Camphor

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-1RTX-1HP-5 MSHP-5 MS
Column length (m) 60.30.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.40.50.
Tend (C) 250.240.230.250.320.
Heat rate (K/min) 3.3.2.3.5.
Initial hold (min) 1.  1.5.
Final hold (min) 20. 5.3. 
I 1145.1126.1123.1144.1143.
ReferenceSardashti, Valizadeh, et al., 2013Alizadeh and Shaabani, 2012Bendiabdellah, El Amine Dib, et al., 2012Jian-Yu, Zhu, et al., 2012Nawrath, Mgode, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase VF-5 MSHP-5HP-5HP-5HP-5 MS
Column length (m) 60.25.25.25.30.
Carrier gas HeliumHydrogenHydrogenHydrogenHelium
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm) 0.250.520.520.520.25
Tstart (C) 40.40.40.40.50.
Tend (C) 250.280.280.280.250.
Heat rate (K/min) 4.4.4.4.7.
Initial hold (min) 2.   1.
Final hold (min)  10.10.10.5.
I 1155.1138.1139.1139.1143.
ReferenceSrisajjalerwaja, Apichartsrangkoon, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Zouari, Ayadi, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSVF-5 MSVF-5 MSDB-1
Column length (m) 30.30.60.60.50.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.35.30.30.60.
Tend (C) 220.250.260.260.250.
Heat rate (K/min) 4.5.2.2.8.
Initial hold (min) 20.3.   
Final hold (min) 20.10.28.28. 
I 1126.1180.1149.1152.1125.
ReferenceFeizbakhsh and Naeemy, 2011Kadri, Zarai, et al., 2011Leffingwell and Alford, 2011Leffingwell and Alford, 2011Misharina T., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CBHP-5HP-5 MSZB-5 MSZB-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas NitrogenNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.260.250.250.250.25
Tstart (C) 45.50.30.60.60.
Tend (C) 280.280.250.290.290.
Heat rate (K/min) 3.5.5.5.5.
Initial hold (min)  1.3.  
Final hold (min) 22.1.10.  
I 1126.1122.1174.1149.1153.
ReferenceMothana, Hasson, et al., 2011Tekaya-Karoui, Boughalleb, et al., 2011Zarai, Kadri, et al., 2011Boix, Victorio, et al., 2010Boix, Victorio, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1DB-5DB-5 MSBP-1SPB-1
Column length (m) 60.30.60. 30.
Carrier gas HeliumHeliumHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.220.250.25 0.20
Phase thickness (μm) 0.250.250.25 0.20
Tstart (C) 60.50.40.60.70.
Tend (C) 230.250.250.220.220.
Heat rate (K/min) 2.2.5.5.3.
Initial hold (min)   15.10. 
Final hold (min) 30. 15.30.15.
I 1123.1146.1149.1122.1117.
ReferenceDib, Djabou, et al., 2010Ho, Wang, et al., 2010Mesa-Arango, Betancur-Galvis, et al., 2010Mishra, Chaudhary, et al., 2010Neves, Rosa, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSHP-5 MSSLB-5 MSSLB-5 MS
Column length (m) 30.30.30.10.10.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.100.10
Phase thickness (μm) 0.250.250.250.100.10
Tstart (C) 100.70.60.50.50.
Tend (C) 220.290.220.250.250.
Heat rate (K/min) 2.5.6.10.10.
Initial hold (min)   3.  
Final hold (min)  10.   
I 1146.1150.1126.1146.1149.
ReferencePripdeevech, Chumpolsri, et al., 2010Radulovic, Blagojevic, et al., 2010Safaei-Ghomi and Batooli, 2010Scandinaro, Tranchida, et al., 2010Scandinaro, Tranchida, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1-MSCP Sil 5 CBDB-1DB-5HP-5MS
Column length (m) 60.25.30.30.30.
Carrier gas Helium HeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.150.250.250.25
Tstart (C) 30.50.50.40.50.
Tend (C) 200.230.220.250.250.
Heat rate (K/min) 2.3.4.10.7.
Initial hold (min) 4. 2.1.1.
Final hold (min) 35. 2.3.5.
I 1112.1140.1114.1146.1152.
ReferenceTakeoka, Hobbs, et al., 2010Usman, Zubair, et al., 2010Xu, Tang, et al., 2010Yang, Zhang, et al., 2010Zouari, Zouari, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-5HP-5 MSDB-5DB-5
Column length (m) 30.30.30.30.50.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.20
Phase thickness (μm) 0.250.250.250.250.32
Tstart (C) 60.35.60.50.60.
Tend (C) 260.220.250.250.220.
Heat rate (K/min) 2.3.2.5.5.
Initial hold (min) 5. 8.2.3.
Final hold (min) 999.40.15.  
I 1139.1143.1160.1146.1143.
ReferenceDayisoylu and Alma, 2009El-Massry, El-Ghorab, et al., 2009Farhat, Ginies, et al., 2009Ho, Wang, et al., 2009Kazemi and Akhavani, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase VF-5HP-5RTX-1RTX-1OV-1
Column length (m) 30.25.60.60.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.200.220.220.25
Phase thickness (μm) 0.250.330.250.250.25
Tstart (C) 60.60.60.60.40.
Tend (C) 300.240.230.230.300.
Heat rate (K/min) 10.3.2.2.4.
Initial hold (min) 2.   2.
Final hold (min) 10.7.30.30.10.
I 1161.1150.1123.1123.1115.
ReferenceLi and Zhao, 2009Maridass, 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009Nibret and Wink, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-55 % Phenyl methyl siloxaneDB-5DB-5HP-5 MS
Column length (m) 30.60.30.50.30.
Carrier gas HeliumHeliumNitrogenNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (μm) 0.250.250.250.320.25
