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Dibenzothiophene, 4-methyl-


Lee's RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-5DB-5HP-5
Column length (m) 30.60.30.30.50.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.5
Program not specified60C (1 min) => 45 C/min => 150C (2 min) => 2 C/min => 300 C (25 min)110C(1min) => 40C/min => 160C => 10C/min => 300C925min)35C(2min) => 25C/min => 160C => 3C/min => 300C(25min)35C => 25C/min => 160C => 3C/min => 300C(50min)
I 311.80310.76310.9310.3311.8
ReferenceZhou, Wang, et al., 2004Mössner, de Alda, et al., 1999Becker and Colmsjö, 1998Becker and Colmsjö, 1998Becker, Nilsson, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-30DB-5CP Sil 8 CBCP Sil 8 CB
Column length (m) 30.25.30.50.50.
Carrier gas HeNitrogenHeHeHe
Substrate      
Column diameter (mm) 0.250.200.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Program 90C (1min) => 10C/min => 120C => 4C/min => 310C (20min)not specified60 0C (3 min) 10 0C/min -> 100 0C (3 min) 5 0C/min -> 300 0Cnot specifiednot specified
I 311.34312.72313.7312.5312.6
ReferenceZamperlini, Silva, et al., 1997Wang, Xue, et al., 1994Paschke, Herbel, et al., 1992Bundt, Herbel, et al., 1991Bundt, Herbel, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Lee's RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zhou, Wang, et al., 2004
Zhou, J.; Wang, T.; Shi, Q.; Huang, Y.; Mao, T.; Zhong, N.; Zhang, Y.; Zhang, X., Determination of sulfur and oxygen containing polycyclic aromatic hydrocarbons in inhalable particulate by gas chromatography - mass spectrometry, J. Chin. Mass Spectrom. Soc., 2004, 25, 3, 134-140. [all data]

Mössner, de Alda, et al., 1999
Mössner, S.G.; de Alda, M.J.L.; Sander, L.C.; Lee, M.L.; Wise, S.A., Gas chromatographic retention behavior of polycyclic aromatic sulfur heterocyclic compounds, (dibenzothiophene, naphtho[b]thiophenes, benzo[b]naphthothiophenes and alkyl-substituted derivatives) on stationary phases of different selectivity, J. Chromatogr. A, 1999, 841, 2, 207-228, https://doi.org/10.1016/S0021-9673(99)00363-5 . [all data]

Becker and Colmsjö, 1998
Becker, G.; Colmsjö, A., Gas chromatography-atomic emission detection for quantification of polycyclic aromatic sulfur heterocycles, Anal. Chim. Acta., 1998, 376, 3, 265-272, https://doi.org/10.1016/S0003-2670(98)00546-7 . [all data]

Becker, Nilsson, et al., 1998
Becker, G.; Nilsson, U.; Colmsjö, A.; Östman, C., Determination of polycyclic aromatic sulfur heterocyclic compounds in airborne particulate by gas chromatography with atomic emission and mass spectrometric detection, J. Chromatogr. A, 1998, 826, 1, 57-66, https://doi.org/10.1016/S0021-9673(98)00729-8 . [all data]

Zamperlini, Silva, et al., 1997
Zamperlini, G.C.M.; Silva, M.R.S.; Vilegas, W., Identification of polycyclic aromatic hydrocarbons in sugar cane soot by gas chromatography-mass spectrometry, Chromatographia, 1997, 46, 11/12, 655-663, https://doi.org/10.1007/BF02490527 . [all data]

Wang, Xue, et al., 1994
Wang, X.; Xue, W.; Zhu, J.; Gu, Y.; Sheng, G.; Fu, J., Characterization of polynuclear aromatic sulfur heterocycles in a coal, J. Fuel Chemistry and Technology, 1994, 22, 2, 196-202. [all data]

Paschke, Herbel, et al., 1992
Paschke, A.; Herbel, W.; Steinhart, H.; Franke, S.; Francke, W., Determination of mono- to tetracyclic aromatic hydrocarbons in lubricating oil, J. Hi. Res. Chromatogr., 1992, 15, 12, 827-833, https://doi.org/10.1002/jhrc.1240151211 . [all data]

Bundt, Herbel, et al., 1991
Bundt, J.; Herbel, W.; Steinhart, H.; Franke, S.; Francke, W., Structure-type separation of diesel fuels by solid phase extraction and identification of the two- and three-ring aromatics by capillary GC-mass spectrometry, J. Hi. Res. Chromatogr., 1991, 14, 2, 91-98, https://doi.org/10.1002/jhrc.1240140205 . [all data]


Notes

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