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Hexahydrofarnesyl acetone


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5SPB-1DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.50.50.
Tend (C) 280.280.250.250.250.
Heat rate (K/min) 4.3.3.5.5.
Initial hold (min) 5.  3.3.
Final hold (min)   10.15.15.
I 1845.1847.1842.1838.1843.
ReferenceSaroglou, Marin, et al., 2007Vagionas, Ngassapa, et al., 2007Yu, Liao, et al., 2007Blagojevic, Radulovic, et al., 2006Blagojevic, Radulovic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.260.260.280.250.
Heat rate (K/min) 5.3.3.3.10.
Initial hold (min) 10.   2.
Final hold (min)     10.
I 1843.1847.1845.1850.1842.
ReferenceFlamini, Tebano, et al., 2006Javidnia, Miri, et al., 2006Javidnia K., Miri R., et al., 2006Kukic J., Petrovic S., et al., 2006Liu J.M., Nan P., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5HP-5MSHP-5MSHP-5MS
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 240.240.280.280.285.
Heat rate (K/min) 4.4.4.4.4.3
Initial hold (min)   5.5. 
Final hold (min)      
I 1858.1849.1845.1843.1849.
ReferenceRezazadeh, Hamedani, et al., 2006Rezazadeh, Hamedani, et al., 2006Saroglou, Dorizas, et al., 2006Saroglou, Dorizas, et al., 2006Vujisic L., Vuckovic I., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5MSHP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.50.80.60.50.
Tend (C) 300.220.300.250.260.
Heat rate (K/min) 4.3.4.10.10.
Initial hold (min) 5.  2.3.
Final hold (min)  20. 10. 
I 1842.1847.1845.61855.1846.
ReferenceVundac, Pfeifhofer, et al., 2006Xian Q., Chen H., et al., 2006Zhao C.X., Li, et al., 2006Zhao J.Y., Liu J.M., et al., 2006Zhao, Wang X.Y., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5HP-5HP-5DB-5
Column length (m) 25.30.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.40.250.250.250.25
Tstart (C) 80.60.60.60.40.
Tend (C) 270.220.260.260.260.
Heat rate (K/min) 10.5.3.3.2.
Initial hold (min)  10.  5.
Final hold (min)     20.
I 1817.1843.1843.1845.1835.
ReferenceZiegenbein, Hanssen, et al., 2006Celik, Gokturk, et al., 2005Javidnia, Miri, et al., 2005Javidnia, Miri, et al., 2005, 2Senatore, Napolitano, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSHP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 80.80.80.60.60.
Tend (C) 290.290.290.280.220.
Heat rate (K/min) 2.4.6.4.5.
Initial hold (min)    5.10.
Final hold (min)      
I 1846.1847.91848.91845.1843.
ReferenceZhao, Liang, et al., 2005Zhao, Liang, et al., 2005Zhao, Liang, et al., 2005Grujic-Jovanovic, Skaltsa, et al., 2004Dural, Bagci, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5HP-5HP-1
Column length (m) 30.30.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.33
Tstart (C) 60.60.60.60.40.
Tend (C) 240.220.280.280.260.
Heat rate (K/min) 3.5.3.4.2.
Initial hold (min)  10. 5.5.
Final hold (min)     20.
I 1843.1843.1848.1845.1847.
ReferenceFlamini, Cioni, et al., 2003Flamini, Luigi Cioni, et al., 2003Fokialakis, Melliou, et al., 2003Karioti, Skaltsa, et al., 2003Senatore, Rigano, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-1HP-5MSDB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.200.250.250.25
Phase thickness (mum) 0.250.200.250.250.25
Tstart (C) 60.70.60.60.60.
Tend (C) 280.220.300.240.280.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min) 5.   5.
Final hold (min)  15.   
I 1845.1828.1850.1844.1845.
ReferenceSkaltsa, Demetzos, et al., 2003Cavaleiro, Salgueiro, et al., 2002Couladis, Chinou, et al., 2002Flamini, Cioni, et al., 2002Fokialakis, Magiatis, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-5SE-54HP-5MS
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.300.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.60.80.60.
Tend (C) 280.250.280.300.280.
Heat rate (K/min) 3.5.3.8.4.
Initial hold (min) 5.2.5. 5.
Final hold (min)  5.   
I 1848.1855.1845.1848.1845.
ReferenceMagiatis, Skaltsounis, et al., 2002Shang, Hu, et al., 2002Aligiannis, Kalpoutzakis, et al., 2001Azevedo, Zinu, et al., 2001Skaltsa, Mavrommati, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54HP-5HP-5HP-5CP Sil 5 CB
Column length (m) 25.30.30.30.25.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.310.250.250.250.25
Phase thickness (mum)  0.250.250.25 
Tstart (C) 35.50.50.50.60.
Tend (C) 230.280.280.280.260.
Heat rate (K/min) 4.4.4.4.5.
Initial hold (min) 3.5.5.5. 
Final hold (min) 10.    
I 1868.811846.1846.1846.1835.
ReferenceYin, Xiu, et al., 2001Lazari, Skaltsa, et al., 2000Lazari, Skaltsa, et al., 2000, 2Lazari, Skaltsa, et al., 1999Weyerstahl, Marschall, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase SPB-1SE-54DB-5DB-5
Column length (m) 60.25.30.60.
Carrier gas N2H2HeHe
Substrate     
Column diameter (mm) 0.320.310.250.32
Phase thickness (mum) 0.25  1.
Tstart (C) 40.35.50.40.
Tend (C) 200.250.250.220.
Heat rate (K/min) 4.4.4.3.
Initial hold (min)  3.  
Final hold (min) 20.   
I 1822.1851.1848.1846.
ReferenceChen, Huang, et al., 1998Li, Wang, et al., 1998Gómez, Ledbetter, et al., 1993Le Quere and Latrasse, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Saroglou, Marin, et al., 2007
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Zhao C.X., Li, et al., 2006
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Zhao, Wang X.Y., et al., 2006
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Flamini, Cioni, et al., 2003
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Flamini, Luigi Cioni, et al., 2003
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Karioti, Skaltsa, et al., 2003
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Senatore, Rigano, et al., 2003
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Skaltsa, Demetzos, et al., 2003
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Cavaleiro, Salgueiro, et al., 2002
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Couladis, Chinou, et al., 2002
Couladis, M.; Chinou, I.B.; Tzakou, O.; Loukis, A., Composition and antimicrobial activity of the essential oil of Ballota pseudodictamnus L. Bentham, Phytother. Res., 2002, 16, 8, 723-726, https://doi.org/10.1002/ptr.1043 . [all data]