Tstart (C) 45.90.40.60.50.
Tend (C) 250.225.230.220.280.
Heat rate (K/min) 3.3.2.5.4.
Initial hold (min) 3.  3. 
Final hold (min) 5.3. 5. 
I 1145.1147.1147.1143.1144.
ReferencePorto, Decorti, et al., 2009Retta, Gattuso, et al., 2009Scrivanti, Anton, et al., 2009Shafaghat and Sadeghi, 2009Zhao, Zeng, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra 2ZB-1DB-5Elite-1HP-5 MS
Column length (m) 50.30.60.30.30.
Carrier gas HeliumNitrogenNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.200.250.250.320.25
Phase thickness (μm) 0.110.250.250.250.25
Tstart (C) 60.45.60.60.60.
Tend (C) 230.230.250.246.250.
Heat rate (K/min) 2.3.5.3.2.
Initial hold (min) 5.   8.
Final hold (min) 30. 10. 15.
I 1140.1111.1153.1150.1151.
ReferenceByun and Shin, 2008Mierendorff, Stahl-Biskup, et al., 2008Mosayebi, Amin, et al., 2008Raj, Baby, et al., 2008Sahraoui, Vian, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1HP-5HP-5 MSDB-5CP Sil 5 CB
Column length (m) 30.30.30.50.30.
Carrier gas HeliumHeliumHeliumNitrogenN2
Substrate      
Column diameter (mm) 0.250.250.250.200.32
Phase thickness (μm) 0.250.320.250.320.25
Tstart (C) 65.60.50.60.60.
Tend (C) 260.250.230.220.300.
Heat rate (K/min) 6.5.3.5.4.
Initial hold (min)  30.10.3. 
Final hold (min)   10.5. 
I 1149.1145.1143.1143.1122.
ReferenceWang, Yi, et al., 2008Yassa and Akhani, 2008Adams, Beauchamp, et al., 2007Amiri, 2007Baran, von Reuss, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSSE-52DB-5HP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas He HeHeN2
Substrate      
Column diameter (mm) 0.250.250.260.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.50.
Tend (C) 280.220.240.280.240.
Heat rate (K/min) 3.3.3.3.5.
Initial hold (min)  1.  1.
Final hold (min)  5.  4.
I 1138.1117.1138.1146.1143.
ReferenceBasta, Pavlovic, et al., 2007Bicchi, Cordero, et al., 2007Bos, Woerdenbag, et al., 2007Bozin B., Mlmica-Dukic N., et al., 2007Cheraif, Ben Jannet, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5ZP-5DB-5Col-Elite 5MS
Column length (m) 30.30.60.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.260.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.35.40.60.30.
Tend (C) 290.220.260.210.246.
Heat rate (K/min) 3.3.6.30.3.
Initial hold (min)   7.3. 
Final hold (min)  40.1.  
I 1138.1145.1153.1139.1148.
ReferenceElfami, Bos, et al., 2007El-Ghorab A., El-Massry K.F., et al., 2007Füssel, Dötterl, et al., 2007Ghasemi, Yamini, et al., 2007Gudaityte and Venskutonis R.P., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DBP-5RTX-5 MSHP-101RTX-5Sil MSSPB-1
Column length (m) 25.30.25.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.2
Phase thickness (μm) 0.220.250.20.250.2
Tstart (C) 40.45.70.50.70.
Tend (C) 250.210.200.260.220.
Heat rate (K/min) 3.3.3.5.3.
Initial hold (min) 1. 2.2. 
Final hold (min) 10.  10.15.
I 1126.1146.1104.1143.1118.
ReferenceHeravi and Sereshti, 2007Hudaib and Aburjai, 2007Jerkovic, Mastelic, et al., 2007Matasyoh, Matasyoh, et al., 2007Pinto, Salgueiro, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-1DB-1DB-5DBP-5
Column length (m) 30.60.60.30.25.
Carrier gas He HeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.22
Tstart (C) 50.60.60.50.40.
Tend (C) 250.250.250.240.250.
Heat rate (K/min) 2.5.5.4.3.
Initial hold (min)     1.
Final hold (min)     10.
I 1140.1124.1128.1142.1126.
ReferenceRaal, Orav, et al., 2007Salehi, Asghari, et al., 2007Salehi, Fakhari, et al., 2007Sefidkon, Abbasi, et al., 2007Sereshti and Samadi, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5MSHP-5 MSHP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeliumHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.50.
Tend (C) 280.280.280.250.280.
Heat rate (K/min) 3.3.3.3.9.
Initial hold (min)    5.3.
Final hold (min)    10.3.
I 1145.1110.1146.1137.1140.
ReferenceTsokou, Georgopoulos, et al., 2007Tzakou, Bazos, et al., 2007Vagionas, Graikou, et al., 2007Vichi, Riu-Aumatell, et al., 2007Abdelwahed, Hayder, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5ZB-5HP-5MSHP-1SPB-1
Column length (m) 30.30.30.50.30.
Carrier gas N2 HeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.20.20
Phase thickness (μm) 0.250.250.250.50.20
Tstart (C) 50.40.60.60.70.
Tend (C) 280.300.280.250.220.
Heat rate (K/min) 9.2.3.2.3.
Initial hold (min) 3.    
Final hold (min) 3.  120.15.
I 1143.1143.1144.1120.1118.
ReferenceAbdelwahed, Hayder, et al., 2006Biondi, Sari, et al., 2006Bozin, Mimicá-Dukic, et al., 2006Castel, Fernandez, et al., 2006Cavaleiro, Pinto, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSDB-5HP-5HP-1
Column length (m) 30.30.30.30.50.
Carrier gas He HeliumHeHe
Substrate      
Column diameter (mm) 0.320.250.260.250.2
Phase thickness (μm) 0.250.250.250.250.33
Tstart (C) 60.60.60.50.60.
Tend (C) 246.280.290.300.250.
Heat rate (K/min) 3.4.3.5.2.
Initial hold (min)    5. 
Final hold (min)    5.40.
