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3-Dodecene, (E)-


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillarySqualane100.1185.Heinzen, Soares, et al., 1999 
CapillarySE-30120.1193.Gusev, Sokolov, et al., 1989H2; Column length: 40. m; Column diameter: 0.30 mm
CapillarySE-30120.1193.Gusev, Sokolov, et al., 1989H2; Column length: 40. m; Column diameter: 0.30 mm
CapillaryOV-101110.1193.Rang, Kuningas, et al., 1987He; Column length: 50. m; Column diameter: 0.25 mm
CapillarySqualane100.1185.Sojak, Hrivnak, et al., 1973 
CapillarySqualane115.1185.Sojak, Hrivnak, et al., 1973 
CapillarySqualane130.1185.Sojak, Hrivnak, et al., 1973 
CapillarySqualane86.1185.Sojak, Hrivnak, et al., 1973 
CapillarySqualane100.1185.1Soják and Hrivnák, 1972H2; Column length: 200. m; Column diameter: 0.2 mm
CapillarySqualane115.1185.2Soják and Hrivnák, 1972H2; Column length: 200. m; Column diameter: 0.2 mm
CapillarySqualane130.1185.3Soják and Hrivnák, 1972H2; Column length: 200. m; Column diameter: 0.2 mm
CapillarySqualane86.1185.0Soják and Hrivnák, 1972H2; Column length: 200. m; Column diameter: 0.2 mm

Kovats' RI, polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
CapillaryPEG 4000100.1246.Rang, Orav, et al., 1988 
CapillaryPEG 4000110.1246.Rang, Orav, et al., 1988 
CapillaryPEG 4000120.1246.Rang, Orav, et al., 1988 
CapillaryPEG 4000140.1246.Rang, Orav, et al., 1988 
CapillaryPEG 4000160.1246.Rang, Orav, et al., 1988 
CapillaryPEG-20M100.1241.Rang, Orav, et al., 1988 
CapillaryPEG-20M110.1241.Rang, Orav, et al., 1988 
CapillaryPEG-20M120.1241.Rang, Orav, et al., 1988 
CapillaryPEG-20M130.1241.Rang, Orav, et al., 1988 
CapillaryPEG-20M140.1241.Rang, Orav, et al., 1988 
CapillaryPEG-20M90.1240.Rang, Orav, et al., 1988 
CapillaryPEG 4000100.1246.Rang, Kuningas, et al., 1977Column diameter: 0.25 mm
CapillaryPEG 4000120.1246.Rang, Kuningas, et al., 1977Column diameter: 0.25 mm
CapillaryPEG 4000140.1246.Rang, Kuningas, et al., 1977Column diameter: 0.25 mm
CapillaryPEG 4000160.1246.Rang, Kuningas, et al., 1977Column diameter: 0.25 mm

Kovats' RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-Wax1237.Umano and Shibamoto, 1987He, 40. C @ 10. min, 2. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 200. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryPolydimethyl siloxane1185.Junkes, Castanho, et al., 2003Program: not specified

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Heinzen, Soares, et al., 1999
Heinzen, V.E.F.; Soares, M.F.; Yunes, R.A., Semi-empirical topological method for the prediction of the chromatographic retention of cis- and trans-alkene isomers and alkanes, J. Chromatogr. A, 1999, 849, 2, 495-506, https://doi.org/10.1016/S0021-9673(99)00530-0 . [all data]

Gusev, Sokolov, et al., 1989
Gusev, G.M.; Sokolov, V.P.; Yurov, V.V.; Kuznetsov, A.V.; Potatuev, A.A., Identification of olefins during hydrocarboxylation, Zh. Anal. Khim., 1989, 44, 551-555. [all data]

Rang, Kuningas, et al., 1987
Rang, S.; Kuningas, K.; Strenze, T.; Orav, A.; Eisen, O., Retention and Thermodynamics of Solution of n-Alkenes in OV-101, J. Chromatogr., 1987, 406, 75-80, https://doi.org/10.1016/S0021-9673(00)94018-4 . [all data]

Sojak, Hrivnak, et al., 1973
Sojak, L.; Hrivnak, J.; Majer, P.; Janak, J., Capillary Gas Chromatography of Linear Alkenes on Squalane, Anal. Chem., 1973, 45, 2, 293-302, https://doi.org/10.1021/ac60324a039 . [all data]

Soják and Hrivnák, 1972
Soják, L.; Hrivnák, J., Open tubular column gas chromatography of the catalytic dehydrogenation products of n-dodecane, J. Chromatogr. Sci., 1972, 10, 11, 701-704, https://doi.org/10.1093/chromsci/10.11.701 . [all data]

Rang, Orav, et al., 1988
Rang, S.A.; Orav, A.E.; Kuningas, K.R.; Meister, A.E.; Strense, T.V.; Eisen, O.G., Gas-Chromatographic Characteristics of unsaturated hydrocarbons, Academy of Sciences of Estonia SSR, Tallinn, Estonia SSR, 1988, 208. [all data]

Rang, Kuningas, et al., 1977
Rang, S.; Kuningas, K.; Orav, A.; Eisen, O., Capillary Gas Chromatography of C6-C14 n-Alkenes on Polyphenyl Ether and Polyethylene Glycol 4000, Chromatographia, 1977, 10, 2, 55-64, https://doi.org/10.1007/BF02274460 . [all data]

Umano and Shibamoto, 1987
Umano, K.; Shibamoto, T., Analysis of headspace volatiles from overheated beef fat, J. Agric. Food Chem., 1987, 35, 1, 14-18, https://doi.org/10.1021/jf00073a004 . [all data]

Junkes, Castanho, et al., 2003
Junkes, B.S.; Castanho, R.D.M.; Amboni, C.; Yunes, R.A.; Heinzen, V.E.F., Semiempirical Topological Index: A Novel Molecular Descriptor for Quantitative Structure-Retention Relationship Studies, Internet Electronic Journal of Molecular Design, 2003, 2, 1, 33-49. [all data]


Notes

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