Flamini, Cioni, et al., 2002
Flamini, G.; Cioni, P.L.; Morelli, I., Analysis of the essential oil of the aerial parts of Viola etrusca from Monte Labbro (South Tuscany, Italy) and in vivo analysis of flower volatiles using SPME, Flavour Fragr. J., 2002, 17, 2, 147-149, https://doi.org/10.1002/ffj.1060 . [all data]

Fokialakis, Magiatis, et al., 2002
Fokialakis, N.; Magiatis, P.; Mitaku, S., Essential oil constituents of Valeriana italica and Valeriana tuberosa. Stereochemical and conformational study of 15-acetoxyvaleranone, Z. Naturforsch., 2002, 57c, 791-796. [all data]

Magiatis, Skaltsounis, et al., 2002
Magiatis, P.; Skaltsounis, A.-L.; Chinou, I.; Haroutounian, S.A., Chemical composition and in-vitro antimicrobial activity of the essential oils of three greek Achillea species, Z. Naturforsch., 2002, 57c, 287-290. [all data]

Shang, Hu, et al., 2002
Shang, C.; Hu, Y.; Deng, C.; Hu, K., Rapid determination of volatile constituents of Michelia alba flowers by gas chromatography-mass spectrometry with solid-phase microextraction, J. Chromatogr. A, 2002, 942, 1-2, 283-288, https://doi.org/10.1016/S0021-9673(01)01382-6 . [all data]

Aligiannis, Kalpoutzakis, et al., 2001
Aligiannis, N.; Kalpoutzakis, E.; Chinou, I.B.; Mitaku, S.; Gikas, E.; Tsarbopoulos, A., Composition and antimicrobial activity of the essential oils of five taxa of Sideritis from Greece, J. Agric. Food Chem., 2001, 49, 2, 811-815, https://doi.org/10.1021/jf001018w . [all data]

Azevedo, Zinu, et al., 2001
Azevedo, D.A.; Zinu, C.J.A.; Aquino Neto, F.R.; Simoneit, B.R.T., Possible origin of acyclic (linear and isoprenoid) and tricyclic terpane methyl ketones in a Tasmanian tasmanite bitumen, Org. Geochem., 2001, 32, 3, 443-448, https://doi.org/10.1016/S0146-6380(00)00164-9 . [all data]

Skaltsa, Mavrommati, et al., 2001
Skaltsa, H.D.; Mavrommati, A.; Constantinidis, T., A chemotaxonomic investigation of volatile constituents in Stachys subsect. Swainsonianeae (Labiatae), Phytochemistry, 2001, 57, 2, 235-244, https://doi.org/10.1016/S0031-9422(01)00003-6 . [all data]

Yin, Xiu, et al., 2001
Yin, W.; Xiu, Z.; Aijin, H., Analysis of the volatile components in trogopterorum feces by capillary gas chromatography and gas chromatography/mass spectrometry, Fenxi Huaxue, 2001, 29, 2, 195-198. [all data]

Lazari, Skaltsa, et al., 2000
Lazari, D.M.; Skaltsa, H.D.; Constantinidis, T., Volatile constituents of Cerastium candidissimum, a Greek endemic species, Flavour Fragr. J., 2000, 15, 3, 174-176, https://doi.org/10.1002/1099-1026(200005/06)15:3<174::AID-FFJ886>3.0.CO;2-Y . [all data]

Lazari, Skaltsa, et al., 2000, 2
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Lazari, Skaltsa, et al., 1999
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Notes

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