I 1145.1146.1138.1148.1123.
ReferenceCoronel, Cerda-Garcia-Rojas, et al., 2006Ebrahim Sajjadi and Mehregan, 2006Elfami, Komar, et al., 2006Figuérédo, Cabassu, et al., 2006Filippi, Lanfranchi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DB-1DB-5Methyl Silicone
Column length (m) 60.30.60.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.90.
Tend (C) 240.240.240.240.220.
Heat rate (K/min) 5.5.5.5.7.
Initial hold (min) 2.2.2.2.2.
Final hold (min)      
I 1158.1143.1158.1143.1133.
ReferenceGohari, Hadjiakhoondi, et al., 2006Gohari, Hadjiakhoondi, et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Kitchlu, Bakshi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas NitrogenN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.520.250.250.25
Tstart (C) 50.50.60.60.60.
Tend (C) 280.280.220.260.220.
Heat rate (K/min) 5.5.4.4.4.
Initial hold (min)    4.5.
Final hold (min) 5.5.   
I 1145.1145.1147.1149.1148.
ReferenceMarzouk, Mansour, et al., 2006Marzouk, Neffati, et al., 2006Morteza-Semnani, Akbarzadeh, et al., 2006Morteza-Semnani, Saeedi, et al., 2006Morteza-Semnani K., Saeedi M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP-Sil 5 CBDB-5SE-52HP-5MS
Column length (m) 30.25.25.50.30.
Carrier gas  HydrogenN2HeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.150.15 0.25
Tstart (C) 50.50.50.50.40.
Tend (C) 265.230.200.240.260.
Heat rate (K/min) 2.53.4.3.4.
Initial hold (min) 0.5 3.  
Final hold (min)      
I 1142.1136.1147.1145.1151.
ReferenceNickavar B., Kamalinejad M., et al., 2006Olawore, Usman, et al., 2006Ouamba, Ouabonzi, et al., 2006Ozcan, Chalchat, et al., 2006Petrovic, Ristic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSDB-5DB-5
Column length (m) 30.30.30.15.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.40.
Tend (C) 280.260.280.305.240.
Heat rate (K/min) 3.5.4.15.4.
Initial hold (min)    2. 
Final hold (min)      
I 1110.1151.1146.1145.1143.
ReferencePitarokili, Tzakou, et al., 2006Sabulal, Dan, et al., 2006Sajjadi, 2006Sebastián, Urzúa, et al., 2006Sefidkon and Jamzad, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-5DB-1Methyl SiliconeDB-1
Column length (m) 60. 30.25.50.
Carrier gas HeHe N2N2
Substrate      
Column diameter (mm) 0.25 0.320.30.25
Phase thickness (μm)   0.250.150.25
Tstart (C) 40.50.60.50.90.
Tend (C) 250.250.230.210.240.
Heat rate (K/min) 4.5.3.2.4.
Initial hold (min)  3.3.5. 
Final hold (min)  15.10.  
I 1116.1143.1127.1158.1128.
ReferenceSefidkon, Jamzad, et al., 2006Stojanovic, Palic, et al., 2006Tohar, Mohd, et al., 2006Tonzibo, Coffy, et al., 2006Velasco-Negueruela, Pérez-Alonso, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-1HP-1DB-5DB-5MS
Column length (m) 25.30.50.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.20.2490.25
Phase thickness (μm) 0.520.250.50.250.25
Tstart (C) 50.50.60.60.60.
Tend (C) 280.250.250.290.240.
Heat rate (K/min) 2.54.2.3.3.
Initial hold (min) 5.1.   
Final hold (min)  10.60.  
I 1143.1099.1130.1138.1144.
ReferenceWang, Kong, et al., 2006Wong, Sivasothy, et al., 2006Bendimerad and Bendiab, 2005Bos, Stojanova, et al., 2005Busman, Zoghbi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1HP-5HP-5
Column length (m) 50.25.60.30.25.
Carrier gas   HeHeH2
Substrate      
Column diameter (mm) 0.30.250.250.250.32
Phase thickness (μm) 0.250.150.250.250.52
Tstart (C) 60.40.60.50.40.
Tend (C) 240.220.250.300.240.
Heat rate (K/min) 2.3.5.5.4.
Initial hold (min)  5. 5. 
Final hold (min)    5. 
I 1145.1156.1131.1148.1141.
ReferenceChagonda and Chalchat, 2005Chagonda and Chalchat, 2005, 2Fakhari, Salehi, et al., 2005Figuérédo, Cabassu, et al., 2005Jovanovic, Kitic, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm)   0.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.240.280.220.220.
Heat rate (K/min) 3.3.3.4.4.
Initial hold (min)   30.5.5.
Final hold (min)      
I 1145.1144.1112.1146.1146.
ReferenceKhayyat and Karimi, 2005Khayyat and Karimi, 2005Marongiu, Piras, et al., 2005Morteza-Semnani, Akbarzadeh, et al., 2005Morteza-Semnani, Akbarzadeh, et al., 2005, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.25 0.25 
Tstart (C) 60.40.60.60.40.
Tend (C) 220.250.240.220.240.
Heat rate (K/min) 4.5.5.3.4.
Initial hold (min) 4.0.5 4. 
Final hold (min)  2.   
I 1147.1139.1143.1142.1143.
ReferenceMorteza-Semnani and Saeedi, 2005Özel, Gögüs, et al., 2005Saeidnia, Gohari, et al., 2005Salehi, Sefidkon, et al., 2005Sefidkon and Jamzad, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSRTX-1HP-5MSDB-5
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 230.280.250.240.280.
Heat rate (K/min) 3.3.5.3.3.
Initial hold (min)    3. 
Final hold (min) 20. 10.  
I 1146.1145.1131.1163.1118.
ReferenceSkoula and Grayer, 2005Slavkovska, Couladis, et al., 2005Sonboli A., Fakhari A.R., et al., 2005Tepe B., Sokmen M., et al., 2005Tzakou and Constantinidis, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSSPB-1DB-5BP-1
