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1-Pentanol

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Normal alkane RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Polydimethyl siloxane: CP-Sil 5 CBVF-5 MSVF-5 MSVF-5 MSHP-5 MS
Column length (m) 60.60.60.60.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (mum) 1.00.250.250.250.25
Tstart (C) 45.40.30.30.70.
Tend (C) 210.250.260.260.290.
Heat rate (K/min) 3.64.2.2.5.
Initial hold (min) 1.452.   
Final hold (min) 2.72 28.28. 
I 754.765.768.773.762.
ReferenceBramston-Cook, 2013Srisajjalerwaja, Apichartsrangkoon, et al., 2012Leffingwell and Alford, 2011Leffingwell and Alford, 2011Lazarevic, Radulovic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5HP-5 MSMega 5 MSHP-5 MS
Column length (m) 30.30.30.60.30.
Carrier gas HeliumHydrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.70.35.40.50.
Tend (C) 290.290.195.240.230.
Heat rate (K/min) 5.5.2.3.4.
Initial hold (min)   5.2.4.
Final hold (min) 10. 30. 10.
I 762.762.763.762.771.
ReferenceRadulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Kim and Chung, 2009Romeo, Verzera, et al., 2009Forero, Quijano, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1HP-5HP-5 MS5 % Phenyl methyl siloxaneRTX-5
Column length (m) 30.10.30.30.10.
Carrier gas HeliumHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.250.100.250.250.18
Phase thickness (mum) 1.00.400.251.0.2
Tstart (C) 60.40.50.40.40.
Tend (C) 250.280.250.250.275.
Heat rate (K/min) 5.20.6.57.50.
Initial hold (min) 5.1.1.510.0.5
Final hold (min)  1.10.5.0.5
I 749.776.779.772.749.
ReferenceFrerot, Velluz, et al., 2008Mildner-Szkudlarz and Jelen, 2008Thakeow, Angeli, et al., 2008Ramirez R. and Cava R., 2007Setkova, Risticevic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Elite-5MSSPB-5SPB-5DB-5SPB-5
Column length (m) 30.60.60.30.30.
Carrier gas He  N2He
Substrate      
Column diameter (mm) 0.320.320.320.320.53
Phase thickness (mum) 0.51.1.1. 
Tstart (C) 40.40.40.40.100.
Tend (C) 280.230.230.230.250.
Heat rate (K/min) 4.3.3.6.5.
Initial hold (min) 5.5.5.2. 
Final hold (min) 10.5.5.15. 
I 765.768.768.759.764.
ReferenceTava, Pecetti, et al., 2007Vasta, Ratel, et al., 2007Vasta, Ratel, et al., 2007Fan and Qian, 2006Kilic, Kollmannsberger, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MDN-5HP-5HP-5
Column length (m) 30.60.60.30.30.
Carrier gas  HeHeHeliumHelium
Substrate      
Column diameter (mm) 0.250.320.250.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 38.30.40.40.40.
Tend (C) 220.260.270.250.250.
Heat rate (K/min) 5.2.4.5.5.
Initial hold (min) 1.2.4.2.2.
Final hold (min) 2.28.5.5.5.
I 766.780.0765.760.760.
ReferenceKrist, Stuebiger, et al., 2005Leffingwell and Alford, 2005van Loon, Linssen, et al., 2005N/AN/A
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-15 % Phenyl methyl siloxaneDB-5MS
Column length (m) 30.60.60.0.30.
Carrier gas HeliumHeHeHe 
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum) 0.250.250.251.0.25
Tstart (C) 40.35.35.40.90.
Tend (C) 250.230.230.250.200.
Heat rate (K/min) 5.2.2.7.30.
Initial hold (min) 2.4.4.10. 
Final hold (min) 5.25.25.5.10.
I 763.744.747.766.775.
ReferenceN/APark, Lee, et al., 2004Park, Lee, et al., 2004Ramírez, Estévez, et al., 2004Robledo and Arzuffi, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MDN-5DB-5SPB-1SPB-1
Column length (m) 60.30.30.30.30.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.40.60.40.40.
Tend (C) 280.280.280.200.200.
Heat rate (K/min) 5.20.4.3.3.
Initial hold (min) 2.1.10.10.10.
Final hold (min) 4.1.40.  
I 771.776.768.748.747.
ReferenceDhanda, Pegg, et al., 2003Mildner-Szkudlarz, Jelen, et al., 2003Pino, Marbot, et al., 2003Vichi, Castellote, et al., 2003Vichi, Pizzale, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5HP-5SPB-5HP-5OV-101
Column length (m)  30.30.60.50.
Carrier gas   HeliumHeNitrogen
Substrate      
Column diameter (mm)  0.250.250.320.25
Phase thickness (mum)   0.251. 
Tstart (C) 40.50.60.40.40.
Tend (C) 260.200.250.240.200.
Heat rate (K/min) 5.3.4.3.2.
Initial hold (min)   2. 10.
Final hold (min)   20.  
I 745.767.768.766.744.
ReferenceDiaz and Kite, 2002Isidorov and Jdanova, 2002Pino, Marbot, et al., 2002García, Martín, et al., 2000Tamura, Boonbumrung, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5DB-1DB-5DB-5
Column length (m) 50.30.60.60.60.
