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Camphor

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5MSDB-5RTX-1
Column length (m) 30.30.30.30.60.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.220.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.250.280.240.230.
Heat rate (K/min) 3.2.3.3.2.
Initial hold (min)  8. 2. 
Final hold (min)  30.  30.
I 1154.1147.1146.1147.1122.
ReferenceBaccouri, Ben Temime, et al., 2007Benkaci-Ali, Baaliouamer, et al., 2007Kundakovic, Fokialakis, et al., 2007Martins, Santos, et al., 2007Muselli, Rossi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-101HP-101SPB-1HP-5MS
Column length (m) 60.25.25.30.30.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.220.200.20.250.25
Phase thickness (mum) 0.250.200.20.250.25
Tstart (C) 60.70.70.50.60.
Tend (C) 230.200.200.250.280.
Heat rate (K/min) 2.3.3.5.4.
Initial hold (min)  2.2.3.5.
Final hold (min) 35.15.15.15. 
I 1125.1126.1109.1139.1143.
ReferencePaolini J., Costa J., et al., 2007Politeo, Jukic, et al., 2007Politeo, Jukic, et al., 2007, 2Radulovic, Lazarevic, et al., 2007Radulovic, Lazarevic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-5HP-5MSDB-5HP-5MSSPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.50.80.50.
Tend (C) 250.280.250.300.250.
Heat rate (K/min) 3.3.3.4.5.
Initial hold (min)     3.
Final hold (min)   10. 15.
I 1142.1150.1145.1150.81139.
ReferenceSimoniatto, Bonani, et al., 2007Vagionas, Ngassapa, et al., 2007Yu, Liao, et al., 2007Zeng, Zhao, et al., 2007Blagojevic, Radulovic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5BP-1BP-1DB-5
Column length (m) 30.30.50.50.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.20.250.220.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 250.240.220.220.240.
Heat rate (K/min) 5.3.2.2.3.
Initial hold (min) 3.   3.
Final hold (min) 15. 20.20.3.
I 1143.1154.1115.1120.1144.
ReferenceBlagojevic, Radulovic, et al., 2006Block, Flamini, et al., 2006Boti, Bighelli, et al., 2006Bousmaha, Boti, et al., 2006Dob, Dahmane, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-5HP-5HP-5MSHP-5MS
Column length (m) 50.50.30.20.30.
Carrier gas HeN2He He
Substrate      
Column diameter (mm) 0.220.20.250.250.25
Phase thickness (mum) 0.250.320.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.220.250.240.280.
Heat rate (K/min) 2.5.3.5.3.
Initial hold (min)  3. 4. 
Final hold (min) 20.5. 15. 
I 1121.1143.1145.1144.1143.
ReferenceDuquesnoy, Dinh, et al., 2006Esmaeili, Nematollahi, et al., 2006Javidnia, Miri, et al., 2006Kallio, Jussila, et al., 2006Kukic J., Petrovic S., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSDB-5SPB-1DB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.20.25
Phase thickness (mum) 0.250.250.250.20.25
Tstart (C) 60.60.60.70.50.
Tend (C) 250.280.280.220.265.
Heat rate (K/min) 10.3.3.3.2.5
Initial hold (min) 2.    
Final hold (min) 10.  15. 
I 1155.1125.1138.1118.1115.
ReferenceLiu J.M., Nan P., et al., 2006Pavlovic, Kovacevic, et al., 2006Pavlovic, Tzakou, et al., 2006Pinto, Pina-Vaz, et al., 2006Ramezani, Behravan, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1HP-5MSDB-5DB-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.20.250.250.250.25