Column length (m) 50.30.50.30.50.
Carrier gas   HeHe 
Substrate      
Column diameter (mm) 0.250.250.20.250.22
Phase thickness (μm) 0.250.250.330.250.25
Tstart (C) 60.40.50.90.60.
Tend (C) 240.220.220.220.220.
Heat rate (K/min) 3.3.4.7.2.
Initial hold (min)  5.3.2. 
Final hold (min)  10.30.5.20.
I 1126.1137.1121.1130.1120.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2005Vichi, Riu-Aumatell, et al., 2005Wong, Lee, et al., 2005Agnihotri, Thappa, et al., 2004Blanc, Muselli, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-1ZB-5DB-5
Column length (m) 30.30.25.60.60.
Carrier gas N2He HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.60.40.40.
Tend (C) 230.275.180.260.280.
Heat rate (K/min) 2.4.3.6.4.
Initial hold (min)   10.4.64.
Final hold (min)   10.1. 
I 1143.1138.1144.1167.1142.
ReferenceGonzález, Guerra, et al., 2004Hajhashemi V., Ghannadi A., et al., 2004bin Jantan, Ayop, et al., 2004Jürgens and Dötterl, 2004Kalvandi, Sefidkon, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-1NB-30
Column length (m) 60.60.60.60.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.320.2
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.35.35.35.50.
Tend (C) 230.230.230.230.250.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min) 4.4.4.4. 
Final hold (min) 25.25.25.25. 
I 1118.1121.1122.1123.1123.
ReferencePark, Lee, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004Raal, Arak, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30DB-5DB-1DB-1DB-5
Column length (m) 50.30.30.60.30.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.200.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.35.50.70.50.
Tend (C) 250.220.265.230.250.
Heat rate (K/min) 2.2.52.52.3.
Initial hold (min)   1.2.5.
Final hold (min)  6.20.20. 
I 1123.1146.1108.1135.1143.
ReferenceRaal, Paaver, et al., 2004Rohloff, Mordal, et al., 2004Sarkhail, Amin, et al., 2004Sawamura, Son, et al., 2004Sefidkon, Jamzad, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5HP-5DB-5
Column length (m) 60.30.25.25.30.
Carrier gas HeHeN2H2He
Substrate      
Column diameter (mm) 0.250.250.20.320.249
Phase thickness (μm) 0.250.250.50.520.25
Tstart (C) 40.40.30.40.60.
Tend (C) 280.250.280.240.300.
Heat rate (K/min) 4.2.3.4.3.
Initial hold (min) 5.5.   
Final hold (min)  20.   
I 1119.1143.1155.1143.1137.
ReferenceSefidkon and Shaabani, 2004Senatore, Rigano, et al., 2004Shafi, Nambiar, et al., 2004Simic, Sokovic, et al., 2004Woerdenbag, Windono, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HTHP-5MSDB-5HP-5MSMethyl Silicone
Column length (m) 27.30.30.30.12.5
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)  0.250.250.25 
Tstart (C) 50.60.60.60.50.
Tend (C) 250.275.240.280.270.
Heat rate (K/min) 2.4.4.3.4.
Initial hold (min) 2.    
Final hold (min) 20.    
I 1141.1143.1146.1148.1126.
ReferenceYusufoglu, Celik, et al., 2004Afsharypuor and Jahromy, 2003Cabanillas, Lopez, et al., 2003Couladis, Özcan, et al., 2003Curini, Bianchi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5MSRSL-200RSL-200
Column length (m) 60.30.30.30.30.
Carrier gas HeN2HeH2H2
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.50.60.40.40.
Tend (C) 250.200.275.280.280.
Heat rate (K/min) 4.5.4.6.6.
Initial hold (min)    5.5.
Final hold (min)    5.5.
I 1116.1117.1143.1131.1125.
ReferenceDabiri and Sefidkon, 2003Fekam Boyom, Ngouana, et al., 2003Hajhashemi, Ghannadi, et al., 2003Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-5DB-5MSDB-5ZB-1
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.390.250.250.250.25
Tstart (C) 60.60.60.60.45.
Tend (C) 220.240.240.280.230.
Heat rate (K/min) 5.3.3.3.3.
Initial hold (min)      
Final hold (min)    30. 
I 1126.1144.1145.1130.1111.
ReferenceKhanavi, Hadjiakhoondi, et al., 2003Machado, Zoghbi, et al., 2003Maia, Taveira, et al., 2003Marongiu, Porcedda, et al., 2003Mierendorff, Stahl-Biskup, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1HP-5DB-1NB-30
Column length (m) 25.50.30.60.50.
Carrier gas H2N2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.150.250.250.250.5
Tstart (C) 50.95.60.50.50.
Tend (C) 230.240.280.250.250.
Heat rate (K/min) 3.4.3.4.2.
Initial hold (min)      
Final hold (min)      
I 1113.1140.1136.1117.1125.
ReferenceOyedeji, Ekundayo, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003Pitarokili, Tzakou, et al., 2003Pourmortazavi, Sefidkon, et al., 2003Raal, Arak, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1Methyl SiliconeHP-1HP-5
Column length (m) 60.60. 50.25.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.25 0.20.32
Phase thickness (μm) 0.250.25 0.50.53
Tstart (C) 40.40.35.60.40.
Tend (C) 220.220.180.220.280.
Heat rate (K/min) 4.4.4.2.4.
Initial hold (min)      
Final hold (min)    40. 
I 1121.1123.1099.1120.1141.
