	RTX-1
Column length (m)	30.	50.	30.	25.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.25
T_start (C)	50.	60.	50.	90.	60.
T_end (C)	300.	250.	250.	220.	300.
Heat rate (K/min)	5.	2.	3.	7.	4.
Initial hold (min)	5.			2.
Final hold (min)	5.	40.	10.
I	1286.	1269.	1285.	1290.	1266.
Reference	Figuérédo, Cabassu, et al., 2006	Filippi, Lanfranchi, et al., 2006	Havlik, Kokoska, et al., 2006	Kitchlu, Bakshi, et al., 2006	Kula, Izydorczyk, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	HP-5 MS	HP-5	DB-5	SE-52
Column length (m)	30.	30.	30.	30.	50.
Carrier gas	N2	Nitrogen	N2	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.52	0.25
T_start (C)	50.	50.	50.	50.	50.
T_end (C)	300.	280.	280.	250.	240.
Heat rate (K/min)	4.	5.	5.	3.	3.
Initial hold (min)				5.
Final hold (min)		5.	5.
I	1264.	1278.	1278.	1284.	1284.
Reference	Lis and Milczarek, 2006	Marzouk, Mansour, et al., 2006	Marzouk, Neffati, et al., 2006	Mirza, Navaei, et al., 2006	Ozcan, Chalchat, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5MS	DB-5	HP-5	DB-5
Column length (m)	50.	30.	30.	25.	30.
Carrier gas	N2	He	Hydrogen	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	95.	40.	70.	60.	60.
T_end (C)	240.	260.	280.	240.	260.
Heat rate (K/min)	4.	4.	4.	3.	5.
Initial hold (min)			4.
Final hold (min)
I	1280.	1288.	1283.	1291.	1291.
Reference	Pala-Paul J., Perez-Alonso M.J., et al., 2006	Petrovic, Ristic, et al., 2006	Pino, Marbot, et al., 2006	Potzernheim, Bizzo, et al., 2006	Sabulal, Dan, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	SPB-5	SPB-5	DB-1
Column length (m)	15.	30.		60.	50.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.2	0.25		0.32	0.25
Phase thickness (μm)	0.25	0.25		1.	0.25
T_start (C)	60.	40.	50.	40.	90.
T_end (C)	305.	240.	250.	230.	240.
Heat rate (K/min)	15.	4.	5.	3.	4.
Initial hold (min)	2.		3.	5.
Final hold (min)			15.	2.
I	1283.	1283.	1285.	1307.	1279.
Reference	Sebastián, Urzúa, et al., 2006	Sefidkon and Jamzad, 2006	Stojanovic, Palic, et al., 2006	Tornambe, Cornu, et al., 2006	Velasco-Negueruela, Pérez-Alonso, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	BPX-5	SPB-1	DB-5	HP-5MS
Column length (m)	25.	50.	30.	30.	30.
Carrier gas	H2		He	He	He
Substrate
Column diameter (mm)	0.32	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.52	1.	0.25	0.25	0.25
T_start (C)	50.	70.	50.	60.	60.
T_end (C)	280.	280.	250.	210.	280.
Heat rate (K/min)	2.5	4.	4.	3.	3.
Initial hold (min)	5.		1.	5.
Final hold (min)		4.	10.
I	1275.	1315.	1259.	1283.	1277.
Reference	Wang, Kong, et al., 2006	Wohlmuth, Smith, et al., 2006	Wong, Sivasothy, et al., 2006	Askari and Sefidkon, 2005	Basta, Tzakou, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	Methyl Silicone	DB-1	HP-5MS
Column length (m)	25.	50.	60.	60.	25.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.3	0.3	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25
T_start (C)	50.	60.	50.	60.	50.
T_end (C)	250.	240.	240.	250.	250.
Heat rate (K/min)	3.	2.	3.	5.	3.
Initial hold (min)	3.				3.
Final hold (min)					10.
I	1284.	1284.	1282.	1276.	1286.
Reference	Cégiéla-Carlioz, Bessière, et al., 2005	Chagonda and Chalchat, 2005	Chalchat and Özcan, 2005	Fakhari, Salehi, et al., 2005	Ghasemi Y., Faridi P., et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-1	DB-5MS	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	60.
T_end (C)	250.	265.	280.	220.	280.
Heat rate (K/min)	5.	2.5	3.	4.	3.
Initial hold (min)		1.	30.	5.
Final hold (min)	10.	30.
I	1277.	1262.	1263.	1289.	1289.
