Methaqualone


Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryPackedPacked
Active phase BP-1DB-1BP-1SE-30SE-30
Column length (m) 25.30.25.2. 
Carrier gas N2N2N2N2N2
Substrate    1% se-30 on Anachrom ABS(80-100mesh)AW-DMCS
Column diameter (mm) 0.220.530.53 0.53
Phase thickness (μm) 0.251.51.  
Temperature (C) 200.200.200.220.210.
I 2125.2125.2129.2130.2144.
ReferenceJapp, Gill, et al., 1987Japp, Gill, et al., 1987Japp, Gill, et al., 1987Musumarra, Scarlata, et al., 1987Oyama, Sano, et al., 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPackedPackedPackedPacked
Active phase OV-1OV-101OV-101OV-101OV-101
Column length (m)  2.2.2.2.
Carrier gas  N2N2N2N2
Substrate  Chromosorb G AW DMCS (80-100 mesh)Chromosorb G AW DMCS (80-100 mesh)Chromosorb G AW DMCS (80-100 mesh)Chromosorb G AW DMCS (80-100 mesh)
Column diameter (mm)      
Phase thickness (μm)      
Temperature (C) 200.200.200.200.200.
I 2130.2130.2130.2130.2135.
ReferenceBerninger and Möller, 1977Möller, 1976Möller, 1976Möller, 1976Möller, 1976
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type PackedPacked
Active phase OV-101OV-101
Column length (m) 2.2.
Carrier gas N2N2
Substrate Chromosorb WChromosorb W
Column diameter (mm)   
Phase thickness (μm)   
Temperature (C) 190.230.
I 2127.2162.
ReferenceMöller, 1976Möller, 1976
Comment MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Japp, Gill, et al., 1987
Japp, M.; Gill, R.; Osselton, M.D., Comparison of drug retention indices determined on packed, wide bore capillary and narrow bore capillary columns, J. Forensic Sci., 1987, 32, 6, 1574-1586. [all data]

Musumarra, Scarlata, et al., 1987
Musumarra, G.; Scarlata, G.; Romano, G.; Cappello, G.; Clementi, S.; Giulietti, G., Qualitative organic analysis. Part 2. Identification of drugs by principal components analysis of standardized TLC data in four eluent systems and of retention indices on SE 30, J. Anal. Toxicol., 1987, 11, 4, 154-163, https://doi.org/10.1093/jat/11.4.154 . [all data]

Oyama, Sano, et al., 1987
Oyama, N.; Sano, T.; Syoyama, M.; Maeda, K., Studies on systematic analysis of poisonous compounds in forensic chemistry. II. Application of capillary column gas chromatography to substance identification by means of retention indices, Eisei Kagaku, 1987, 33, 5, 342-348, https://doi.org/10.1248/jhs1956.33.342 . [all data]

Berninger and Möller, 1977
Berninger, H.; Möller, M.R., Retentionsindices zur gaschromatographischen Identifizierung von Arzneimitteln, Arch. Toxicol., 1977, 37, 4, 295-305, https://doi.org/10.1007/BF00330821 . [all data]

Möller, 1976
Möller, M.R., Comparability of retention indices of polar substances at elevated temperatures, Chromatographia, 1976, 9, 7, 311-314, https://doi.org/10.1007/BF02268832 . [all data]


Notes

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