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Hexahydrofarnesyl acetone


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSHP-5 MSSLB-5 MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.70.50.50.50.
Tend (C) 220.290.280.250.240.
Heat rate (K/min) 5.5.4.3.3.
Initial hold (min) 10.  2. 
Final hold (min)  10. 10. 
I 1848.1847.1846.1841.1868.
ReferenceOgunwande, Flamini, et al., 2010Radulovic, Blagojevic, et al., 2009Zhao, Zeng, et al., 2009Lo Presti, Sciarrone, et al., 2008Sarikurkcu, Tepe, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-5MSHP-5MSHP-5DB-5
Column length (m) 20.30.30.30.30.
Carrier gas HeliumHeHeHeliumHe
Substrate      
Column diameter (mm) 0.180.250.250.250.25
Phase thickness (mum) 0.200.250.250.250.25
Tstart (C) 50.60.60.40.60.
Tend (C) 280.280.250.260.320.
Heat rate (K/min) 4.3.2.4.10.
Initial hold (min) 1. 8.  
Final hold (min)   15. 4.
I 1845.1837.1836.1840.1842.
ReferenceSkalicka-Wozniak, Los, et al., 2008Basta, Tzakou, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Ristic, Krivokuca-Dokic, et al., 2007Smelcerovic, Spiteller, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-101DB-5DB-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.250.20.250.25
Tstart (C) 60.60.70.60.60.
Tend (C) 240.240.200.220.260.
Heat rate (K/min) 5.5.3.4.4.
Initial hold (min) 2.2.2. 4.
Final hold (min)   15.  
I 1833.1833.1837.1847.1847.
ReferenceGohari, Hadjiakhoondi, et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Mastelic, Jerkovic, et al., 2006Morteza-Semnani, Akbarzadeh, et al., 2006Morteza-Semnani, Saeedi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5SPB-5HP-5MS
Column length (m) 30.30.30. 30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.25 0.25
Phase thickness (mum) 0.250.250.25 0.25
Tstart (C) 40.60.40.50.60.
Tend (C) 260.280.260.250.280.
Heat rate (K/min) 4.3.2.5.3.
Initial hold (min)   5.3. 
Final hold (min)   20.15. 
I 1853.1824.1846.1845.1824.
ReferencePetrovic, Ristic, et al., 2006Pitarokili, Tzakou, et al., 2006Senatore, Landolfi, et al., 2006Stojanovic, Palic, et al., 2006Tzakou, Said, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5HP-5MS
Column length (m) 25.30.30.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.320.320.25
Phase thickness (mum) 0.520.250.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 280.250.260.260.280.
Heat rate (K/min) 2.510.5.5.3.
Initial hold (min) 5.2.2.2. 
Final hold (min)  10.14.14. 
I 1844.1854.1846.1847.1825.
ReferenceWang, Kong, et al., 2006Wang, Yang, et al., 2006Yayli, Gülec, et al., 2006Yayli, Gülec, et al., 2006Basta, Tzakou, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1BPX5HP-5DB-5DB-5
Column length (m) 50.25.60.30.30.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.20.220.320.250.25
Phase thickness (mum) 0.50.250.250.250.25
Tstart (C) 60.50.30.60.60.
Tend (C) 250.320.260.240.220.
Heat rate (K/min) 2.5.2.3.4.
Initial hold (min)  5.2. 5.
Final hold (min) 60. 28.  
I 1830.1847.1848.51836.1838.