Reference	Jassbi, Mehrdad, et al., 2005	Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005	Marongiu, Piras, et al., 2005	Morteza-Semnani, Akbarzadeh, et al., 2005	Petrakis, Roussis, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	HP-5MS	RTX-1	DB-5
Column length (m)	30.	30.	30.	60.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	40.
T_end (C)	240.	220.	280.	250.	210.
Heat rate (K/min)	5.	3.	3.	5.	2.
Initial hold (min)		4.			2.
Final hold (min)				10.	33.
I	1285.	1285.	1285.	1276.	1293.
Reference	Saeidnia, Gohari, et al., 2005	Salehi, Sefidkon, et al., 2005	Slavkovska, Couladis, et al., 2005	Sonboli A., Fakhari A.R., et al., 2005	Stevanovic, Garneau, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	HP-5MS	SPB-1	BP-1
Column length (m)	30.	50.	30.	50.	50.
Carrier gas	He			He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.2	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.25
T_start (C)	60.	60.	40.	50.	60.
T_end (C)	280.	240.	220.	220.	220.
Heat rate (K/min)	3.	3.	3.	4.	2.
Initial hold (min)			5.	3.
Final hold (min)			10.	30.	20.
I	1259.	1247.	1282.	1272.	1272.
Reference	Tzakou and Constantinidis, 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Vichi, Riu-Aumatell, et al., 2005	Wong, Lee, et al., 2005	Blanc, Muselli, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	RTX-1	SE-54	RTX-1
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	Nitrogen	N2	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	275.	240.	300.	260.	300.
Heat rate (K/min)	4.	3.	4.	2.	4.
Initial hold (min)				5.
Final hold (min)
I	1282.	1283.	1273.	1281.	1270.
Reference	Hajhashemi V., Ghannadi A., et al., 2004	JAvidnia, Mojab, et al., 2004	Kalemba and Thiem, 2004	Kilic, Hafizoglu, et al., 2004	Lis, Boczek, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	HP-5MS	NB-30	DB-5
Column length (m)	30.	30.	30.	50.	30.
Carrier gas		He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.20	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	50.	35.
T_end (C)	210.	280.	280.	250.	220.
Heat rate (K/min)	2.	3.	3.	2.	2.5
Initial hold (min)	2.
Final hold (min)	33.				6.
I	1292.	1284.	1288.	1274.	1289.
Reference	Lopez Arze, Collin, et al., 2004	Malencic, Couladis, et al., 2004	Mimica-Dukic, Bozin, et al., 2004	Raal, Paaver, et al., 2004	Rohloff, Mordal, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	HP-1	HP-5	DB-5
Column length (m)	30.	30.	30.	25.	30.
Carrier gas	He	He	He	H2	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.249
Phase thickness (μm)	0.25	0.25	0.33	0.52	0.25
T_start (C)	60.	60.	40.	40.	60.
T_end (C)	280.	280.	260.	240.	300.
Heat rate (K/min)	4.	4.	2.	4.	3.
Initial hold (min)			5.
Final hold (min)			20.
I	1280.	1285.	1243.	1285.	1281.
Reference	Sadeghpour, Asghari, et al., 2004	Sajjadi and Shahpiri, 2004	Senatore, Napolitano, et al., 2004	Simic, Sokovic, et al., 2004	Woerdenbag, Windono, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	HP-5MS	RTX-5Sil	HP-5MS
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.25
T_start (C)	60.	40.	60.	70.	60.
T_end (C)	275.	190.	280.	200.	220.
Heat rate (K/min)	4.	4.	3.	4.	5.
Initial hold (min)					20.
Final hold (min)		5.		10.	20.
I	1285.	1242.	1282.	1286.	1293.
Reference	Afsharypuor and Jahromy, 2003	Azodanlou, Darbellay, et al., 2003	Couladis, Özcan, et al., 2003	Dudai, Larkov, et al., 2003	Feizbaksh, Saber Tehrani, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5MS	HP-5MS	HP-5MS	RSL-200
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He	He	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	40.
T_end (C)	200.	275.	280.	275.	280.
Heat rate (K/min)	5.	4.	4.	4.	6.
Initial hold (min)					5.
Final hold (min)					5.
I	1263.	1283.	1285.	1287.	1277.
Reference	Fekam Boyom, Ngouana, et al., 2003	Ghannadi, Aghazari, et al., 2003	Ghasemi, Asghari, et al., 2003	Hajhashemi, Ghannadi, et al., 2003	Jirovetz, Buchbauer, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	ZB-1	DB-1	OV-101	DB-5
Column length (m)	30.	30.	60.	50.	30.
Carrier gas	He	N2	He	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.5	0.25
T_start (C)	60.	45.	50.	50.	60.