ReferenceRasooli and Mirmostafa, 2003Rasooli and Mirmostafa, 2003Santos and Cordeiro, 2003Valette, Fernandez, et al., 2003Velickovic, Randjelovic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5DB-5
Column length (m) 25.25.25.25.25.
Carrier gas H2HeliumHeliumHeliumN2
Substrate      
Column diameter (mm) 0.320.320.320.320.25
Phase thickness (μm) 0.530.530.530.530.25
Tstart (C) 40.40.40.40.50.
Tend (C) 280.280.280.280.250.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min)      
Final hold (min)     10.
I 1146.1140.1141.1146.1144.
ReferenceVelickovic, Randjelovic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Zrira, Elamrani, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101BP-1HP-5RSL-200DB-5
Column length (m) 25.25.30.30.30.
Carrier gas  N2HeH2 
Substrate      
Column diameter (mm) 0.320.500.250.320.25
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.60.60.40.40.
Tend (C) 200.220.275.280.210.
Heat rate (K/min) 5.5.4.6.2.
Initial hold (min)    5.2.
Final hold (min)  10. 5.33.
I 1128.1123.1141.1139.1149.
ReferenceBoyom, Keumedjio, et al., 2002Das, Ram, et al., 2002Ghannadi, Sajjadi, et al., 2002Jirovetz, Buchbauer, et al., 2002Kabouss, Charrouf, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5DB-5MSCP Sil 5 CBZEBRON-5
Column length (m) 60.30.30.25.6.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 50.35.60.60.40.
Tend (C) 240.280.240.220.200.
Heat rate (K/min) 5.3.3.5.3.
Initial hold (min) 3.2.  5.
Final hold (min) 10.15.  15.
I 1159.1149.1142.1126.1108.
ReferenceKim and Lee, 2002Krauze-Baranowska, Mardarowicz, et al., 2002Maia, Zoghbi, et al., 2002Monfared, Davarani, et al., 2002Öztürk, Akay, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1HP-5DB-1
Column length (m) 60.60.50.30.60.
Carrier gas HeHeN2H2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.40.60.40.50.
Tend (C) 280.280.240.280.250.
Heat rate (K/min) 4.4.3.4.4.
Initial hold (min) 5.5.  5.
Final hold (min)      
I 1120.1118.1126.1143.1117.
ReferenceSefidkon, Jalili, et al., 2002Sefidkon, 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002Velickovic, Randjelovic, et al., 2002Yamini, Sefidkon, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5SPB-1SPB-5DB-1
Column length (m) 30.30.30.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.25 0.25
Tstart (C) 60.60.40.40.40.
Tend (C) 270.240.240.220.280.
Heat rate (K/min) 3.3.2.3.4.
Initial hold (min)    5.5.
Final hold (min)    15. 
I 1141.1139.1118.1141.1115.
ReferenceZoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2Chiasson, Bélanger, et al., 2001Cornu, Carnat, et al., 2001Dabiri and Sefidkon, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5SPB-1SPB-5DB-1
Column length (m) 60.30.30.60.60.
Carrier gas HeN2N2HeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.70.50.50.
Tend (C) 280.220.180.240.270.
Heat rate (K/min) 4.5.2.3.4.
Initial hold (min) 5.10.2.3. 
Final hold (min)   1.10. 
I 1120.1145.1126.1160.1116.
ReferenceDabiri and Sefidkon, 2001Flamini, Cioni, et al., 2001Kamath, Asha, et al., 2001Kim and Lee, 2001Mirza, Ahmadi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1DB-5HP-5 MSPTE-5
Column length (m) 50.30.30.30.60.
Carrier gas HeN2H2HeliumH2
Substrate      
Column diameter (mm) 0.20.250.250.250.32
Phase thickness (μm)  0.250.250.250.3
Tstart (C) 50.80.60.50.60.
Tend (C) 250.225.285.250.285.
Heat rate (K/min) 2.4.3.5.4.3
Initial hold (min)    2. 
Final hold (min)    5. 
I 1120.1113.1143.1124.1143.
ReferenceOrav and Kann, 2001Palá-Paúl, Pérez-Alonso, et al., 2001Santos-Gomes and Fernandes-Ferreira, 2001Shang, Hu, et al., 2001Stojanovic, Palic, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RSL-200HP-5HP-1DB-5
Column length (m) 30.60.30.60.60.
Carrier gas HeH2HeHeHydrogen or helium (He2 wrote in original paper)
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.25 0.250.30
Tstart (C) 60.40.80.60.60.
Tend (C) 240.250.200.200.285.
Heat rate (K/min) 3.6.9.4.4.3
Initial hold (min)    5. 
Final hold (min)   10.25. 
I 1145.1132.1137.1129.1143.
ReferenceTellez M., Estell R., et al., 2001Jirovetz, Puschmann, et al., 2000Lis-Balchin and Roth, 2000Meccia, Rojas, et al., 2000Simic, Andjelkovic, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeOV-1SE-30RTX-1DB-5
Column length (m) 60.25.30.30.30.
Carrier gas  HydrogenN2N2 
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (μm) 0.250.300.250.251.
Tstart (C) 40.50.60.60.40.
Tend (C) 220.200.220.300.200.
Heat rate (K/min) 5.3.4.4.3.
Initial hold (min) 10.1.10. 5.
Final hold (min)  10.   
I 1121.301107.1122.1125.1158.
ReferenceBaraldi, Rapparini, et al., 1999Bicchi, Binello, et al., 1999Jassbi, Ahmad, et al., 1999Kalemba, 1999Meynier, Novelli, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1DB-1DB-5SE-30PONA
Column length (m) 25.50.30.30.50.
Carrier gas H2HeHeHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.200.5
Tstart (C) 40.70.40.60.40.
Tend (C) 220.240.250.200.250.