Tstart (C) 70.60.50.50.50.
Tend (C) 220.280.250.250.285.
Heat rate (K/min) 3.4.5.5.4.3
Initial hold (min)  5.2.2. 
Final hold (min) 15.    
I 1118.1145.1146.1146.1136.
ReferenceSalgueiro L.R., Pinto E., et al., 2006Saroglou, Dorizas, et al., 2006Su, Ho, et al., 2006Su, Ho, et al., 2006, 2Vujisic L., Vuckovic I., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBSPB-1DB-5BP-1SE-54
Column length (m) 25.30.30.50.50.
Carrier gas H2HeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.20.220.25
Phase thickness (mum)  0.250.250.250.27
Tstart (C) 80.50.50.60.50.
Tend (C) 270.250.250.220.300.
Heat rate (K/min) 10.5.5.2.5.
Initial hold (min)  3.3.  
Final hold (min)  15.15.20. 
I 1123.1139.1126.1123.1144.
ReferenceZiegenbein, Hanssen, et al., 2006Boskovic, Radulovic, et al., 2005Boskovic, Radulovic, et al., 2005Boti J.B., Koukoua G., et al., 2005Brantner, Pfeifhofer, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-1DB-15 % Phenyl methyl siloxaneCP Sil 5 CB
Column length (m) 60.30.30.30.50.
Carrier gas  N2N2HeH2
Substrate      
Column diameter (mm) 0.220.320.320.250.22
Phase thickness (mum) 0.250.250.251.0.13
Tstart (C) 60.50.50.40.40.
Tend (C) 220.260.260.250.300.
Heat rate (K/min) 2.2.2.7.4.
Initial hold (min)  3.3.10. 
Final hold (min) 20.5.5.5.10.
I 1122.1118.1143.1189.1122.
ReferenceCozzani, Muselli, et al., 2005Dob, Berramdane, et al., 2005Dob, Berramdane, et al., 2005, 2Estevez, Ventanas, et al., 2005Idzojtic, Kajba, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSDB-5DB-1Mega 5MS
Column length (m) 25.30.30.30.30.
Carrier gas  HeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.40.50.40.
Tend (C) 180.250.260.200.240.
Heat rate (K/min) 3.4.2.5.3.
Initial hold (min) 10.2.5. 2.
Final hold (min) 10.20.20.  
I 1144.1143.1143.1127.1127.
Referencebin Jantan, Yalvema, et al., 2005Pino, Mesa, et al., 2005Senatore, Napolitano, et al., 2005Tchoumbougnang, Zollo, et al., 2005Verzera, Trozzi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSSPB-1SPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.250.250.250.2
Tstart (C) 80.80.80.70.70.
Tend (C) 290.290.290.220.220.
Heat rate (K/min) 2.4.6.3.3.
Initial hold (min)      
Final hold (min)    15.15.
I 1145.31149.31151.81121.1117.
ReferenceZhao, Liang, et al., 2005Zhao, Liang, et al., 2005Zhao, Liang, et al., 2005Antunes, Sevinate-Pinto, et al., 2004Cavaleiro, Salgueiro, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBP-1DB-5HP-5MSDB-5MS
Column length (m) 30.50.30.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.40.
Tend (C) 280.220.260.280.280.
Heat rate (K/min) 3.2.3.4.4.
Initial hold (min)    5.2.
Final hold (min)  20.   
I 1144.1121.1145.1146.1147.
ReferenceChorianopoulos, Kalpoutzakis, et al., 2004Gonny, Bradesi, et al., 2004Javidnia, Miri, et al., 2004Karioti, Hadjipavlou-Litina, et al., 2004Mardarowicz, Wianowska, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-5BP-1DB-1DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2 He