T_end (C)	280.	230.	270.	250.	280.
Heat rate (K/min)	3.	3.	4.	2.	4.
Initial hold (min)					10.
Final hold (min)	30.				40.
I	1280.	1266.	1272.	1268.	1285.
Reference	Marongiu, Porcedda, et al., 2003	Mierendorff, Stahl-Biskup, et al., 2003	Mirza, Nik, et al., 2003	Orav, Kailas, et al., 2003	Pino, Marbot, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-1	DB-5	HP-5	HP-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	75.	60.	60.
T_end (C)	280.	250.	220.	280.	280.
Heat rate (K/min)	3.	4.	3.	4.	4.
Initial hold (min)			4.
Final hold (min)
I	1269.	1264.	1291.	1287.	1283.
Reference	Pitarokili, Tzakou, et al., 2003	Pourmortazavi, Sefidkon, et al., 2003	Priestap, van Baren, et al., 2003	Sajjadi and Mehregan, 2003	Sajjadi and Mehregan, 2003, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DB-1	HP-5	HP-5
Column length (m)	60.	30.	50.	25.	25.
Carrier gas	He	He	N2	H2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.53	0.53
T_start (C)	50.	60.	90.	40.	40.
T_end (C)	280.	240.	240.	280.	280.
Heat rate (K/min)	4.	3.	4.	4.	4.
Initial hold (min)
Final hold (min)
I	1270.	1284.	1260.	1285.	1289.
Reference	Shahmir, Ahmadi, et al., 2003	da Silva, Luz, et al., 2003	Velasco-Negueruela, Pérez-Alonso, et al., 2003	Velickovic, Randjelovic, et al., 2003	Velickovic, Randjelovic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	DB-5	DB-5	OV-101
Column length (m)	25.	25.	25.	30.	25.
Carrier gas	Helium	Helium	N2	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.249	0.32
Phase thickness (μm)	0.53	0.53	0.25	0.25
T_start (C)	40.	40.	50.	60.	50.
T_end (C)	280.	280.	250.	300.	200.
Heat rate (K/min)	4.	4.	4.	3.	5.
Initial hold (min)
Final hold (min)			10.	5.
I	1283.	1289.	1286.	1284.	1276.
Reference	Velickovic, Ristic, et al., 2003	Velickovic, Ristic, et al., 2003	Zrira, Elamrani, et al., 2003	Bos, Koulman, et al., 2002	Boyom, Keumedjio, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-1	5 % Phenyl methyl siloxane	DB-5MS	DB-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	75.	60.	60.
T_end (C)	280.	220.	200.	280.	280.
Heat rate (K/min)	3.	3.	3.	3.	3.
Initial hold (min)			4.
Final hold (min)	30.	15.	8.
I	1280.	1267.	1289.	1288.	1288.
Reference	Caredda, Marongiu, et al., 2002	Cavaleiro, Salgueiro, et al., 2002	Cicció and Gómez-Laurito, 2002	Congiu, Falconieri, et al., 2002	Congiu, Falconieri, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	SE-30	HP-5	DB-5
Column length (m)	30.	30.	50.	30.	30.
Carrier gas	H2	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	40.	60.	70.	50.	40.
T_end (C)	245.	275.	240.	200.	210.
Heat rate (K/min)	3.	4.	4.	3.	2.
Initial hold (min)	20.				2.
Final hold (min)					33.
I	1268.	1283.	1274.	1290.	1293.
Reference	Gancel, Ollé, et al., 2002	Ghannadi, Sajjadi, et al., 2002	Iñigo, Palá-Paúl, et al., 2002	Isidorov and Jdanova, 2002	Kabouss, Charrouf, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	OV-101	DB-1	OV-101	HP-1
Column length (m)	60.	25.	30.	50.	50.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.2	0.25
Phase thickness (μm)	0.25		0.25	0.5	0.25
T_start (C)	50.	50.	60.	50.	90.
T_end (C)	240.	200.	250.	250.	220.
Heat rate (K/min)	5.	5.	4.	2.	3.
Initial hold (min)	3.		10.
Final hold (min)	10.
I	1299.	1271.	1298.	1268.	1283.
Reference	Kim and Lee, 2002	Menut, Bessière, et al., 2002	Norouzi-Arasi, Yavari, et al., 2002	Orav, Kailas, et al., 2002	Priestap, van Baren, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	DB-5	SPB-5	DB-1
Column length (m)	60.	30.	30.	60.	60.
Carrier gas	He	H2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	40.	40.	60.	40.	40.
T_end (C)	280.	280.	240.	220.	280.
Heat rate (K/min)	4.	4.	3.	3.	4.