Heat rate (K/min) 3.4.2.3.6.
Initial hold (min) 5. 5.4.5.
Final hold (min) 5. 60.  
I 1111.1113.1125.1126.1139.
ReferenceOberhofer, Nikiforov, et al., 1999Palá-Paúl, Pérez-Alonso, et al., 1999Porta, Porcedda, et al., 1999Prikhod'ko, Klyuev, et al., 1999Ramalho, de Freitas, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1CP Sil 5 CBDB-5MSSE-30
Column length (m) 25.60.25.30.25.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.25 0.250.2
Phase thickness (μm) 0.390.250.390.25 
Tstart (C) 60.40.60.60.60.
Tend (C) 220.280.220.240.180.
Heat rate (K/min) 5.4.5.3.3.
Initial hold (min) 5.5.  10.
Final hold (min) 20.    
I 1124.1123.1129.1144.1128.
ReferenceRustaiyan, Masoudi, et al., 1999Sefidkon, Dabiri, et al., 1999Weyerstahl, Marschall, et al., 1999Zoghbi, Andrade, et al., 1999Jantan, Ahmad, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-1DB-5HP-1HP-1OV-101
Column length (m) 30.30.25.25.25.
Carrier gas HeHe   
Substrate      
Column diameter (mm) 0.250.250.320.20.32
Phase thickness (μm)  0.25   
Tstart (C) 60.60.35.35.50.
Tend (C) 240.240.250.200.200.
Heat rate (K/min) 4.3.4.5.5.
Initial hold (min)    5. 
Final hold (min)      
I 1119.1141.1120.1121.1134.
ReferenceLamarque, Maestri, et al., 1998Maia, Zohhbi, et al., 1998Ong, Acree, et al., 1998Quiroz A. and Niemeyer H.M., 1998Zollo, Biyiti, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBCP Sil 5 CBDB-5OV-101
Column length (m) 25.25.25.30.50.
Carrier gas N2N2HeHeliumHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 50.50.60.60.50.
Tend (C) 290.290.300.240.250.
Heat rate (K/min) 4.4.6.3.2.
Initial hold (min)      
Final hold (min)      
I 1112.1112.1112.1144.1118.
ReferenceBos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997, 2Tellez, Estell, et al., 1997Orav, Kailas, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-1OV-101HP-5HP-5
Column length (m) 25.60.50.  
Carrier gas N2HeHe  
Substrate      
Column diameter (mm) 0.500.320.2  
Phase thickness (μm)  0.500.5  
Tstart (C) 60.50.70.40.40.
Tend (C) 220.250.180.210.210.
Heat rate (K/min) 5.8.1.2.2.
Initial hold (min)  1.   
Final hold (min)  6.   
I 1132.1140.1130.1146.1147.
ReferenceRajeswara, Kaul, et al., 1996Sagrero-Nieves and Bartley, 1996Orav, Kuningas, et al., 1995Collin, Deslauriers, et al., 1993Collin, Deslauriers, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBMethyl SiliconeOV-101OV-101SE-54
Column length (m) 25.25.50.50.30.
Carrier gas     Hydrogen
Substrate      
Column diameter (mm) 0.250.500.250.250.25
Phase thickness (μm)     0.25
Tstart (C) 60.60.80.80.60.
Tend (C) 280.220.200.200.250.
Heat rate (K/min) 5.5.2.2.2.
Initial hold (min)     5.
Final hold (min)     2.
I 1126.1130.1125.1125.1137.
ReferenceKaul, Singh, et al., 1993Mallavarapu, Ramesh, et al., 1993Tamura, Yang, et al., 1993Tamura, Yang, et al., 1993Kollmannsberger, Nitz, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1RSL-150BP-1HP-1HP-1
Column length (m) 30.30.25.12.12.
Carrier gas N2    
Substrate      
Column diameter (mm)  0.320.330.20.2
Phase thickness (μm)  0.20 0.330.33
Tstart (C) 80.30.45.40.40.
Tend (C) 220.200.180.  
Heat rate (K/min) 4.3.3.16.4.
Initial hold (min)   3.0.3950.4
Final hold (min)      
I 1118.1122.1118.1118.01105.8
ReferenceVelasco-Negueruela, Pérez Alonso, et al., 1991Ronse and De Pooter, 1990Wyllie, Brophy, et al., 1990Yin and Sun, 1990Yin and Sun, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-1HP-1OV-101DB-1
Column length (m) 12.25.50.50.10.
Carrier gas    N2H2
Substrate      
Column diameter (mm) 0.20.320.20.250.25
Phase thickness (μm) 0.330.520.11 0.25
Tstart (C) 40.40.40.80.50.
Tend (C)    200.250.
Heat rate (K/min) 8.8.6.2.5.
Initial hold (min) 0.8010.83.194  
Final hold (min)      
I 1118.21117.91121.31128.1117.
ReferenceYin and Sun, 1990Yin and Sun, 1990Yin and Sun, 1990Sugisawa, Yamamoto, et al., 1989Perry, Baxter, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-1SE-30+IgepalSE-30+Igepal
Column length (m) 50.100.100.
Carrier gas    
Substrate    
Column diameter (mm) 0.320.250.25
Phase thickness (μm)    
Tstart (C) 0.70.70.
Tend (C) 250.170.170.
Heat rate (K/min) 3.1.1.
Initial hold (min)    
Final hold (min)    
I 1113.1132.1138.
ReferenceHabu, Flath, et al., 1985Shibamoto and Jennings, 1977Shibamoto and Jennings, 1977
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Safaei-Ghomi and Batooli, 2010
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Scandinaro, Tranchida, et al., 2010
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Takeoka, Hobbs, et al., 2010
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Usman, Zubair, et al., 2010
Usman, L.A.; Zubair, M.F.; Adabayo, S.A.; Oladosu, I.A.; Muhammad, N.O.; Akolade, J.O., Chemical composition of leaf and fruit essential oils of Hoslundia opposita Vahl grown in Nigeria, Americal-Eurasian J. Agric. Environ. Sci., 2010, 8, 1, 40-43. [all data]