Substrate      
Column diameter (mm) 0.20.250.320.250.25
Phase thickness (mum) 0.20.250.250.250.25
Tstart (C) 70.60.60.50.50.
Tend (C) 220.250.220.265.290.
Heat rate (K/min) 3.4.5.2.54.
Initial hold (min)  2.   
Final hold (min) 15.20.13.  
I 1121.1143.1121.1117.1140.
ReferenceMoldão-Martins, Beirão-da-Costa, et al., 2004Pino, Marbot, et al., 2004Raina, Kumar, et al., 2004Ramezani, Behravan, et al., 2004Reis, Pansarim, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5HP-5MSDB-5MSDB-5MS
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.250.330.250.250.25
Tstart (C) 50.60.60.40.40.
Tend (C) 250.240.280.200.200.
Heat rate (K/min) 3.3.3.4.4.
Initial hold (min)    5.5.
Final hold (min)  7. 20.20.
I 1147.1150.1126.1149.1150.
ReferenceSalido, Valenzuela, et al., 2004Sartoratto, Machado, et al., 2004Tzakou, Vagias, et al., 2004Yu, Kim, et al., 2004Yu, Kim, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5RTX-1DB-1
Column length (m) 25.30.30.60.30.
Carrier gas N2N2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 75.60.60.60.40.
Tend (C) 210.220.240.230.250.
Heat rate (K/min) 3.5.3.2.2.
Initial hold (min) 10.10.  5.
Final hold (min) 1.  45.20.
I 1146.1144.1145.1123.1105.
Referencebin Ahmad and bin Jantan, 2003Angelini, Carpanese, et al., 2003Bader, Flamini, et al., 2003Cavalli, Tomi, et al., 2003de Feo, Bruno, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2N2 HeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.60.25.75.75.
Tend (C) 220.220.150.230.230.
Heat rate (K/min) 5.5.3.3.3.
Initial hold (min) 10.10.5.10.10.
Final hold (min)    20. 
I 1145.1145.1142.1146.1149.
ReferenceFlamini, Luigi Cioni, et al., 2003Flamini, Luigi Cioni, et al., 2003, 2Isidorov, Vinogorova, et al., 2003Jantan, Ling, et al., 2003bin Jantan, Yassin, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5HP-5MSHP-5
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 260.280.240.280.280.
Heat rate (K/min) 4.4.3.3.3.
Initial hold (min)  5.   
Final hold (min)      
I 1145.1142.1145.1144.1143.
ReferenceJavidnia, Miri, et al., 2003Karioti, Skaltsa, et al., 2003Macchioni, Cioni, et al., 2003Mimica-Dukic, Kujundzic, et al., 2003Ngassapa, Runyoro, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1MS5HP-5DB-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.40.40.60.60.
Tend (C) 250.270.180.280.240.
Heat rate (K/min) 3.2.3.4.3.
Initial hold (min)  5. 5. 
Final hold (min)  20.   
I 1144.1106.1141.1143.1145.
ReferenceSalido, Altarejos, et al., 2003Senatore, Lentini, et al., 2003Shao, Marriott, et al., 2003Skaltsa, Demetzos, et al., 2003Tampieri, Galuppi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5Mega 5MSDB-5HP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.70.50.60.
Tend (C) 280.240.230.280.240.
Heat rate (K/min) 3.3.4.3.3.
Initial hold (min)  2.2.5. 
Final hold (min)   20.  
I 1145.1127.1149.1143.1145.
ReferenceTzakou, Couladis, et al., 2003Verzera, Trozzi, et al., 2003Choi, Kim. M.-S.L., et al., 2002Demetzos, Angelopoulou, et al., 2002Flamini, Cioni, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-5 MSSE-30HP-5RTX-5
