1-Pentanol

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Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxAT-WaxFFAPVF-Wax MSCP Wax 52 CB
Column length (m) 60.60.60.60.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.50
Tstart (C) 60.60.45.60.40.
Tend (C) 220.280.220.220.230.
Heat rate (K/min) 3.4.5.3.4.
Initial hold (min) 1. 1.5.2.
Final hold (min) 5. 5.25.15.
I 1260.1206.1233.1244.1254.
ReferenceFeng, Zhuang, et al., 2011Kiss, Csoka, et al., 2011Piyachaiseth, Jirapakkul, et al., 2011Duarte, Dias, et al., 2010Birtic, Ginies, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-WaxDB-WaxHP-InnowaxStabilwaxDB-Wax
Column length (m) 60.30.30.60.30.
Carrier gas HeliumHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.5
Tstart (C) 50.40.50.40.40.
Tend (C) 230.230.250.240.240.
Heat rate (K/min) 6.3.6.53.5.
Initial hold (min) 2.2.1.55. 
Final hold (min) 15.5.10.10. 
I 1255.1255.1237.1238.1259.
ReferenceMo, Fan, et al., 2009Zhao, Xu, et al., 2009Thakeow, Angeli, et al., 2008Cros, Vandanjon, et al., 2007Dury-Brun, Fournier, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBFFAPCP-Wax 52CBCP-Wax 52CBCP-Wax 52CB
Column length (m) 30.30.60.60.60.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 0.250.50.50.50.5
Tstart (C) 40.35.40.40.40.
Tend (C) 220.320.220.220.220.
Heat rate (K/min) 3.4.4.4.4.
Initial hold (min) 1.5.8.8.8.
Final hold (min) 2.45.20.20.20.
I 1260.1272.1256.1257.1259.
ReferenceHymete, Rohloff, et al., 2007Nebesny, Budryn, et al., 2007Povolo, Contarini, et al., 2007Povolo, Contarini, et al., 2007Povolo, Contarini, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20BP-20TR-WAXDB-WaxDB-Wax
Column length (m) 30.30.60.30.30.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.70.40.40.40.
Tend (C) 220.220.200.230.230.
Heat rate (K/min) 4.4.3.4.4.
Initial hold (min) 4.4.10.2.2.
Final hold (min) 5.5.10.5.15.
I 1259.1259.1250.1268.1268.
ReferenceRawat, Gulati, et al., 2007Rawat, Gulati, et al., 2007Tena N., Lazzez A., et al., 2007Xu, Fan, et al., 2007Fan and Qian, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxTR-WAXZB-WaxInnowaxStabilwax DA
Column length (m) 30.60.60.60.60.
Carrier gas N2HeHeHe 
Substrate      
Column diameter (mm) 0.320.250.320.250.25
Phase thickness (μm) 0.250.250.50.250.5
Tstart (C) 40.40.40.60.40.
Tend (C) 230.200.250.240.180.
Heat rate (K/min) 6.3.3.5.5.
Initial hold (min) 2.10.2. 5.
Final hold (min) 15. 10.30. 
I 1264.1255.1264.1244.1241.
ReferenceFan and Qian, 2006, 2Salas J.J., Garcia-Gonzalez D.L., et al., 2006Wierda R.L., Fletcher G., et al., 2006Joichi, Yomogida, et al., 2005Nogueira, Lubachevsky, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxTR-WAXZB-WaxZB-WaxHP-FFAP
Column length (m) 60.60.30.30.30.
Carrier gas  H2HeliumHeliumHe
Substrate      
Column diameter (mm) 0.530.250.320.320.25
Phase thickness (μm) 1.0.250.250.250.25
Tstart (C) 50.40.40.40.40.
Tend (C) 180.200.250.250.120.
Heat rate (K/min) 3.3.5.5.5.
Initial hold (min) 10.10.2.2.5.
Final hold (min)   5.5.3.
I 1213.1255.1252.1255.1262.
ReferenceRizzolo, Cambiaghi, et al., 2005Salas, Sánchez, et al., 2005N/AN/ALópez, Guzmán, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PEG-20MDB-WaxStabilwaxDB-WaxCarbowax 20M
Column length (m) 50.30.60.60.50.
Carrier gas  H2HeliumH2Helium
Substrate      
Column diameter (mm) 0.200.250.250.320.70
Phase thickness (μm) 0.200.50.250.25 
Tstart (C) 40.50.40.40.50.
Tend (C) 180.200.240.230.280.
Heat rate (K/min) 3.3.3.4.4.
Initial hold (min) 5.10.5.5.2.
Final hold (min) 30.10.10.25. 
I 1248.1272.1238.1253.1275.