Xu, Tang, et al., 2010
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Yang, Zhang, et al., 2010
Yang, X.; Zhang, H.; Zhang, Y.; Zhao, H.; Dong, A.; Xu, L.; Yang, L.; Ma, Y.; Wang, J., Analysis if the essential oils of pine cones of Pinus koraiensis Steb. et Zucc. and P. sylvestris L. from China, J. Essen. Oil Res., 2010, 22, 5, 446-448, https://doi.org/10.1080/10412905.2010.9700368 . [all data]

Zouari, Zouari, et al., 2010
Zouari, S.; Zouari, N.; Fakhfakh, N.; Bougatel, A.; Ayadi, M.A.; Neffati, M., Chemical composition and biological activities of a new essential oil chemotype of Tunisian Artemisia herba alba Asso, J. Medicinal Plants Res., 2010, 4, 10, 871-880. [all data]

Dayisoylu and Alma, 2009
Dayisoylu, K.S.; Alma, M.H., Chemical analysis of essential oils from cone's rosin of Cilician fir (Abies cilicica subsp. cilicica), Afr. J. Biotechnol., 2009, 8, 15, 3502-3505. [all data]

El-Massry, El-Ghorab, et al., 2009
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Farhat, Ginies, et al., 2009
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Ho, Wang, et al., 2009
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Kazemi and Akhavani, 2009
Kazemi, M.; Akhavani, S., Constituents of Artemisia tournefortiana Rchb. essential oil from Iran, J. Appl. Chem. Res., 2009, 3, 10, 1-5. [all data]

Li and Zhao, 2009
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Maridass, 2009
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Museli, Pau, et al., 2009
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Nibret and Wink, 2009
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Porto, Decorti, et al., 2009
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Retta, Gattuso, et al., 2009
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Scrivanti, Anton, et al., 2009
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Shafaghat and Sadeghi, 2009
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Zhao, Zeng, et al., 2009
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Byun and Shin, 2008
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Mierendorff, Stahl-Biskup, et al., 2008
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Mosayebi, Amin, et al., 2008
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Raj, Baby, et al., 2008
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Sahraoui, Vian, et al., 2008
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Wang, Yi, et al., 2008
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Yassa and Akhani, 2008
Yassa, N.; Akhani, H., The essential oils composition in two species of the genus Eriocycla Lindl. (Apiaceae) from Iran, 2008, retrieved from http://biology.ut.ac.ir/members/akhani/PdfReprintNumber/27.pdf. [all data]

Adams, Beauchamp, et al., 2007
Adams, R.P.; Beauchamp, P.S.; Dev, V.; Dutz, S.M., New Natural Products Isolated from One-Seeded Juniperus of the Southwestern United States: Isolation and Occurence of 2-Ethenyl-3-methyl Phanol and Its Derivatives, J. Essent. Oil Res., 2007, 19, 2, 146-152, https://doi.org/10.1080/10412905.2007.9699247 . [all data]

Amiri, 2007
Amiri, H., Quantative and qualative changes of essential oil of Salvia bracteata BAnk et Sol. in different growth stages, DARU, 2007, 15, 2, 79-82. [all data]

Baran, von Reuss, et al., 2007
Baran, S.; von Reuss, S.H.; König, W.A.; Kalemba, D., Composition of the essential oil of Abies koreana Wils., Flavour Fragr. J., 2007, 22, 1, 78-83, https://doi.org/10.1002/ffj.1762 . [all data]

Basta, Pavlovic, et al., 2007
Basta, A.; Pavlovic, M.; Couladis, M.; Tzakou, O., Essential oil composition of the flowerheads of Chrysanthemum coronarium L. from Greece, Flavour Fragr. J., 2007, 22, 3, 197-200, https://doi.org/10.1002/ffj.1781 . [all data]

Bicchi, Cordero, et al., 2007
Bicchi, C.; Cordero, C.; Liberto, E.; Rubiolo, P.; Sgorbini, B.; Sandra, P., Sorptive tape extraction in the analysis of the volatile fraction emitted from biological solid matrices, J. Chromatogr. A, 2007, 1148, 2, 137-144, https://doi.org/10.1016/j.chroma.2007.03.007 . [all data]

Bos, Woerdenbag, et al., 2007
Bos, R.; Woerdenbag, H.J.; Kayser, O.; Quax, W.J.; Ruslan, K.; Elfami, Essential oil constituents of Piper cubeba L. fils. from Indonesia, J. Essent. Oil Res., 2007, 19, 1, 14-17, https://doi.org/10.1080/10412905.2007.9699217 . [all data]

Bozin B., Mlmica-Dukic N., et al., 2007
Bozin B.; Mlmica-Dukic N.; Samojlik I.; Jovin E., Antimicrobial and antioxidant properties of rosemary and sage (Rosmarinus officinalis L. and Salvia officinalis L., lamiaceae) essential oils, J. Agric. Food Chem., 2007, 55, 19, 7879-7885, https://doi.org/10.1021/jf0715323 . [all data]

Cheraif, Ben Jannet, et al., 2007
Cheraif, I.; Ben Jannet, H.; Hammami, M.; Khouja, M.L.; Mighri, Z., Chemical composition and antimicrobial activity of essential oils of Cupressus arizonica Greene, Biochem. Syst. Ecol., 2007, 35, 12, 813-820, https://doi.org/10.1016/j.bse.2007.05.009 . [all data]

Elfami, Bos, et al., 2007
Elfami; Bos, R.; Ruslan, K.; Woerdenbag, H.J.; Kayser, P.; Quax, W.J., Essential Oil Constituents of Piper cubeba from Indonesia, 2007, 53-60. [all data]