ReferenceBendimerad and Bendiab, 2005Dickschat, Bode, et al., 2005Leffingwell and Alford, 2005Miyazawa, Nishiguchi, et al., 2005Morteza-Semnani, Akbarzadeh, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5HP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.40.60.60.
Tend (C) 220.265.260.280.280.
Heat rate (K/min) 4.2.52.3.3.
Initial hold (min) 4.1.5.  
Final hold (min)  20.20.  
I 1847.1823.1846.1846.1823.
ReferenceMorteza-Semnani and Saeedi, 2005Sarkhail, Amin, et al., 2005Senatore, Apostolides Arnold, et al., 2005Slavkovska, Couladis, et al., 2005Tzakou and Constantinidis, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5MSDB-1DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.50.40.
Tend (C) 300.260.280.265.250.
Heat rate (K/min) 4.5.3.2.52.
Initial hold (min)  2. 1.5.
Final hold (min) 5.13. 20.20.
I 1843.1846.1846.1823.1845.
ReferenceUtsunomia, Kawata, et al., 2005Yayli, Yasar, et al., 2005Malencic, Couladis, et al., 2004Sarkhail, Amin, et al., 2004Senatore, Rigano, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m) 30.30.25.30.25.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm)  0.250.250.250.2
Phase thickness (mum)  0.250.250.25 
Tstart (C) 50.40.40.60.60.
Tend (C) 280.260.280.220.220.
Heat rate (K/min) 15.2.3.4.3.
Initial hold (min) 1.5.5.5. 
Final hold (min)   5.  
I 1849.1843.1829.1845.1813.
ReferenceSasaerila, Gries, et al., 2003Senatore and Bruno, 2003Merle, Blázquez, et al., 2002Morteza-Semnani, Saeedi, et al., 2002Schwob, Bessière, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-1RTX-1Optima-1CP Sil 5 CBSE-54
Column length (m) 25.30.25.25.25.
Carrier gas HeN2HeN2 
Substrate      
Column diameter (mm) 0.200.250.20 0.31
Phase thickness (mum) 0.250.250.250.39 
Tstart (C) 50.60.50.60.35.
Tend (C) 250.300.250.220.250.
Heat rate (K/min) 3.4.3.5.4.
Initial hold (min) 3. 3. 3.
Final hold (min)      
I 1815.1823.1836.1833.1824.
ReferenceBrun, Bessière, et al., 2001Kalemba, Marschall, et al., 2001de Beck, Bessière, et al., 2000Weyerstahl, Marschall, et al., 1999Ding, Deng, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima 1HP-1Ultra-2DB-1SE-54
Column length (m) 25.30.50.30.25.
Carrier gas HeliumHeHeHeN2
Substrate      
Column diameter (mm) 0.200.250.320.250.25
Phase thickness (mum) 0.250.10.521.0 
Tstart (C) 50.50.40.40.60.
Tend (C) 200.300.250.250.260.
Heat rate (K/min) 3.5.4.3.6.
Initial hold (min)  2.3. 2.
Final hold (min)  3.30.30. 
I 1833.1836.1850.1833.1846.
ReferenceFons, Rapior, et al., 1998Boatright and Crum, 1997King, Matthews, et al., 1995Peppard, 1992Bestmann, Classen, et al., 1988
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase DB-1
Column length (m) 60.
Carrier gas  
Substrate  
Column diameter (mm) 0.32
Phase thickness (mum)  
Tstart (C) 50.
Tend (C) 250.
Heat rate (K/min) 4.
Initial hold (min) 0.1
Final hold (min) 5.
I 1828.
ReferenceFlath, Mon, et al., 1983
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Ogunwande, Flamini, et al., 2010
Ogunwande, I.A.; Flamini, G.; Cioni, P.L.; Omikorede, O.; Azeez, R.A.; Ayodele, A.A.; Kamil, Y.O., Aromatic plants growing in Nigeria: essential oil constituents of Cassia alata (Linn.) Roxb. and Helianthus annuus L., Rec. Nat. Prod., 2010, 4, 4, 211-217. [all data]

