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Dibenzothiophene, 4-methyl-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-Petro1932.Lu, Wu, et al., 200450. m/0.20 mm/0.50 «mu»m, He, 35. C @ 5. min, 2. K/min, 300. C @ 5. min
CapillaryPONA1927.Yang, Wang, et al., 200250. m/0.20 mm/0.50 «mu»m, 1.5 K/min, 270. C @ 10. min; Tstart: 120. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-Petro1927.Lu, Wu, et al., 200450. m/0.20 mm/0.50 «mu»m, He; Program: not specified

Lee's RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryRxi-5 MS312.22Zeigler, Schantz, et al., 201230. m/0.25 mm/0.25 «mu»m, Helium, 60. C @ 1. min, 5. K/min, 340. C @ 0. min
CapillaryDB-5MS311.95Sun, Zhou, et al., 200830. m/0.25 mm/0.25 «mu»m, 50. C @ 2. min, 6. K/min, 300. C @ 16. min
CapillaryDB-5MS311.92Schade and Andersson, 200630. m/0.25 mm/0.25 «mu»m, He, 60. C @ 1. min, 10. K/min; Tend: 300. C
CapillaryHP-5317.78Marynowski, Pieta, et al., 200460. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 35. C; Tend: 300. C
CapillaryHP-5MS312.00Zhou, Wang, et al., 200430. m/0.25 mm/0.25 «mu»m, 65. C @ 5. min, 3. K/min, 290. C @ 20. min
CapillaryDB-5311.9Becker and Colmsjö, 199830. m/0.25 mm/0.25 «mu»m, He, 110. C @ 1. min, 10. K/min, 325. C @ 5. min
CapillaryDB-5312.73Williams and Bottrill, 1995He, 60. C @ 2. min, 5. K/min; Column length: 25. m; Column diameter: 0.3 mm; Tend: 270. C
CapillaryDB-5312.22Wang, Fingas, et al., 199430. m/0.32 mm/0.25 «mu»m, He, 50. C @ 2. min, 6. K/min; Tend: 300. C
CapillarySE-30313.17Wang, Xue, et al., 1994Nitrogen, 4. K/min; Column length: 25. m; Column diameter: 0.20 mm; Tstart: 80. C; Tend: 290. C
CapillaryCP Sil 8 CB312.4Bundt, Herbel, et al., 199150. m/0.25 mm/0.25 «mu»m, He, 4. K/min; Tstart: 80. C; Tend: 300. C
CapillaryDB-5312.6Palmentier, Britten, et al., 198980. C @ 1. min, 3.5 K/min, 300. C @ 10. min; Column length: 30. m; Column diameter: 0.32 mm
CapillaryDB-5312.7Palmentier, Britten, et al., 198980. C @ 1. min, 3.5 K/min, 300. C @ 10. min; Column length: 30. m; Column diameter: 0.32 mm
CapillaryOV-73312.5Arpino, Ignatiadis, et al., 198768. m/0.28 mm/0.15 «mu»m, 1.5 K/min
CapillaryDB-5315.2Viau, Studak, et al., 1984Helium, 4. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 90. C; Tend: 250. C
CapillarySE-52312.72Vassilaros, Kong, et al., 198220. m/0.30 mm/0.25 «mu»m, H2, 40. C @ 2. min, 4. K/min; Tend: 265. C