Column length (m) 30.30.25.30.30.
Carrier gas N2HeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.45.60.60.45.
Tend (C) 220.180.180.280.300.
Heat rate (K/min) 5.2.53.3.3.
Initial hold (min) 10.10.10.5.6.
Final hold (min)   10. 10.
I 1145.1144.1126.1143.1148.
ReferenceFlamini, Cioni, et al., 2002, 2Hudaib, Speroni, et al., 2002bin Jantan, Ayop, et al., 2002Magiatis, Skaltsounis, et al., 2002Mondello, Zappia, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1CP Sil 8 CBCP Sil 5 CBCP Sil 5 CBDB-1
Column length (m) 24.60.25.30.50.
Carrier gas HeHeN2H2He
Substrate      
Column diameter (mm) 0.320.250.250.250.22
Phase thickness (mum) 0.170.250.250.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 250.250.280.280.220.
Heat rate (K/min) 4.4.4.2.2.
Initial hold (min) 2.8.6.10. 
Final hold (min) 20.10. 40.20.
I 1114.1151.1108.1108.1122.
ReferenceNath, Sarma, et al., 2002Oruna-Concha, Ames, et al., 2002Pino, Marbot, et al., 2002Pino, Marbot, et al., 2002, 2Pintore, Usai, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSRTX-5RTX-5HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.45.45.60.60.
Tend (C) 250.250.250.280.380.
Heat rate (K/min) 5.3.3.3.3.
Initial hold (min) 2.6.6.5. 
Final hold (min) 5.    
I 1124.1143.1152.1140.1147.
ReferenceShang, Hu, et al., 2002Shellie, Mondello, et al., 2002Shellie, Mondello, et al., 2002Aligiannis, Kalpoutzakis, et al., 2001Couladis, Tsortanidou, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SE-30DB-5BP-1HP-5MS
Column length (m) 30.25.30.50.30.
Carrier gas HeN2H2 He
Substrate      
Column diameter (mm) 0.250.200.250.220.25
Phase thickness (mum) 0.50 0.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 280.180.240.220.250.
Heat rate (K/min) 3.3.3.2.3.
Initial hold (min)  10.   
Final hold (min)  1. 20. 
I 1145.1149.1142.1123.1147.
ReferenceCouladis, Tzakou, et al., 2001bin Jantan, Basni, et al., 2001Nogueira, Bittrich, et al., 2001Rezzi, Cavaleiro, et al., 2001Salido, Altarejos, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSBPX-5HP-5HP-101SE-30
Column length (m) 30.50.30.25.50.
Carrier gas HeH2HeHe 
Substrate      
Column diameter (mm) 0.250.220.250.20.2
Phase thickness (mum) 0.250.250.250.2 
Tstart (C) 60.60.40.70.50.
Tend (C) 280.180.200.200.250.
Heat rate (K/min) 4.4.2.3.6.
Initial hold (min) 5.5.5.2. 
Final hold (min)  5.20.10. 
I 1143.1170.1138.1122.1136.
ReferenceSkaltsa, Mavrommati, et al., 2001Zabaras and Wyllie, 2001Kim, Thuy, et al., 2000Milos and Radonic, 2000Paramonov, Khalilova, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBMega 5MSDB-1DB-1DB-1
Column length (m) 50.30.60.60.60.
Carrier gas H2He HeHe
Substrate      
Column diameter (mm) 0.220.250.320.320.25
Phase thickness (mum) 0.130.251. 0.25
Tstart (C) 40.40.-50.60.50.
Tend (C) 300.240.175.230.220.
Heat rate (K/min) 4.3.6.3.4.
Initial hold (min)  2.2.  
Final hold (min) 10.  5. 
I 1133.1127.1136.61126.1126.
ReferencePfeifhofer, 2000Verzera, la Rosa, et al., 2000Helmig, Klinger, et al., 1999Javidnia and Shafiee, 1999Mirza and Sefidkon, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeOV-1CP Sil 5 CBOV-1DB-5