Radulovic, Blagojevic, et al., 2009
Radulovic, N.S.; Blagojevic, P.D.; Palic, R.M.; Zlatkovic, B.K.; Stevanovic, B.M., Volatiles from vegetative organs of the paleoendemic resurrection plants Ramonda serbica Panc. and Ramonda nathaliae Panc. at Petrov, J. Serb. Chem. Soc., 2009, 74, 1, 35-44, https://doi.org/10.2298/JSC0901035R . [all data]

Zhao, Zeng, et al., 2009
Zhao, C.; Zeng, Y.; Wan, M.; Li, R.; Liang, Y.; Li, C.; Zeng, Z.; Chau, F.-T., Comparative analysis of essential oils from eight herbal medicines with pungent flavor and cool nature by GC-MS and chemometric resolution methods, J. Sep. Sci., 2009, 32, 4, 660-670, https://doi.org/10.1002/jssc.200800484 . [all data]

Lo Presti, Sciarrone, et al., 2008
Lo Presti, M.; Sciarrone, D.; Crupi, M.C.; Costa, R.; Ragusa, S.; Dugo, G.; Mondello, L., Evaliation of the volatile and chiral composition in Pistacia lentiscus L. essential oil, Flavour Fragr. J., 2008, 23, 4, 249-257, https://doi.org/10.1002/ffj.1878 . [all data]

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Sarikurkcu, C.; Tepe, B.; Daferera, D.; Polissiou, M.; Harmandar, M., Studies on the anioxidant activity of the essential oil and methanol extract of Marrubium globosum subsp. globosum (lamiaceae) by three different chemical assays, Bioresource Technol., 2008, 99, 10, 4239-4246, https://doi.org/10.1016/j.biortech.2007.08.058 . [all data]

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Basta, A.; Tzakou, O.; Couladis, M.; Yannitsaros, A., Essential oil composition of Prasium majus L. from Greece, Flavour Fragr. J., 2007, 22, 5, 347-349, https://doi.org/10.1002/ffj.1802 . [all data]

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Ferhat, M.A.; Tigrine-Kordjani, N.; Chemat, S.; Meklati, B.Y.; Chemat, F., Rapid Extraction of Volatile Compounds Using a New Simultaneous Microwave Distillation: Solvent Extraction Device, Chromatographia, 2007, 65, 3-4, 217-222, https://doi.org/10.1365/s10337-006-0130-5 . [all data]

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Mastelic, J.; Jerkovic, I.; Mesic, M., Volatile constituents from flowers, leaves, bark and wood of Prunus mahaleb L., Flavour Fragr. J., 2006, 21, 2, 306-313, https://doi.org/10.1002/ffj.1596 . [all data]

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Morteza-Semnani, Saeedi, et al., 2006
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Pitarokili, Tzakou, et al., 2006
Pitarokili, D.; Tzakou, O.; Loukis, A., Essential oil composition of Salvia verticillata, S. verbenaca, S. glutinosa and S. candidissima growing wild in Greece, Flavour Fragr. J., 2006, 21, 4, 670-673, https://doi.org/10.1002/ffj.1647 . [all data]

Senatore, Landolfi, et al., 2006
Senatore, F.; Landolfi, S.; Celik, S.; Bruno, M., Volatile components of Centaurea calcitrapa L. and Centaurea sphaerocephala L. ssp. sphaerocephala, two Asteraceae growing wild in Sicily, Flavour Fragr. J., 2006, 21, 2, 282-285, https://doi.org/10.1002/ffj.1585 . [all data]

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Wang, Kong, et al., 2006
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Basta, Tzakou, et al., 2005
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Bendimerad and Bendiab, 2005
Bendimerad, N.; Bendiab, S.A.T., Composition and antibacterial activity of Pseudocytisus integrifolius (Salisb.) essential oil from Algeria, J. Agric. Food Chem., 2005, 53, 8, 2947-2952, https://doi.org/10.1021/jf047937u . [all data]

Dickschat, Bode, et al., 2005
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Leffingwell and Alford, 2005
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Miyazawa, Nishiguchi, et al., 2005
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Morteza-Semnani, Akbarzadeh, et al., 2005
Morteza-Semnani, K.; Akbarzadeh, M.; Rostami, B., The essential oil composition of Teucrium chamaedrys L. from Iran, Flavour Fragr. J., 2005, 20, 5, 544-546, https://doi.org/10.1002/ffj.1479 . [all data]

Morteza-Semnani and Saeedi, 2005
Morteza-Semnani, K.; Saeedi, M., The essential oil composition of Phlomis bruguieri Desf. from Iran, Flavour Fragr. J., 2005, 20, 3, 344-346, https://doi.org/10.1002/ffj.1459 . [all data]

Sarkhail, Amin, et al., 2005
Sarkhail, P.; Amin, G.; Surmaghi, M.H.S.; Shafiee, A., Composition of the volatile oils of Phlomis lanceolata Boiss. Hohen., Phlomis anisodonta Boiss. and Phlomis bruguieri Desf. from Iran, Flavour Fragr. J., 2005, 20, 3, 327-329, https://doi.org/10.1002/ffj.1427 . [all data]