ReferenceNarain, Almeida, et al., 2004Alves and Franco, 2003Cros, Vandanjon, et al., 2003Dregus and Engel, 2003Saura, LAencina, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Supelcowax-10RTX-WaxDB-WaxDB-Wax
Column length (m) 30.30.60.60.60.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.50.25 
Tstart (C) 40.40.40.40.60.
Tend (C) 200.200.180.220.180.
Heat rate (K/min) 3.3.5.3.3.
Initial hold (min) 10.10.5.10.4.
Final hold (min)   20.10. 
I 1250.1248.1258.1253.1251.
ReferenceVichi, Castellote, et al., 2003Vichi, Pizzale, et al., 2003Galindo-Cuspinera, Lubran, et al., 2002Hayata, Sakamoto, et al., 2002Ito, Sugimoto, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxSupelcowax-10DB-Wax
Column length (m) 60.60.30.60.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.50.50.35.50.
Tend (C) 200.210.220.200.180.
Heat rate (K/min) 2.1.54.4.3.
Initial hold (min) 2.5.3.10. 
Final hold (min)  10.  40.
I 1244.1259.1233.1285.1217.
ReferenceUmano, Hagi, et al., 2002Chyau and Mau, 2001Weckerle, Bastl-Borrmann, et al., 2001Girard and Durance, 2000Lee and Shibamoto, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxCarbowax 20MDB-WaxCarbowax
Column length (m) 60.60.25.60.50.
Carrier gas NitrogenHeHe N2
Substrate      
Column diameter (mm) 0.250.250.30.320.2
Phase thickness (μm)  0.25   
Tstart (C) 40.40.60.30.80.
Tend (C) 200.200.190.170.200.
Heat rate (K/min) 2.2.5.2.1.
Initial hold (min) 10.2.2.4. 
Final hold (min)   20.60.20.
I 1276.1250.1235.1246.1210.
ReferenceTamura, Boonbumrung, et al., 2000Umano, Hagi, et al., 2000Xue, Ye, et al., 2000Buttery, Orts, et al., 1999Menon, Chacko, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxSupelcowax-10PEG-20MDB-Wax
Column length (m) 60.60.60.25.30.
Carrier gas He H2 He
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm) 0.25 0.5 0.25
Tstart (C) 40.30.35.50.50.
Tend (C) 200.170.250.230.240.
Heat rate (K/min) 2.2.5.2.4.
Initial hold (min) 2.4.5. 3.
Final hold (min)  30.20. 10.
I 1250.1246.1259.1228.1246.
ReferenceUmano, Nakahara, et al., 1999Buttery and Ling, 1998Campeanu, Burcea, et al., 1998Ding, Deng, et al., 1998Parada and Duque, 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxInnowaxDB-WaxDB-WaxDB-Wax
Column length (m) 30.30.60.60.60.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.25  
Tstart (C) 50.40.50.60.50.
Tend (C) 240.240.230.180.200.
Heat rate (K/min) 4.6.2.2.3.
Initial hold (min) 3.10.   
Final hold (min) 10.25.  40.
I 1249.1260.1230.1252.1262.
ReferenceParada and Duque, 1998Petersen, Poll, et al., 1998Ravichandran and Parthiban, 1998Sekiwa, Kubota, et al., 1997Wada and Shibamoto, 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TC-WaxSupelcowax-10DB-WaxSupelcowax-10Carbowax 20M
Column length (m) 60.60.30.90.60.
Carrier gas  HeHydrogenHe 
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (μm)  0.250.500.25 
Tstart (C) 80.40.30.35.60.
Tend (C) 240.200.190.220.180.
Heat rate (K/min) 3.3.3.2.2.
Initial hold (min) 5.3.6.20.4.
Final hold (min)  30. 30. 
I 1244.1260.1257.1244.1231.
ReferenceShuichi, Masazumi, et al., 1996Wong and Lai, 1996Young, Gilbert, et al., 1996Girard and Lau, 1995Kawakami, Ganguly, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxPEG-20MPEG-20MDB-Wax
Column length (m) 60.60.50.50.60.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm)   0.150.15 
Tstart (C) 60.60.60.60.60.
Tend (C) 180.180.180.180.220.
Heat rate (K/min) 2.2.2.2.3.
Initial hold (min) 4.4.4.4.4.
Final hold (min)      
I 1242.1243.1229.1231.1249.
ReferenceKobayashi, Tsuda, et al., 1995Kobayashi, Tsuda, et al., 1995Togari, Kobayashi, et al., 1995Togari, Kobayashi, et al., 1995Chung, Eiserich, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MCarbowax 20MPEG-20MCarbowax 20MDB-Wax
