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1-Pentanol

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Van Den Dool and Kratz RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxHP-InnowaxDB-WaxDB-WaxHP-Innowax
Column length (m) 30.60.30.30.60.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.50.50.25
Tstart (C) 40.40.40.40.50.
Tend (C) 200.250.250.250.220.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min) 1.2.5.5.4.
Final hold (min) 10.10.15.15.10.
I 1252.1244.1258.1260.1254.
ReferenceCho, Namgung, et al., 2008Hashizume M., Gordon M.H., et al., 2007Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 2007Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 2007Quijano, Linares, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-WaxZB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 30.30.60.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.40.40.50.
Tend (C) 250.250.200.200.230.
Heat rate (K/min) 5.5.4.4.10.
Initial hold (min) 2.2.1.1.5.
Final hold (min) 5.5.10.10.25.
I 1255.1252.1252.1255.1241.
ReferenceWu, Zorn, et al., 2007Wu, Zorn, et al., 2007Cho, Choi, et al., 2006Cho, Choi, et al., 2006Fernandez-Segovia, Escriche, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBOV-351StabilwaxSupelcowax-10DB-Wax
Column length (m) 60.50.60.60.60.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (mum) 0.250.20.250.251.
Tstart (C) 35.60.40.40.45.
Tend (C) 203.220.240.280.250.
Heat rate (K/min) 3.5.3.4.5.
Initial hold (min) 4. 5.2.1.
Final hold (min)   10. 12.
I 1242.1220.1238.1255.1262.
ReferenceAlasalvar, Taylor, et al., 2005Bonvehí, 2005Cros, Lignot, et al., 2005Elmore, Nisyrios, et al., 2005Malliaa, Fernandez-Garcia, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxSupelcowax-10Carbowax 20MZB-WaxDB-Wax
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.150.25
Tstart (C) 40.60.45.35.45.
Tend (C) 200.240.250.220.240.
Heat rate (K/min) 5.3.2.1.86.
Initial hold (min) 5.5.0.1710.10.
Final hold (min) 2.10. 10.30.
I 1232.1261.1239.1249.1274.
ReferencePena, Barciela, et al., 2005Riu-Aumatell, Lopez-Tamames, et al., 2005Verzera, Campisi, et al., 2005Ledauphin, Saint-Clair, et al., 2004Nielsen, Larsen, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxStabilwaxDB-WaxZB-Wax
Column length (m) 30.30.60.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 45.45.40.40.40.
Tend (C) 240.240.240.240.220.
Heat rate (K/min) 6.6.3.6.3.
Initial hold (min) 10.10.5.10. 
Final hold (min) 30.30.10.30. 
I 1274.1274.1238.1274.1233.
ReferenceNielsen, Larsen, et al., 2004, 2Nielsen, Larsen, et al., 2004, 3Cros, Vandanjon, et al., 2003Nielsen, Larsen, et al., 2003Brunton, Cronin, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10AT-WaxSupelcowax-10DB-WaxDB-Wax
Column length (m) 60.60.60.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.65.35.40.40.
Tend (C) 195.250.195.200.200.
Heat rate (K/min) 2.2.2.2.2.
Initial hold (min) 5.10.5.5.5.
Final hold (min) 90.60.90.20.30.
I 1251.1238.1251.1245.1250.
ReferenceChung, Yung, et al., 2002Pino, Marbot, et al., 2002Chung, Yung, et al., 2001Kim, Shin, et al., 2001Kim, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBCP-Wax 52CBDB-WaxDB-WaxDB-Wax
Column length (m) 50.60.30.30.60.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.320.320.32
Phase thickness (mum)  0.250.50.50.5
Tstart (C) 50.45.60.60.30.
Tend (C) 200.250.245.245.160.
Heat rate (K/min) 2.2.3.3.3.
Initial hold (min)  0.173.3. 
Final hold (min)   20.20.5.
I 1256.1239.1250.1249.1258.
ReferenceLiu, Yang, et al., 2001Verzera, Campisi, et al., 2001Wirth, Guo, et al., 2001Wirth, Guo, et al., 2001Beauchene, Grua-Priol, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxCP-Wax 52CBSupelcowax-10CP-Wax 52CB
Column length (m) 30.30.50.60.50.
