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Heptachlor

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Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryOV-1190.1889.Erdmann, Rochholz, et al., 1992 
CapillaryOV-1220.1910.Erdmann, Rochholz, et al., 1992 
PackedOV-1200.1891.Dubsky, Hána, et al., 1979Column length: 2. m

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
PackedSE-301890.Ramsey, Lee, et al., 1980He, Chromosorb G HP (80-100 mesh); Column length: 1.5 m; Program: not specified

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryOV-11861.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1. K/min; Tend: 240. C
CapillaryOV-11863.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1. K/min; Tend: 240. C
CapillaryOV-11865.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1.3 K/min; Tend: 240. C
CapillaryOV-11867.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1.3 K/min; Tend: 240. C
CapillaryOV-11861.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1.5 K/min; Tend: 240. C
CapillaryOV-11863.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 1.5 K/min; Tend: 240. C
CapillaryOV-11866.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 2. K/min; Tend: 240. C
CapillaryOV-11867.de Paoli, Taccheo-Barbina, et al., 199125. m/0.32 mm/0.10 «mu»m, 160. C @ 1. min, 2. K/min; Tend: 240. C
PackedSE-301870.Perrigo and Peel, 1981N2, Chromosorb W, 130. C @ 2. min, 8. K/min, 290. C @ 8. min; Column length: 1.8 m

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-11860.7Dearth and Hites, 1991H2, 50. C @ 1. min, 3. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tend: 320. C
CapillaryDB-51886.1Dearth and Hites, 1991H2, 50. C @ 1. min, 3. K/min; Column length: 30. m; Column diameter: 0.25 mm; Tend: 320. C
PackedSE-301930.Marozzi, Gambaro, et al., 1982Gas Chrom P, 2.5 K/min; Column length: 2. m; Tstart: 120. C; Tend: 200. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
Capillary5 % Phenyl methyl siloxane1922.Department of Food Safety and Welfare, 200630. m/0.25 mm/0.25 «mu»m, Helium; Program: 50 0C(1 min) 25 0C/min -> 125 0C 10 0C/min -> 300 0C (10 min)
Capillary5 % Phenyl methyl siloxane1920.Department of Food Safety and Welfare, 200630. m/0.25 mm/0.25 «mu»m, Helium; Program: 50 0C(1 min) 25 0C/min -> 125 0C 10 0C/min -> 300 0C (10 min)
CapillaryUltra-11841.Tameo and Kiyos, 1991Program: not specified
CapillaryOV-11873.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified
CapillaryOV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.1870.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified
CapillaryOV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.1873.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified
CapillaryOV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.1890.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified
OtherMethyl Silicone1880.Ardrey and Moffat, 1981Program: not specified

Normal alkane RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryCarbowax 20M2484.Tameo and Kiyos, 1991Program: not specified
CapillarySuperox 0.6; Carbowax 20M2505.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified
CapillaryCarbowax 400, Carbowax 20M, Carbowax 1540, Carbowax 4000, Superox 06, PEG 20M, etc.2505.Waggott and Davies, 1984Hydrogen; Column length: 50. m; Column diameter: 0.32 mm; Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Erdmann, Rochholz, et al., 1992
Erdmann, F.; Rochholz, G.; Schütz, H., Retention-indices on OV-1 of approximately 170 commonly used pesticides, Mikrochim. Acta, 1992, 106, 3-6, 219-226, https://doi.org/10.1007/BF01242093 . [all data]

Dubsky, Hána, et al., 1979
Dubsky, H.; Hána, K.; Komárková, M.; Rittich, B., Stanoveni residui chlórovanych pesticidu plynovou chromatografii, Vet. Med. (Prague), 1979, 24, 3, 493-498. [all data]

Ramsey, Lee, et al., 1980
Ramsey, J.D.; Lee, T.D.; Osselton, M.D.; Moffat, A.C., Gas-liquid chromatographic retention indices of 296 non-drug substances on SE-30 or OV-1 likely to be encountered in toxicological analyses, J. Chromatogr., 1980, 184, 2, 185-206, https://doi.org/10.1016/S0021-9673(00)85641-1 . [all data]

de Paoli, Taccheo-Barbina, et al., 1991
de Paoli, M.; Taccheo-Barbina, M.; Bontempelli, G., Gas chromatographic system for the identification of halogenated pesticides by retention indices using n-alkanes as standards, J. Chromatogr., 1991, 547, 355-365, https://doi.org/10.1016/S0021-9673(01)88659-3 . [all data]

Perrigo and Peel, 1981
Perrigo, B.J.; Peel, H.W., The use of retention indices and temperature-programmed gas chromatography in analytical toxicology, J. Chromatogr. Sci., 1981, 19, 5, 219-226, https://doi.org/10.1093/chromsci/19.5.219 . [all data]

Dearth and Hites, 1991
Dearth, M.A.; Hites, R.A., Complete analysis of technical chlordane using negative ionization mass spectrometry, Environ. Sci. Technol., 1991, 25, 2, 245-254, https://doi.org/10.1021/es00014a005 . [all data]

Marozzi, Gambaro, et al., 1982
Marozzi, E.; Gambaro, V.; Saligari, E.; Mariani, R.; Lodi, F., Use of the retention index in gas chromatographic studies of drugs, J. Anal. Toxicol., 1982, 6, 4, 185-192, https://doi.org/10.1093/jat/6.4.185 . [all data]

Department of Food Safety and Welfare, 2006
Department of Food Safety, Ministry of Health; Welfare, Analytical methods for residual compositional substances of agricultural chemicals, feed aadditives, and veterinary drugs in foods, 2006, retrieved from http://www.mhlw.go.jp/english/topics/foodsafety/positivelist060228/de/060526-1a.pdf. [all data]

Tameo and Kiyos, 1991
Tameo, O.; Kiyos, I., Simultaneous determination of pesticides by capillary gas chromatography, Cannot be traslated (in Japan), 1991, 14, 2, 109-122. [all data]

Waggott and Davies, 1984
Waggott, A.; Davies, I.W., Identification of organic pollutants using linear temperature programmed retention indices (LTPRIs) - Part II, 1984, retrieved from http://dwi.defra.gov.uk/research/completed-research/reports/dwi0383.pdf. [all data]

Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C., Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase, J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1 . [all data]


Notes

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