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Kovats' RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-5BPX-5HP-1Petrocol DH-100
Column length (m)    30.100.
Carrier gas    HeHe
Column diameter (mm)    0.250.2
Phase thickness (μm)    0.25 
Program not specifiednot specifiednot specified35C => 2C/min => 100C => 5C/min => 230C(2min)5C(10min) => 5C/min => 50C(48min) => 1.5C/min => 195C(91min)
I 647.667.664.629.649.7
ReferenceSGE, 2005SGE, 2005SGE, 2005Wongpornchai, Sriseadka, et al., 2003Haagen-Smit Laboratory, 1997
Column type CapillaryPackedCapillaryCapillaryPacked
Active phase DB-1Apiezon MSPB-1SqualaneSE-30
Column length (m)
Carrier gas He N2N2 
Substrate  Chromosorb W  Chromosrb G
Column diameter (mm) 0.32 0.750.25 
Phase thickness (μm) 1.0    
Program -40 C for 12 min; -40 - 125 C at 3 deg.min; 125-185 C at 6 deg/min; 185 - 220 C at 20 deg/min; hold 220 C for 2 minnot specifiednot specifiednot specifiednot specified
I 649.681.3661.6652.650.
ReferenceHoekman, 1993Jalali-Heravi and Garkani-Nejad, 1993Castello, Timossi, et al., 1988Papazova and Pankova, 1975Moffat, Stead, et al., 1974


Go To: Top, Kovats' RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

SGE, 2005
SGE, Guide to GC column selection, 2005, retrieved from [all data]

Wongpornchai, Sriseadka, et al., 2003
Wongpornchai, S.; Sriseadka, T.; Choonvisase, S., Identification and quantitation of the rice aroma compound, 2-acetyl-1-pyrroline, in bread flowers (Vallaris glabra Ktze), J. Agric. Food Chem., 2003, 51, 2, 457-462, . [all data]

Haagen-Smit Laboratory, 1997
Haagen-Smit Laboratory, Procedure for the detailed hydrocarbon analysis of gasolines by single column high efficiency (capillary) column gas chromatography, SOP NO. MLD 118, Revision No. 1.1, California Environmental Protection Agency, Air Resources Board, El Monte, California, 1997, 22. [all data]

Hoekman, 1993
Hoekman, S.K., Improved gas chromatography procedure for speciated hydrocarbon measurements of vehicle emissions, J. Chromatogr., 1993, 639, 2, 239-253, . [all data]

Jalali-Heravi and Garkani-Nejad, 1993
Jalali-Heravi, M.; Garkani-Nejad, Z., Prediction of gas chromatographic retention indices of some benzene derivatives, J. Chromatogr., 1993, 648, 2, 389-393, . [all data]

Castello, Timossi, et al., 1988
Castello, G.; Timossi, A.; Gerbino, T.C., Gas Chromatographic Separation of Halogenated Compounds on Non-Polar and Polar Wide Bore Capillary Columns, J. Chromatogr., 1988, 454, 129-143, . [all data]

Papazova and Pankova, 1975
Papazova, D.I.; Pankova, M.C., Identification of individual aromatic hydrocarbons in kerosene fraction (b.p. 150-250 °), J. Chromatogr., 1975, 105, 2, 411-414, . [all data]

Moffat, Stead, et al., 1974
Moffat, A.C.; Stead, A.H.; Smalldon, K.W., Optimum use of paper, thin-layer and gas-liquid chromatography for the identification of basic drugs. III. Gas-liquid chromatography, J. Chromatogr., 1974, 90, 1, 19-33, . [all data]


Go To: Top, Kovats' RI, non-polar column, custom temperature program, References