Carrier gas He  HeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum) 0.50.5 0.250.2
Tstart (C) 60.60.60.35.30.
Tend (C) 245.245.220.195.220.
Heat rate (K/min) 3.3.4.2.2.
Initial hold (min) 3.3.5. 1.3
Final hold (min) 20.20.30.90. 
I 1250.1250.1251.1250.1233.
ReferenceBureau, Baumes, et al., 2000Bureau, Razungles, et al., 2000Chevance, Farmer, et al., 2000Chung, 2000Jensen, Christensen, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxHP-WaxCP-Wax 52CBCP-Wax 52CBSupelcowax-10
Column length (m) 60.15.50.50.60.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.320.530.320.320.25
Phase thickness (mum) 0.51.  0.25
Tstart (C) 40.40.60.60.35.
Tend (C) 250.220.220.220.195.
Heat rate (K/min) 4.5.4.4.2.
Initial hold (min) 2.3.5.5.5.
Final hold (min) 10.30.30.30.90.
I 1264.1294.1245.1241.1250.
ReferenceLe Guen, Prost, et al., 2000Peng, 2000Chevance and Farmer, 1999Chevance and Farmer, 1999, 2Chung, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxFFAPCarbowax 20MDB-WaxDB-Wax
Column length (m) 60.30.60.60.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.4250.25 
Tstart (C) 40.20.45.50.40.
Tend (C) 200.200.300.230.200.
Heat rate (K/min) 3.4.3.2.2.
Initial hold (min) 5.1.3. 5.
Final hold (min) 60.1.20.  
I 1248.1292.1235.1249.1256.
ReferenceCha, Kim, et al., 1998Ott, Fay, et al., 1997Mondello, Dugo, et al., 1995Shimoda, Shigematsu, et al., 1995Iwaoka, Hagi, et al., 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxSupelcowax-10Carbowax 20M
Column length (m) 60.60.60.60.3.05
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.25 
Phase thickness (mum) 0.250.25 0.25 
Tstart (C) 50.50.40.40.40.
Tend (C) 230.230.200.195.200.
Heat rate (K/min) 2.2.3.2.8.
Initial hold (min)   5.5. 
Final hold (min) 60.60. 40.60.
I 1252.1252.1256.1246.1236.
ReferenceShiratsuchi, Shimoda, et al., 1994Shiratsuchi, Shimoda, et al., 1994, 2Sumitani, Suekane, et al., 1994Chung and Cadwallader, 1993Peng, 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPackedCapillary
Active phase DB-WaxDB-WaxDB-WaxCarbowax 20MCarbowax 20M
Column length (m) 60.30.30.3.0530.
Carrier gas HeHeHe He
Substrate    Supelcoport 
Column diameter (mm) 0.250.250.25 0.25
Phase thickness (mum)   0.25 0.25
Tstart (C) 35.40.50.40.40.
Tend (C) 180.200.220.200.240.
Heat rate (K/min) 3.2.4.8.4.
Initial hold (min) 5.10.3.4.3.
Final hold (min)   20.  
I 1206.1249.1241.1236.1250.
ReferenceStashenko, Macku, et al., 1992Umano, Hagi, et al., 1992Humpf and Schreier, 1991Peng, Yang, et al., 1991Schwab, Mahr, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Supelcowax-10CP-WAX 57CBSupelcowax-10Supelcowax-10
Column length (m) 60.60.50.60.60.
Carrier gas      
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 40.40.60.40.40.
Tend (C) 175.175.200.175.175.
Heat rate (K/min) 2.2.4.2.2.
Initial hold (min) 5.5.5.5.5.
Final hold (min) 20.20. 20.20.
I 1258.1260.1251.1255.1258.
ReferenceTanchotikul and Hsieh, 1989Tanchotikul and Hsieh, 1989Salter L.J., Mottram D.S., et al., 1988Vejaphan, Hsieh, et al., 1988Vejaphan, Hsieh, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryPacked
Active phase Carbowax 20MOV-351Carbowax 20M
Column length (m) 50.25. 
Carrier gas HeN2 
Substrate   Celite 545
Column diameter (mm) 0.320.32 
Phase thickness (mum)    
Tstart (C) 50.50.75.
Tend (C) 200. 228.
Heat rate (K/min) 2.6.4.6
Initial hold (min) 5.  
Final hold (min) 40.  
I 1236.1216.1228.
ReferenceChen, Kuo, et al., 1986Korhonen, 1984van den Dool and Kratz, 1963
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Cho, Namgung, et al., 2008
Cho, I.H.; Namgung, H.-J.; Choi, H.-K.; Kim, Y.-S., Volatiles and key odorants in the pileus and stipe of pine-mushroom (Tricholoma matsutake Sing.), Food Chem., 2008, 106, 1, 71-76, https://doi.org/10.1016/j.foodchem.2007.05.047 . [all data]