Column length (m) 50.20.25.25.30.
Carrier gas N2HeHe  
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.170.3 0.30.25
Tstart (C) 80.45.60.50.50.
Tend (C) 200.220.260.200.250.
Heat rate (K/min) 2.10.5.3.3.
Initial hold (min)  5. 1. 
Final hold (min)  10. 20. 
I 1136.1120.1126.1112.1143.
ReferenceSumathykutty, Rao, et al., 1999Valero, Sanz, et al., 1999Weyerstahl, Marschall, et al., 1999Bicchi, Rubiolo, et al., 1998Isidorov, Zenkevich, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1Methyl SiliconeDB-5DB-1Ultra-1
Column length (m) 50. 30.60.25.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.22 0.260.250.32
Phase thickness (mum) 0.25 0.250.250.17
Tstart (C) 60.50.50.40.50.
Tend (C) 220.250.225.160.320.
Heat rate (K/min) 2.4.2.2.6.
Initial hold (min)    3. 
Final hold (min) 20. 20.15. 
I 1126.1122.1144.1139.1128.
ReferenceTam, An, et al., 1998Analytical Methods Committee, 1997Sagrero-Nieves, Bartley, et al., 1997Stashenko, Martinez, et al., 1995Ahmad, Sirat, et al., 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101HP-1DB-5OV-101
Column length (m) 50.50.50.0.3226.
Carrier gas N2N2HeH2 
Substrate      
Column diameter (mm) 0.250.250.321.0.26
Phase thickness (mum)   1.05 0.3
Tstart (C) 80.80.40.30.100.
Tend (C) 200.200.230.180.240.
Heat rate (K/min) 2.2.2.1.52.
Initial hold (min)    5. 
Final hold (min)   40.  
I 1125.1125.1131.1147.1126.5
ReferenceYang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992Tang, Zhang, et al., 1990Guichard and Souty, 1988Wang and Sun, 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101OV-101OV-101
Column length (m) 26.26.21.521.526.5
Carrier gas      
Substrate      
Column diameter (mm) 0.260.260.270.270.25
Phase thickness (mum) 0.30.32.0.140.14
Tstart (C) 60.60.60.60.70.
Tend (C) 240.240.240.240.240.
Heat rate (K/min) 2.8.6.6.9.
Initial hold (min)     4.08
Final hold (min)      
I 1116.01129.71141.21119.71129.2
ReferenceWang and Sun, 1987Wang and Sun, 1987Wang and Sun, 1987Wang and Sun, 1987Wang and Sun, 1987, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedCapillary
Active phase OV-101OV-101OV-101
Column length (m) 24.2. 
Carrier gas  Ar 
Substrate  W-AW-DMCS 
Column diameter (mm) 0.26  
Phase thickness (mum) 0.5  
Tstart (C) 80.100.100.
Tend (C) 240.  
Heat rate (K/min) 6.2.2.
Initial hold (min)    
Final hold (min)    
I 1134.741133.1133.
ReferenceWang, Zhong, et al., 1987Szabolcs, Benecke, et al., 1985Benecke, Thieme, et al., 1982
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Pavlovic, Kovacevic, et al., 2006
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Pinto, Pina-Vaz, et al., 2006
Pinto, E.; Pina-Vaz, C.; Salgueiro, L.; Goncalves, M.J.; Costa-de-Oliveira, S.; Cavaleiro, C.; Palmeira, A.; Rodrigues, A.; Martinez-de-Oliveira, J., Antifuncal activity of the essential oil Thymus pulegioides on Candida, Aspergillus and dermatophyte species, Journal of Medical Microbiology, 2006, 55, 10, 1367-1373, https://doi.org/10.1099/jmm.0.46443-0 . [all data]