Initial hold (min)	5.			5.	5.
Final hold (min)				15.
I	1268.	1285.	1286.	1284.	1263.
Reference	Sefidkon, Jalili, et al., 2002	Velickovic, Randjelovic, et al., 2002	Zoghbi, Andrade, et al., 2002	Cornu, Carnat, et al., 2001	Dabiri and Sefidkon, 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5	BP-1	SPB-5	CBP-1
Column length (m)	60.	30.	30.	60.	25.
Carrier gas	He	N2	N2	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	50.	50.
T_end (C)	280.	220.	220.	240.	210.
Heat rate (K/min)	4.	5.	5.	3.	3.
Initial hold (min)	5.	10.		3.	2.
Final hold (min)				10.
I	1263.	1287.	1272.	1299.	1266.
Reference	Dabiri and Sefidkon, 2001	Gallori, Flamini, et al., 2001	Gupta, Mallavarapu, et al., 2001	Kim and Lee, 2001	Ly, Yamauchi, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	DB-5	DB-1	PTE-5
Column length (m)	60.	30.	30.	30.	60.
Carrier gas	He	N2	H2	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.32
Phase thickness (μm)	0.25	0.25	0.25		0.3
T_start (C)	50.	80.	60.	60.	60.
T_end (C)	270.	225.	285.	240.	285.
Heat rate (K/min)	4.	4.	3.	3.	4.3
Initial hold (min)
Final hold (min)
I	1264.	1252.	1283.	1282.0	1285.
Reference	Mirza, Ahmadi, et al., 2001	Palá-Paúl, Pérez-Alonso, et al., 2001	Santos-Gomes and Fernandes-Ferreira, 2001	Santos, Moreira, et al., 2001	Stojanovic, Palic, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	DB-1	HP-1	BP-1	OV-1
Column length (m)	60.	25.	60.	25.	25.
Carrier gas	H2	Nitrogen	He	N2	Hydrogen
Substrate
Column diameter (mm)	0.32	0.50	0.25	0.33	0.32
Phase thickness (μm)	0.25	0.25	0.25	1.0	0.30
T_start (C)	40.	60.	60.	60.	50.
T_end (C)	250.	220.	200.	275.	200.
Heat rate (K/min)	6.	5.	4.	4.	3.
Initial hold (min)			5.		1.
Final hold (min)			25.		10.
I	1278.	1272.	1276.	1284.	1258.
Reference	Jirovetz, Puschmann, et al., 2000	Mallavarapu, Rao, et al., 2000	Meccia, Rojas, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000	Bicchi, Binello, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	RTX-1	DB-1	DB-1	CP Sil 5 CB
Column length (m)	30.	30.	25.	30.	25.
Carrier gas	N2	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	50.
T_end (C)	220.	300.	290.	200.	230.
Heat rate (K/min)	4.	4.	4.	4.	3.
Initial hold (min)	10.
Final hold (min)
I	1264.	1274.	1284.	1255.	1266.
Reference	Jassbi, Ahmad, et al., 1999	Kalemba, 1999	Koulman, 1999	Nori-Shargh, Norouzi-Arasi, et al., 1999	Oyedeji, Olawore, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	CP Sil 5 CB	DB-5	DB-1	CP Sil 5 CB
Column length (m)	50.	25.	30.	60.	25.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.39	0.25		0.39
T_start (C)	70.	60.	40.	60.	60.
T_end (C)	240.	220.	220.	230.	220.
Heat rate (K/min)	4.	5.	4.	3.	5.
Initial hold (min)		5.	5.
Final hold (min)		20.		5.
I	1251.	1272.	1284.	1274.	1276.
Reference	Palá-Paúl, Pérez-Alonso, et al., 1999	Rustaiyan, Masoudi, et al., 1999	Sefidkon and Khajavi, 1999	Shafiee, Javidnia, et al., 1999	Weyerstahl, Marschall, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	SPB-5	HP-101	HP-1	CP Sil 5 CB
Column length (m)	30.	50.	25.	60.	25.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.32	0.2	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.2	0.25	0.25
T_start (C)	60.	60.	70.	50.	50.
T_end (C)	240.	240.	200.	280.	290.
Heat rate (K/min)	3.	3.	3.	4.	4.
Initial hold (min)			2.	5.
Final hold (min)		20.	10.
I	1283.	1288.	1268.	1272.	1264.
Reference	Zoghbi, Andrade, et al., 1999	Doneanu and Anitescu, 1998	Milso, Mastelic, et al., 1998	Stashenko, Cervantes, et al., 1998	Bos, Woerdenbag, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	CP Sil 5 CB	SPB-Sulfur	SPB-Sulfur	DB-1
Column length (m)	25.	25.	30.	30.