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Quijano, Linares, et al., 2007
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Bonvehí, 2005
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Verzera, Campisi, et al., 2005
Verzera, A.; Campisi, S.; Zappalá, M., SUPELCO. Using SPME-GC-MS to characterize volatile components of honey as indicators of botanical origin, 2005, retrieved from http://www.sigmaaldrich.com/Brands/SupelcoHome/TheReporter.html. [all data]

Ledauphin, Saint-Clair, et al., 2004
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Nielsen, Larsen, et al., 2004
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Nielsen, Larsen, et al., 2004, 2
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Nielsen, Larsen, et al., 2004, 3
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Nielsen, Larsen, et al., 2003
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Pino, Marbot, et al., 2002
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Chung, Yung, et al., 2001
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Liu, Yang, et al., 2001
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Verzera, Campisi, et al., 2001
Verzera, A.; Campisi, S.; Zappalá, M.; Bonaccorsi, I., SPME-GC-MS analysis of honey volatile components for the characterization of different floral origin, Am. Lab. Fairfield Conn., 2001, 33, 15, 18-21. [all data]

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Beauchene, Grua-Priol, et al., 2000
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Bureau, Baumes, et al., 2000
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Bureau, Razungles, et al., 2000
Bureau, S.M.; Razungles, A.R.; Baumes, R.L., The aroma of Muscat of Frontignan grapes: effect of the light environment of vine or bunch on volatiles and glycoconjugates, J. Sci. Food Agric., 2000, 80, 14, 2012-2020, https://doi.org/10.1002/1097-0010(200011)80:14<2012::AID-JSFA738>3.0.CO;2-X . [all data]

Chevance, Farmer, et al., 2000
Chevance, F.F.V.; Farmer, L.J.; Desmond, E.M.; Novelli, E.; Troy, D.J.; Chizzolini, R., Effect of some fat replacers on the release of volatile aroma compounds from low-fat meat products, J. Agric. Food Chem., 2000, 48, 8, 3476-3484, https://doi.org/10.1021/jf991211u . [all data]

Chung, 2000
Chung, H.Y., Volatile flavor components in red fermented soybean (Glycine max) curds, J. Agric. Food Chem., 2000, 48, 5, 1803-1809, https://doi.org/10.1021/jf991272s . [all data]

Jensen, Christensen, et al., 2000
Jensen, K.; Christensen, L.P.; Hansen, M.; Jørgensen, U.; Kaack, K., Olfactory and quantitative analysis of volatiles in elderberry (Sambucus nigra L) juice processed from seven cultivars, J. Sci. Food Agric., 2000, 81, 2, 237-244, https://doi.org/10.1002/1097-0010(20010115)81:2<237::AID-JSFA809>3.0.CO;2-H . [all data]

Le Guen, Prost, et al., 2000
Le Guen, S.; Prost, C.; Demaimay, M., Characterization of odorant compounds of mussels (Mytilus edulis) according to their origin using gas chromatography-olfactometry and gas chromatography-mass spectrometry, J. Chromatogr. A, 2000, 896, 1-2, 361-371, https://doi.org/10.1016/S0021-9673(00)00729-9 . [all data]

Peng, 2000
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Notes

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, References