Lee's RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS311.80Zhou, Wang, et al., 200430. m/0.25 mm/0.25 «mu»m; Program: not specified
CapillaryDB-5310.76Mössner, de Alda, et al., 199960. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 45 C/min => 150C (2 min) => 2 C/min => 300 C (25 min)
CapillaryDB-5310.9Becker and Colmsjö, 199830. m/0.25 mm/0.25 «mu»m, He; Program: 110C(1min) => 40C/min => 160C => 10C/min => 300C925min)
CapillaryDB-5310.3Becker and Colmsjö, 199830. m/0.25 mm/0.25 «mu»m, He; Program: 35C(2min) => 25C/min => 160C => 3C/min => 300C(25min)
CapillaryHP-5311.8Becker, Nilsson, et al., 199850. m/0.32 mm/0.5 «mu»m, He; Program: 35C => 25C/min => 160C => 3C/min => 300C(50min)
CapillaryDB-5311.34Zamperlini, Silva, et al., 199730. m/0.25 mm/0.25 «mu»m, He; Program: 90C (1min) => 10C/min => 120C => 4C/min => 310C (20min)
CapillarySE-30312.72Wang, Xue, et al., 1994Nitrogen; Column length: 25. m; Column diameter: 0.20 mm; Program: not specified
CapillaryDB-5313.7Paschke, Herbel, et al., 199230. m/0.25 mm/0.25 «mu»m, He; Program: 60 0C (3 min) 10 0C/min -> 100 0C (3 min) 5 0C/min -> 300 0C
CapillaryCP Sil 8 CB312.5Bundt, Herbel, et al., 199150. m/0.25 mm/0.25 «mu»m, He; Program: not specified
CapillaryCP Sil 8 CB312.6Bundt, Herbel, et al., 199150. m/0.25 mm/0.25 «mu»m, He; Program: not specified

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Lu, Wu, et al., 2004
Lu, X.; Wu, J.; Wu, J.; Kong, H.; Hua, R.; Tao, W.; Gu, J.; Xu, G., Characterization and quantitative determination of diesel fractions by comprehensive two-dimensional gas chromatography/time of flight mass spectrometry, Chin. J. Chromatogr., 2004, 22, 1, 5-11. [all data]

Yang, Wang, et al., 2002
Yang, Y.-T.; Wang, H.-Y.; Lu, W.-Z., Determination od sulfur compounds in catalytic diesel oil by gas chromatography with atomic emission detector and its application, Chin. J. Chromatogr., 2002, 20, 6, 493-497. [all data]

Zeigler, Schantz, et al., 2012
Zeigler, C.; Schantz, M.; Wise, S.; Robbat, A., Mass spectra and retention indices for polycyclic aromatic sulfur heterocycles and some alkylated analogs, Polycyclic Aromatic Compounds, 2012, 32, 2, 154-176, https://doi.org/10.1080/10406638.2011.651679 . [all data]

Sun, Zhou, et al., 2008
Sun, P.; Zhou, Q.; Li, G.; Wang, X.; Zhao, Y.; Cao, L., fingerprint analysis of polycyclic aromatic hydrocarbons in crude oil by internal standard method, J. Instrumental Anal., 2008, 27, 4, 344-348. [all data]

Schade and Andersson, 2006
Schade, T.; Andersson, J.T., Speciation of alkylated dibenzothiophenes through correlation of structure and gas chromatographic retention indexes, J. Chromatogr. A, 2006, 1117, 2, 206-213, https://doi.org/10.1016/j.chroma.2006.03.079 . [all data]

Marynowski, Pieta, et al., 2004
Marynowski, L.; Pieta, M.; Janeczek, J., Composition and source of polycyclic aromatic compounds in deposited dust from selected sites around the Upper Silesia, Poland, Geol. Q., 2004, 48, 2, 169-180. [all data]

Zhou, Wang, et al., 2004
Zhou, J.; Wang, T.; Shi, Q.; Huang, Y.; Mao, T.; Zhong, N.; Zhang, Y.; Zhang, X., Determination of sulfur and oxygen containing polycyclic aromatic hydrocarbons in inhalable particulate by gas chromatography - mass spectrometry, J. Chin. Mass Spectrom. Soc., 2004, 25, 3, 134-140. [all data]

Becker and Colmsjö, 1998
Becker, G.; Colmsjö, A., Gas chromatography-atomic emission detection for quantification of polycyclic aromatic sulfur heterocycles, Anal. Chim. Acta., 1998, 376, 3, 265-272, https://doi.org/10.1016/S0003-2670(98)00546-7 . [all data]

Williams and Bottrill, 1995
Williams, P.T.; Bottrill, R.P., Sulfur-polycyclic aromatic hydrocarbons in tyre pyrolysis oil, Fuel, 1995, 74, 5, 736-742, https://doi.org/10.1016/0016-2361(94)00005-C . [all data]