Senatore, Apostolides Arnold, et al., 2005
Senatore, F.; Apostolides Arnold, N.; Bruno, M., Volatile components of Centaurea eryngioides Lam. and Centaurea liberica Trev. var. hermonis Boiss. Lam., two Asteraceae growing wild in Lebanon, Nat. Prod. Res., 2005, 19, 8, 749-754, https://doi.org/10.1080/14786410412331302136 . [all data]

Slavkovska, Couladis, et al., 2005
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Tzakou and Constantinidis, 2005
Tzakou, O.; Constantinidis, T., Chemotaxonomic significance of volatile compounds in Thymus samius and its related species Thymus atticus and Thymus parnassicus, Biochem. Syst. Ecol., 2005, 33, 11, 1131-1140, https://doi.org/10.1016/j.bse.2005.03.008 . [all data]

Utsunomia, Kawata, et al., 2005
Utsunomia, H.; Kawata, J.; Chanoki, W.; Shirakawa, N.; Miyazawa, M., Components of Essential Oil from Woods of Prunus mume Sieb. at Zucc., J. Oleo Sci., 2005, 54, 11, 609-612, https://doi.org/10.5650/jos.54.609 . [all data]

Yayli, Yasar, et al., 2005
Yayli, N.; Yasar, A.; Gülec, C.; Usta, A.; Kolayli, S.; Coskuncelebi, K.; Karaoglu, S., Composition and antimicrobial activity of essential oils from Centaurea sessilis and Centaurea armena, Phytochemistry, 2005, 66, 14, 1741-1745, https://doi.org/10.1016/j.phytochem.2005.04.006 . [all data]

Malencic, Couladis, et al., 2004
Malencic, Dj.; Couladis, M.; Mimica-Dukic, N.; Popovic, M.; Boza, P., Essential oils of three Salvia species from the Pannonian part of Serbia, Flavour Fragr. J., 2004, 19, 3, 225-228, https://doi.org/10.1002/ffj.1291 . [all data]

Sarkhail, Amin, et al., 2004
Sarkhail, P.; Amin, G.; Shafiee, A., Composition of the essential oil of Phlomis persica Boiss and Phlomis chorassanica Bunge from Iran, Flavour Fragr. J., 2004, 19, 6, 538-540, https://doi.org/10.1002/ffj.1338 . [all data]

Senatore, Rigano, et al., 2004
Senatore, F.; Rigano, D.; de Fusco, R.; Bruno, M., Composition of the essential oil from flowerheads of Chrysanthemum coronarium L. (Asteraceae) growing wild in Southern Italy, Flavour Fragr. J., 2004, 19, 2, 149-152, https://doi.org/10.1002/ffj.1285 . [all data]

Sasaerila, Gries, et al., 2003
Sasaerila, Y.; Gries, R.; Gries, G.; Khaskin, G.; King, S.; Takacs, S.; Hardi, Sex pheromone components of male Tirathaba mundella (Lepidoptera : Pyralidae), Chemoecology, 2003, 13, 89-93. [all data]

Senatore and Bruno, 2003
Senatore, F.; Bruno, M., Composition of the essential oil of Pallenis spinosa (L.) Cass. (Asteraceae), Flavour Fragr. J., 2003, 18, 3, 195-197, https://doi.org/10.1002/ffj.1180 . [all data]

Merle, Blázquez, et al., 2002
Merle, H.; Blázquez, M.A.; Boira, H., Chemical composition of the essential oil of Eriobotrya japonica (Thunb.) Lindl. flowers in the western Mediterranean area in International Symposium on Loquat, April 11-13, 2002 (CIHEAM-IAMZ, 2003, p. 191-193), Llácer,G.; Badenes,M.L., ed(s)., Centre International de Hautes Etudes Agronomiques Mediterranean, Valencia, Spain, 2002, 191-193. [all data]

Morteza-Semnani, Saeedi, et al., 2002
Morteza-Semnani, K.; Saeedi, M.; Vahedi, M., Volatile constituents of Iranian Hypericum perfloratum L., Oriental J. Chem., 2002, 18, 3, 443-444. [all data]

Schwob, Bessière, et al., 2002
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Brun, Bessière, et al., 2001
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Notes

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