El-Ghorab A., El-Massry K.F., et al., 2007
El-Ghorab A.; El-Massry K.F.; Shibamoto T., Chemical composition of the volatile extract and antioxidant activities of the volatile and nonvolatile extracts of Egyptian corn silk (Zea mays L.), J. Agric. Food Chem., 2007, 55, 22, 9124-9127, https://doi.org/10.1021/jf071646e . [all data]

Füssel, Dötterl, et al., 2007
Füssel, U.; Dötterl, S.; Jürgens, A.; Aas, G., Inter- and intraspecific variation in floral scent in the genus Salix and its implication for pollination, J. Chem. Ecol., 2007, 33, 4, 749-765, https://doi.org/10.1007/s10886-007-9257-6 . [all data]

Ghasemi, Yamini, et al., 2007
Ghasemi, E.; Yamini, Y.; Bahramifar, N.; Sefidkon, F., Comparative analysis of the oil and supercritical CO2 extract of Artemisia sieberi, J. Food Eng., 2007, 79, 1, 306-311, https://doi.org/10.1016/j.jfoodeng.2006.01.059 . [all data]

Gudaityte and Venskutonis R.P., 2007
Gudaityte, O.; Venskutonis R.P., Chemotypes of Achillea millefolium transferred from 14 different locations in Lithuania to the controlled environment, Biochem. Syst. Ecol., 2007, 35, 9, 582-592, https://doi.org/10.1016/j.bse.2007.03.016 . [all data]

Heravi and Sereshti, 2007
Heravi, M.J.; Sereshti, H., Determination of Essential Oil Components of Artemisia haussknechtii Boiss. using Simultaneous Hydrodistillation-Static Headspace Liquid Phase Microextraction - Gas Chromatography Mass Spectrometry, J. Chromatogr. A, 2007, 1160, 1-2, 81-89, https://doi.org/10.1016/j.chroma.2007.05.096 . [all data]

Hudaib and Aburjai, 2007
Hudaib, M.; Aburjai, T., Volatile components of Thymus vulgaris L. from wild-growing and cultivated plants in Jordan, Flavour Fragr. J., 2007, 22, 4, 322-327, https://doi.org/10.1002/ffj.1800 . [all data]

Jerkovic, Mastelic, et al., 2007
Jerkovic, I.; Mastelic, J.; Marijanovic, Z., Bound volatile compounds and essential oil from the fruit of Maclura pomifera (Raf.) Schneid. (osage orange), Flavour Fragr. J., 2007, 22, 1, 84-88, https://doi.org/10.1002/ffj.1763 . [all data]

Matasyoh, Matasyoh, et al., 2007
Matasyoh, L.G.; Matasyoh, J.C.; Wachira, F.N.; Kinyua, M.G.; Muigai, A.W.T.; Mukiama, T.K., Chemical composition and antimicrobial activity of the essential oil of Ocimum gratissimum L. growing in Eastern Kenya, Afr. J. Biotechnol., 2007, 6, 760-765. [all data]

Pinto, Salgueiro, et al., 2007
Pinto, E.; Salgueiro, L.R.; Cavaleiro, C.; Palmeira, A.; Goncalves, M.J., In vitro susceptibility of some species of yeasts and filamentous fungi to essential oils of Salvia of?cinalis, Ind. Crops Prod., 2007, 26, 2, 135-141, https://doi.org/10.1016/j.indcrop.2007.02.004 . [all data]

Raal, Orav, et al., 2007
Raal, A.; Orav, A.; Arak, E.; Kailas, T.; Müürisepp, M., Variation in the composition of the essential oil of Valeriana officinalis L. roots from Estonia, Proc. Est. Acad. Sci. Chem., 2007, 56, 2, 67-74. [all data]

Salehi, Asghari, et al., 2007
Salehi, P.; Asghari, B.; Mohammadi, F., Hydrodistillation-Headspace Solvent Microextraction: An Efficient Method for Analysis of the Essential Oil from the Seeds of Foeniculum vulgare Mill., Chromatographia, 2007, 65, 1-2, 119-122, https://doi.org/10.1365/s10337-006-0102-9 . [all data]

Salehi, Fakhari, et al., 2007
Salehi, P.; Fakhari, A.R.; Ebrahimi, S.N.; Heydari, R., Rapid essential oil screening of Rosmarinus officinalis L. by hydrodistillation-headspace solvent microextraction, Flavour Fragr. J., 2007, 22, 4, 280-285, https://doi.org/10.1002/ffj.1793 . [all data]

Sefidkon, Abbasi, et al., 2007
Sefidkon, F.; Abbasi, K.; Jamzad, Z.; Ahmadi, S., The effect of distillation methods and stage of plant growth on the essential oil content and composition of Satureja rechingeri Jamzad, Food Chem., 2007, 100, 3, 1054-1058, https://doi.org/10.1016/j.foodchem.2005.11.016 . [all data]

Sereshti and Samadi, 2007
Sereshti, H.; Samadi, S., Comparison of hydrodistillation-headspace liquid phase microextraction techniques with hydrodistillation in determination of essential oils in Artemisia Haussknechtii Boiss, JSUT, 2007, 33, 2, 7-17. [all data]

Tsokou, Georgopoulos, et al., 2007
Tsokou, A.; Georgopoulos, K.; Melliou, E.; Magiatis, P.; Tsitsa, E., Composition and enantiomeric analusis of the essential oil of the fruits and the leaves of Pistacia vera from Greece, Molecules, 2007, 12, 6, 1233-1239, https://doi.org/10.3390/12061233 . [all data]

Tzakou, Bazos, et al., 2007
Tzakou, O.; Bazos, I.; Yannitsaros, A., Volatile metabolites of Pistacia atlantica Desf. from Greece, Flavour Fragr. J., 2007, 22, 5, 358-362, https://doi.org/10.1002/ffj.1805 . [all data]

Vagionas, Graikou, et al., 2007
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Notes

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