Methaqualone


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-1BP-1BP-1BP-1BP-1
Column length (m)  12.12.12.12.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm)  0.220.220.220.22
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 200.120.120.120.120.
Tend (C) 280.270.270.270.270.
Heat rate (K/min) 16.12.15.25.6.
Initial hold (min)      
Final hold (min)      
I 2125.2132.2139.2153.2109.
ReferenceSchutz and Wollrab A., 1988Stowell and Wilson, 1985Stowell and Wilson, 1985Stowell and Wilson, 1985Stowell and Wilson, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryPacked
Active phase BP-1BP-1BP-1BP-1OV-1
Column length (m) 12.12.12.12.2.
Carrier gas HeHeHeHe 
Substrate     Gas Chrom P
Column diameter (mm) 0.220.220.220.22 
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 120.100.120.50.120.
Tend (C) 270.295.280.300.200.
Heat rate (K/min) 8.5.8.20.2.5
Initial hold (min)      
Final hold (min)      
I 2119.2096.2115.2117.2105.
ReferenceStowell and Wilson, 1985Stowell and Wilson, 1985Stowell and Wilson, 1985Stowell and Wilson, 1985Marozzi, Gambaro, et al., 1982
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPacked
Active phase SE-30SE-30SE-30
Column length (m) 2.2.2.
Carrier gas  NitrogenN2
Substrate Gas Chrom PChromosorb W AW DMS (80-100 mesh)Chromosorb W AW DMS
Column diameter (mm)    
Phase thickness (μm)    
Tstart (C) 120.130.130.
Tend (C) 200.290.290.
Heat rate (K/min) 2.58.8.
Initial hold (min)  2.2.
Final hold (min)  8.8.
I 2165.2123.2123.
ReferenceMarozzi, Gambaro, et al., 1982Peel and Perrigo, 1976Peel and Perrigo, 1975
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Schutz and Wollrab A., 1988
Schutz, H.; Wollrab A., The significance of the retention index in toxicologic analysis II, Pharmazie in unzerer Zeit, 1988, 17, 4, 97-101. [all data]

Stowell and Wilson, 1985
Stowell, A.; Wilson, L., Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]

Marozzi, Gambaro, et al., 1982
Marozzi, E.; Gambaro, V.; Saligari, E.; Mariani, R.; Lodi, F., Use of the retention index in gas chromatographic studies of drugs, J. Anal. Toxicol., 1982, 6, 4, 185-192, https://doi.org/10.1093/jat/6.4.185 . [all data]

Peel and Perrigo, 1976
Peel, H.W.; Perrigo, B., A practical gas chromatographic screening procedure for toxicological analysis, Can. Soc. Forens. Sci. J., 1976, 9, 2, 69-74, https://doi.org/10.1080/00085030.1976.10757247 . [all data]

Peel and Perrigo, 1975
Peel, H.W.; Perrigo, B., A practical gas chromatographic screening procedure for toxicological analysis, Can.Soc.Forens.Sci.J., 1975, 9, 2, 69-74, https://doi.org/10.1080/00085030.1976.10757247 . [all data]


Notes

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