Carrier gas N2    
Substrate      
Column diameter (mm) 0.20.320.250.320.32
Phase thickness (mum)  1. 1.1.
Tstart (C) 80.40.30.40.40.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 1.3.4.3.3.
Initial hold (min)  5.25.5.5.
Final hold (min) 20. 20.2.2.
I 759.764.752.763.766.
ReferenceMenon, Chacko, et al., 1999Meynier, Novelli, et al., 1999Buttery, Ling, et al., 1997Kondjoyan, Viallon, et al., 1997Kondjoyan, Viallon, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1Ultra-2DB-1Ultra-2
Column length (m) 30.60.50.60.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.320.320.32
Phase thickness (mum) 0.25 0.52 0.52
Tstart (C) 50.30.40.30.40.
Tend (C) 200.200.250.200.250.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min) 2.25.3.25.3.
Final hold (min)  20.30.20.30.
I 747.752.763.752.759.
ReferenceRapior, Breheret, et al., 1997Buttery and Ling, 1995King, Matthews, et al., 1995Buttery, Stern, et al., 1994King, Hamilton, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-1DB-5
Column length (m) 30.30.60.60.60.
Carrier gas H2H2He He
Substrate      
Column diameter (mm) 0.320.320.250.320.32
Phase thickness (mum) 1.1.0.25 1.0
Tstart (C) 40.40.40.30.40.
Tend (C) 220.220.200.200.240.
Heat rate (K/min) 3.3.3.4.3.
Initial hold (min)   2.25. 
Final hold (min)    20. 
I 764.766.772.740.766.
ReferenceMoio, Dekimpe, et al., 1993Moio, Dekimpe, et al., 1993Shimoda, Shibamoto, et al., 1993Hansen, Buttery, et al., 1992Berdague, Denoyer, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HG-5DB-5DB-5OV-101DB-1
Column length (m) 50.60.60.50.60.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.320.250.250.280.32
Phase thickness (mum) 0.52    
Tstart (C) 35.40.40.80.50.
Tend (C) 250.160.160.200.230.
Heat rate (K/min) 3.2.2.2.4.
Initial hold (min) 15.5.5.  
Final hold (min) 45.   10.
I 781.772.771.756.744.
ReferenceDrumm and Spanier, 1991Macku and Shibamoto, 1991Macku and Shibamoto, 1991, 2Anker, Jurs, et al., 1990Binder, Benson, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5HP-5OV-101
Column length (m)  60.50.50.50.
Carrier gas  HeH2H2Nitrogen
Substrate      
Column diameter (mm)  0.250.30.30.25
Phase thickness (mum)      
Tstart (C) 50.30.80.80.70.
Tend (C) 230.200.250.250.200.
Heat rate (K/min) 4.4.16.16.2.
Initial hold (min)  25.   
Final hold (min) 10.5.   
I 744.744.756.766.742.
ReferenceBinder, Turner, et al., 1990Buttery, Teranishi, et al., 1990Spadone, Takeoka, et al., 1990Spadone, Takeoka, et al., 1990Sugisawa, Nakamura, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101DB-1DB-1
Column length (m) 50.50.50.60.60.
Carrier gas NitrogenN2N2  
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum)      
Tstart (C) 80.80.80.50.50.
Tend (C) 200.200.200.250.250.
Heat rate (K/min) 2.2.2.4.4.
Initial hold (min)     0.1
Final hold (min)    5.5.
I 740.742.743.744.746.
ReferenceSugisawa, Nakamura, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Binder, Flath, et al., 1989Binder and Flath, 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-1SE-30OV-101OV-101
Column length (m) 25.50.50.50.50.
Carrier gas Nitrogen He  
Substrate      
Column diameter (mm) 0.330.320.250.320.32
Phase thickness (mum) 1.00    
Tstart (C) 30.0.20.40.50.
Tend (C) 150.250.260.225.225.
Heat rate (K/min) 5.3.2.4.4.
Initial hold (min) 4. 4.0.10.1
Final hold (min)   16.30.30.
I 761.764.754.747.746.
ReferenceWilkins and Scholl, 1989Habu, Flath, et al., 1985Hackett, Gibbon, et al., 1985Stern, Flath, et al., 1985Stern, Flath, et al., 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101SP 2100SE-30SE-30OV-1
Column length (m) 50.40.50.50.183.
Carrier gas HeHelium HeN2
Substrate      
Column diameter (mm) 0.310.200.50.50.762
Phase thickness (mum)      
Tstart (C) 0.40.40.40.0.
Tend (C) 225.200.170.170.230.
Heat rate (K/min) 3.10.3.3.1.
Initial hold (min) 1. 3.3. 
Final hold (min)      
I 767.756.756.754.762.
Referencedel Rosario, de Lumen, et al., 1984Labropoulos, Palmer, et al., 1982Heydanek and McGorrin, 1981Heydanek and McGorrin, 1981, 2Schreyen, Dirinck, et al., 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bramston-Cook, 2013
Bramston-Cook, R., Kovats indices for C2-C13 hydrocarbons and selected oxygenated/halocarbons with 100 % dimethylpolysiloxane columns, 2013, retrieved from http://lotusinstruments.com/monographs/List .... [all data]