Ramezani, Behravan, et al., 2006
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Su, Ho, et al., 2006
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Vujisic L., Vuckovic I., et al., 2006
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Ziegenbein, Hanssen, et al., 2006
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Boskovic, Radulovic, et al., 2005
Boskovic, Z.; Radulovic, N.; Stojanovic, G., Essential oil composition of four Achillea species from the balkans and its chemotaxonomic significance, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 6, 674-678, https://doi.org/10.1007/s10600-006-0009-6 . [all data]

Boti J.B., Koukoua G., et al., 2005
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Brantner, Pfeifhofer, et al., 2005
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Cozzani, Muselli, et al., 2005
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Dob, Berramdane, et al., 2005
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Pino, Mesa, et al., 2005
Pino, J.A.; Mesa, J.; Muñoz, Y.; Martí, M.P.; Marbot, R., Volatile components from mango (Mangifera indica L.) cultivars, J. Agric. Food Chem., 2005, 53, 6, 2213-2223, https://doi.org/10.1021/jf0402633 . [all data]

Senatore, Napolitano, et al., 2005
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Tchoumbougnang, Zollo, et al., 2005
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Verzera, Trozzi, et al., 2005
Verzera, A.; Trozzi, A.; Zappala, M.; Condurso, C.; Cotroneo, A., Essential Oil Composition of Citrus meyerii Y. Tan. and Citrus medica L. cv. Diamante and Their Lemon Hybrids, J. Agric. Food Chem., 2005, 53, 12, 4890-4894, https://doi.org/10.1021/jf047879c . [all data]

Zhao, Liang, et al., 2005
Zhao, C.-X.; Liang, Y.-Z.; Fang, H.-Z.; Li, X.-N., Temperature-programmed retention indices for gas chromatography-mass spectroscopy analysis of plant essential oils, J. Chromatogr. A, 2005, 1096, 1-2, 76-85, https://doi.org/10.1016/j.chroma.2005.09.067 . [all data]

Antunes, Sevinate-Pinto, et al., 2004
Antunes, T.; Sevinate-Pinto, I.; Barroso, J.G.; Cavaleiro, C.; Salgueiro, L.R., Micromorphology of trichomes and composition of essential oil of Teucrium capitatum, Flavour Fragr. J., 2004, 19, 4, 336-340, https://doi.org/10.1002/ffj.1310 . [all data]

Cavaleiro, Salgueiro, et al., 2004
Cavaleiro, C.; Salgueiro, L.R.; Miguel, M.G.; da Cunha, A.P., Analysis by gas chromatography?mass spectrometry of the volatile components of Teucrium lusitanicum and Teucrium algarbiensis, J. Chromatogr. A, 2004, 1033, 1, 187-190, https://doi.org/10.1016/j.chroma.2004.01.005 . [all data]

Chorianopoulos, Kalpoutzakis, et al., 2004
Chorianopoulos, N.; Kalpoutzakis, E.; Aligiannis, N.; Mitaku, S.; Nychas, G.-J.; Haroutounian, S.A., Essential oils of Satureja, Origanum, and Thymus species: chemical composition and antibacterial activities against foodborne pathogens, J. Agric. Food Chem., 2004, 52, 26, 8261-8267, https://doi.org/10.1021/jf049113i . [all data]

Gonny, Bradesi, et al., 2004
Gonny, M.; Bradesi, P.; Casanova, J., Identification of the components of the essential oil from wild Corsican Daucus carota L. using 13C-NMR spectroscopy, Flavour Fragr. J., 2004, 19, 5, 424-433, https://doi.org/10.1002/ffj.1330 . [all data]

Javidnia, Miri, et al., 2004
Javidnia, K.; Miri, R.; Sadeghpour, H., Composition of the volatile oil of Achillea wilhelmsii C. Koch from Iran, DARU, 2004, 12, 2, 63-66, retrieved from http://www1.tums.ac.ir/daru/. [all data]

Karioti, Hadjipavlou-Litina, et al., 2004
Karioti, A.; Hadjipavlou-Litina, D.; Mensah, M.L.K.; Fleischer, T.C.; Skaltsa, H., Composition and antioxidant activity of the essential oils of Xylopia aethiopica (Dun) A. Rich. (Annonaceae) leaves, stem bark, root bark, and fresh and dried fruits, growing in Ghana, J. Agric. Food Chem., 2004, 52, 26, 8094-8098, https://doi.org/10.1021/jf040150j . [all data]

Mardarowicz, Wianowska, et al., 2004
Mardarowicz, M.; Wianowska, D.; Dawidowicz, A.L.; Sawicki, R., The influence of sample treatment on SPME extracts from conifers. I. Comparison of terpene composition in Engelmann Spruce (Picea engelmanii) using hydrodistillation, SPME and PLE, Annales Universitatis Mariae Curie-Sklodowska Lublin - Polonia, 2004, 59, 3, 25-42. [all data]