Carrier gas	N2	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.25	4.	4.
T_start (C)	50.	60.	45.	45.	80.
T_end (C)	290.	300.	240.	240.	220.
Heat rate (K/min)	4.	6.	5.	5.	6.
Initial hold (min)			13.	13.
Final hold (min)			5.	5.
I	1264.	1264.	1297.	1298.	1265.
Reference	Bos, Woerdenbag, et al., 1997	Bos, Woerdenbag, et al., 1997, 2	Mariaca, Berger, et al., 1997	Mariaca, Berger, et al., 1997	Salgueiro, Vila, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	OV-101	DB-1	HP-1
Column length (m)	60.	30.	50.	60.	25.
Carrier gas	He		He	He	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.32	0.32
Phase thickness (μm)	0.25	0.25		0.50	0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	220.	300.	250.	250.	220.
Heat rate (K/min)	3.	4.	2.	8.	4.
Initial hold (min)		2.		1.	2.
Final hold (min)		5.		6.	20.
I	1271.	1282.2	1268.	1278.	1265.
Reference	Werkhoff and Güntert, 1997	Gawdzik, Mardarowicz, et al., 1996	Orav, Kailas, et al., 1996	Sagrero-Nieves and Bartley, 1996	Thanh, Dung, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-5 MS	HP-5	HP-5	OV-101
Column length (m)	50.	30.			50.
Carrier gas	He	Helium
Substrate
Column diameter (mm)	0.2	0.25			0.25
Phase thickness (μm)	0.5
T_start (C)	70.	50.	40.	40.	80.
T_end (C)	180.	250.	210.	210.	200.
Heat rate (K/min)	1.	4.	2.	2.	2.
Initial hold (min)
Final hold (min)
I	1268.	1287.	1291.	1292.	1274.
Reference	Orav, Kuningas, et al., 1995	Gomez and Ledbetter, 1994	Collin, Deslauriers, et al., 1993	Collin, Deslauriers, et al., 1993	Tamura, Yang, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	DB-1	BP-1	OV-1
Column length (m)	50.	52.	30.	25.	60.
Carrier gas		Helium	N2		Helium
Substrate
Column diameter (mm)	0.25	0.26		0.33	0.50
Phase thickness (μm)					1.2
T_start (C)	80.	40.	80.	45.	40.
T_end (C)	200.	200.	220.	180.	220.
Heat rate (K/min)	2.	3.	4.	3.	2.
Initial hold (min)		0.		3.
Final hold (min)		0.
I	1275.	1272.	1263.	1262.	1267.
Reference	Tamura, Yang, et al., 1993	Tkachenko and Zenkevich, 1993	Velasco-Negueruela, Pérez Alonso, et al., 1991	Wyllie, Brophy, et al., 1990	Wahab, Aboutabl, et al., 1987
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-101	SE-30+Igepal	SE-30+Igepal
Column length (m)	10.	50.	100.	100.
Carrier gas	H2	He
Substrate
Column diameter (mm)	0.25	0.31	0.25	0.25
Phase thickness (μm)	0.25
T_start (C)	50.	0.	70.	70.
T_end (C)	250.	225.	170.	170.
Heat rate (K/min)	5.	3.	1.	1.
Initial hold (min)		1.
Final hold (min)
I	1269.	1261.	1280.	1287.
Reference	Perry, Baxter, et al., 1986	del Rosario, de Lumen, et al., 1984	Shibamoto and Jennings, 1977	Shibamoto and Jennings, 1977
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

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Salehi, Fakhari, et al., 2007
Salehi, P.; Fakhari, A.R.; Ebrahimi, S.N.; Heydari, R., Rapid essential oil screening of Rosmarinus officinalis L. by hydrodistillation-headspace solvent microextraction, Flavour Fragr. J., 2007, 22, 4, 280-285, https://doi.org/10.1002/ffj.1793 . [all data]

Sereshti and Samadi, 2007
Sereshti, H.; Samadi, S., Comparison of hydrodistillation-headspace liquid phase microextraction techniques with hydrodistillation in determination of essential oils in Artemisia Haussknechtii Boiss, JSUT, 2007, 33, 2, 7-17. [all data]

Tsokou, Georgopoulos, et al., 2007
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Tzakou, O.; Bazos, I.; Yannitsaros, A., Volatile metabolites of Pistacia atlantica Desf. from Greece, Flavour Fragr. J., 2007, 22, 5, 358-362, https://doi.org/10.1002/ffj.1805 . [all data]

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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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