Wang, Fingas, et al., 1994
Wang, Z.; Fingas, M.; Li, K., Fractionation of a light crude oil and identification and quantitation of aliphatic, aromatic, and biomarker comopunds by GC-FID and GC-MS, Part II, J. Chromatogr. Sci., 1994, 32, 9, 367-382, https://doi.org/10.1093/chromsci/32.9.367 . [all data]

Wang, Xue, et al., 1994
Wang, X.; Xue, W.; Zhu, J.; Gu, Y.; Sheng, G.; Fu, J., Characterization of polynuclear aromatic sulfur heterocycles in a coal, J. Fuel Chemistry and Technology, 1994, 22, 2, 196-202. [all data]

Bundt, Herbel, et al., 1991
Bundt, J.; Herbel, W.; Steinhart, H.; Franke, S.; Francke, W., Structure-type separation of diesel fuels by solid phase extraction and identification of the two- and three-ring aromatics by capillary GC-mass spectrometry, J. Hi. Res. Chromatogr., 1991, 14, 2, 91-98, https://doi.org/10.1002/jhrc.1240140205 . [all data]

Palmentier, Britten, et al., 1989
Palmentier, J.-P.F.; Britten, A.J.; Charbonneau, G.M.; Karasek, F.W., Determination of polycyclic aromatic hydrocarbons in lubricating oil base stocks using high-performance liquid chromatography and gas chromatography-mass spectrometry, J. Chromatogr., 1989, 469, 241-251, https://doi.org/10.1016/S0021-9673(01)96459-3 . [all data]

Arpino, Ignatiadis, et al., 1987
Arpino, P.J.; Ignatiadis, I.; de Rycke, G., Sulphur-containing polynuclear aromatic hydrocarbons from petroleum. Examination of their possible statistical formation in sediments, J. Chromatogr., 1987, 390, 2, 329-348, https://doi.org/10.1016/S0021-9673(01)94385-7 . [all data]

Viau, Studak, et al., 1984
Viau, A.C.; Studak, S.M.; Karasek, F.W., Comparative analysis of hazardous compounds on flu-ash from municipal waste incineration by gas chromatography / mass spectrometry, Can. J. Chem., 1984, 62, 11, 2140-2145, https://doi.org/10.1139/v84-366 . [all data]

Vassilaros, Kong, et al., 1982
Vassilaros, D.L.; Kong, R.C.; Later, D.W.; Lee, M.L., Linear retention index system for polycyclic aromatic compounds. Critical evaluation and additional indices, J. Chromatogr., 1982, 252, 1-20, https://doi.org/10.1016/S0021-9673(01)88394-1 . [all data]

Mössner, de Alda, et al., 1999
Mössner, S.G.; de Alda, M.J.L.; Sander, L.C.; Lee, M.L.; Wise, S.A., Gas chromatographic retention behavior of polycyclic aromatic sulfur heterocyclic compounds, (dibenzothiophene, naphtho[b]thiophenes, benzo[b]naphthothiophenes and alkyl-substituted derivatives) on stationary phases of different selectivity, J. Chromatogr. A, 1999, 841, 2, 207-228, https://doi.org/10.1016/S0021-9673(99)00363-5 . [all data]

Becker, Nilsson, et al., 1998
Becker, G.; Nilsson, U.; Colmsjö, A.; Östman, C., Determination of polycyclic aromatic sulfur heterocyclic compounds in airborne particulate by gas chromatography with atomic emission and mass spectrometric detection, J. Chromatogr. A, 1998, 826, 1, 57-66, https://doi.org/10.1016/S0021-9673(98)00729-8 . [all data]

Zamperlini, Silva, et al., 1997
Zamperlini, G.C.M.; Silva, M.R.S.; Vilegas, W., Identification of polycyclic aromatic hydrocarbons in sugar cane soot by gas chromatography-mass spectrometry, Chromatographia, 1997, 46, 11/12, 655-663, https://doi.org/10.1007/BF02490527 . [all data]

Paschke, Herbel, et al., 1992
Paschke, A.; Herbel, W.; Steinhart, H.; Franke, S.; Francke, W., Determination of mono- to tetracyclic aromatic hydrocarbons in lubricating oil, J. Hi. Res. Chromatogr., 1992, 15, 12, 827-833, https://doi.org/10.1002/jhrc.1240151211 . [all data]


Notes

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