Moldão-Martins, Beirão-da-Costa, et al., 2004
Moldão-Martins, M.; Beirão-da-Costa, S.; Neves, C.; Cavaleiro, C.; Salgueiro, L.; Beirão-da-Costa, M.L., Olive oil flavoured by the essential oils of Mentha × piperita and Thymus mastichina L., Food Qual. Pref., 2004, 15, 5, 447-452, https://doi.org/10.1016/j.foodqual.2003.08.001 . [all data]

Pino, Marbot, et al., 2004
Pino, J.A.; Marbot, R.; Rosado, A.; Vázquez, C., Volatile constituents of Malay rose apple [Syzygium malaccense (L.) Merr. Perry], Flavour Fragr. J., 2004, 19, 1, 32-35, https://doi.org/10.1002/ffj.1269 . [all data]

Raina, Kumar, et al., 2004
Raina, V.K.; Kumar, A.; Srivastava, S.K.; Syamsundar, K.V.; Kahol, A.P., Essential oil composition of 'kewda' (Pandanus odoratissimus) from India, Flavour Fragr. J., 2004, 19, 5, 434-436, https://doi.org/10.1002/ffj.1331 . [all data]

Ramezani, Behravan, et al., 2004
Ramezani, M.; Behravan, J.; Yazdinezhad, A., Chemical composition and antimicrobial activity of the volatile oil of Artemisia khorassanica from Iran, Pharm. Biol., 2004, 42, 8, 599-602, https://doi.org/10.1080/13880200490902482 . [all data]

Reis, Pansarim, et al., 2004
Reis, M.G.; Pansarim, E.R.; da Silva, U.F.; Estanislau do Amaral, M.C.; Marsaioli, A.J., Pollinator attraction devices (floral fragrances) of some Brazilian orchids, Arkivoc, 2004, 6, 89-97. [all data]

Salido, Valenzuela, et al., 2004
Salido, S.; Valenzuela, L.R.; Altarejos, J.; Nogueras, M.; Sánchez, A.; Cano, E., Composition and infraspecific variability of Artemisia herba-alba from southern Spain, Biochem. Syst. Ecol., 2004, 32, 3, 265-277, https://doi.org/10.1016/j.bse.2003.09.002 . [all data]

Sartoratto, Machado, et al., 2004
Sartoratto, A.; Machado, A.L.M.; Delarmelina, C.; Figueira, G.M.; Duarte, M.C.T.; Rehder, V.L.G., Composition and antimicrobial activity of essential oils from aromatic plants used in Brazil, Braz. J. Microbiol., 2004, 35, 4, 275-280, https://doi.org/10.1590/S1517-83822004000300001 . [all data]

Tzakou, Vagias, et al., 2004
Tzakou, O.; Vagias, C.; Gani, A.; Yannitsaros, A., Volatile constituents of essential oils isolated at different growth stages from three Conyza species growing in Greece, Flavour Fragr. J., 2004, 19, 425-428. [all data]

Yu, Kim, et al., 2004
Yu, E.J.; Kim, T.H.; Kim, K.H.; Lee, H.J., Characterization of aroma-active compounds of Abies nephrolepis (Khingan fir) needles using aroma extract dilution analysis, Flavour Fragr. J., 2004, 19, 1, 74-79, https://doi.org/10.1002/ffj.1314 . [all data]

bin Ahmad and bin Jantan, 2003
bin Ahmad, F.; bin Jantan, I., Chemical constituents of the essential oils of Goniothalamus uvariodes King, Flavour Fragr. J., 2003, 18, 2, 128-130, https://doi.org/10.1002/ffj.1142 . [all data]

Angelini, Carpanese, et al., 2003
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Bader, Flamini, et al., 2003
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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References