Column length (m) 50.50.50.80.60.
Carrier gas HeHeN2  
Substrate      
Column diameter (mm) 0.250.250.250.20.32
Phase thickness (μm)      
Tstart (C) 60.60.60.70.50.
Tend (C) 180.180.180.170.230.
Heat rate (K/min) 2.2.2.2.4.
Initial hold (min) 4.4.   
Final hold (min)     10.
I 1232.1231.1238.1213.1247.
ReferenceKawakami, Kobayashi, et al., 1993Kawakami and Kobayashi, 1991Kubota, Nakamoto, et al., 1991Anker, Jurs, et al., 1990Binder, Benson, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSP-1000DB-WaxCarbowax 20MCarbowax 20M
Column length (m) 60.25.60.50.50.
Carrier gas  N2 N2N2
Substrate      
Column diameter (mm) 0.320.20.320.220.22
Phase thickness (μm)  0.43   
Tstart (C) 50.60.50.80.80.
Tend (C) 230.190.230.200.200.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min)   0.1  
Final hold (min) 10.30.10.  
I 1247.1271.1245.1223.1224.
ReferenceBinder, Turner, et al., 1990De Llano D.G., Ramos M., et al., 1990Binder, Flath, et al., 1989Mihara, Tateba, et al., 1988Mihara, Tateba, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 60.60.50.50.31.
Carrier gas H2H2N2N2Helium
Substrate      
Column diameter (mm) 0.250.250.220.220.50
Phase thickness (μm) 0.250.25   
Tstart (C) 30.30.80.80.40.
Tend (C) 180.180.200.200.200.
Heat rate (K/min) 2.2.3.3.10.
Initial hold (min) 2.2.   
Final hold (min)      
I 1256.1256.1223.1224.1236.
ReferenceTakeoka, Flath, et al., 1988Takeoka, Flath, et al., 1988Mihara, Tateba, et al., 1987Mihara, Tateba, et al., 1987Labropoulos, Palmer, et al., 1982
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase Carbowax 20M
Column length (m) 150.
Carrier gas  
Substrate  
Column diameter (mm) 0.64
Phase thickness (μm)  
Tstart (C) 50.
Tend (C) 170.
Heat rate (K/min) 1.
Initial hold (min) 30.
Final hold (min)  
I 1230.
ReferenceButtery, Parker, et al., 1981
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Feng, Zhuang, et al., 2011
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Duarte, W.F.; Dias, D.R.; Oliveira, J.M.; Teixeira, J.A.; de Almeida e Silva, J.B.; Schwan, R.F., Characterization of different fruit wines made from cacao,cupuassu, gabiroba, jaboticaba and umbu, Food Sci. Technol., 2010, 43, 1564-1572. [all data]

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Cros, Vandanjon, et al., 2007
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Dury-Brun, C.; Fournier, N.; Pernin, K.; Guichard, E.; Voilley, A., A new approach to studying sponge cake aroma after storage in treated paper and plastic packaging by direct gas chromatography?olfactometry (D-GC-O), Flavour Fragr. J., 2007, 22, 4, 255-264, https://doi.org/10.1002/ffj.1788 . [all data]

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Hymete, A.; Rohloff, J.; Iversen, T.-H.; Kjosen, H., Volatile constituents of the roots of Echinops kebericho Mesfin, Flavour Fragr. J., 2007, 22, 1, 35-38, https://doi.org/10.1002/ffj.1746 . [all data]

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Nebesny, E.; Budryn, G.; Kula, J.; Majda, T., The effect of roasting method on headspace composition of robusta coffee bean aroma, Eur. Food Res. Technol., 2007, 225, 1, 9-19, https://doi.org/10.1007/s00217-006-0375-0 . [all data]

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Alves and Franco, 2003
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Cros, Vandanjon, et al., 2003
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Notes

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