Srisajjalerwaja, Apichartsrangkoon, et al., 2012
Srisajjalerwaja, S.; Apichartsrangkoon, A.; Chaikham, P.; Chakrabandhu, Y.; Pathomrungsiyounggul, P.; Leksawasdi, N.; Supraditareporn, W.; Hirun, S., Color, capsaicin and volatile components of baked thai green chili (Capsicum anmuum Linn. var. Jak Ka Pat), J. Agricultural Sci., 2012, 4, 12, 75-84. [all data]

Leffingwell and Alford, 2011
Leffingwell, J.; Alford, E.D., Volatile constituents of the giant pufball mushroom (Calvatia gigantea), Leffingwell Rep., 2011, 4, 1-17. [all data]

Lazarevic, Radulovic, et al., 2010
Lazarevic, J.; Radulovic, N.; Palic, R.; Zlatkovic, B., Chemical Analusis of volatile constituents of Berula erecta (Hudson) Coville subsp. erecta (Apiaceae) from Serbia, J. Essential Oil. Res., 2010, 22, 3, 153-156, https://doi.org/10.1080/10412905.2010.9700290 . [all data]

Radulovic, Blagojevic, et al., 2010
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Radulovic, Dordevic, et al., 2010
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Kim and Chung, 2009
Kim, J.-S.; Chung, H.Y., GC-MS analysis of the volatile components in dried boxthorn (Lycium chimensis) Fruit, J. Korean Soc. Appl. Biol. Chem., 2009, 52, 5, 516-524, https://doi.org/10.3839/jksabc.2009.088 . [all data]

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Forero, Quijano, et al., 2008
Forero, M.D.; Quijano, C.E.; Pino, J.A., Volatile compounds of Chile pepper (Capsicum annuum L. var. glabriusculum) at two ripening stages, Flavour Fragr. J., 2008, 24, 1, 25-30, https://doi.org/10.1002/ffj.1913 . [all data]

Frerot, Velluz, et al., 2008
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Mildner-Szkudlarz and Jelen, 2008
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Thakeow, Angeli, et al., 2008
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Tava, Pecetti, et al., 2007
Tava, A.; Pecetti, L.; Ricci, M.; Pagnotta, M.A.; Russi, L., Volatile compounds from leaves and flowers of Bituminaria bituminosa (L.) Stirt. (Fabaceae) from Italy, Flavour Fragr. J., 2007, 22, 5, 363-370, https://doi.org/10.1002/ffj.1806 . [all data]

Vasta, Ratel, et al., 2007
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Krist, Stuebiger, et al., 2005
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Leffingwell and Alford, 2005
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van Loon, Linssen, et al., 2005
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Mildner-Szkudlarz, Jelen, et al., 2003
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Pino, Marbot, et al., 2003
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Vichi, Castellote, et al., 2003
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Vichi, Pizzale, et al., 2003
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Diaz and Kite, 2002
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Isidorov and Jdanova, 2002
Isidorov, V.; Jdanova, M., Volatile organic compounds from leaves litter, Chemosphere, 2002, 48, 9, 975-979, https://doi.org/10.1016/S0045-6535(02)00074-7 . [all data]

Pino, Marbot, et al., 2002
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García, Martín, et al., 2000
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Tamura, Boonbumrung, et al., 2000
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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References