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(1R,5S,6R)-2,7,7-Trimethylbicyclo[3.1.1]hept-2-en-6-yl acetate


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSRTX-1RTX-1SE-52HP-5MS
Column length (m) 30.60.60.50.30.
Carrier gas HeliumHeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.220.220.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 250.230.230.280.280.
Heat rate (K/min) 7.2.2.3.3.
Initial hold (min) 1.    
Final hold (min) 5.30.30.20. 
I 1267.1244.1253.1264.1264.
ReferenceZouari, Zouari, et al., 2010Museli, Pau, et al., 2009Museli, Pau, et al., 2009Djarri, Medjroubi, et al., 2008Basta, Pavlovic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Col-Elite 5MSDBP-5DB-1DB-5DBP-5
Column length (m) 30.25.50.30.25.
Carrier gas HeHeliumHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.220.250.250.22
Tstart (C) 30.40.95.50.40.
Tend (C) 246.250.240.240.250.
Heat rate (K/min) 3.3.4.4.3.
Initial hold (min)  1.  1.
Final hold (min)  10.  10.
I 1258.1230.1258.1263.1230.
ReferenceGudaityte and Venskutonis R.P., 2007Heravi and Sereshti, 2007Pala-Paul, Brophy, et al., 2007Sefidkon, Abbasi, et al., 2007Sereshti and Samadi, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-1NB-30DB-5HP-5MS
Column length (m) 30.50.30.15.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.20.20.25
Phase thickness (mum) 0.250.330.250.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 280.250.250.305.200.
Heat rate (K/min) 4.2.2.15.4.
Initial hold (min)    2.30.
Final hold (min)  40.   
I 1265.1244.1248.1264.1256.
ReferenceEbrahim Sajjadi and Mehregan, 2006Filippi, Lanfranchi, et al., 2006Orav, Raal, et al., 2006Sebastián, Urzúa, et al., 2006Gauvin and Smadja, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5DB-5HP-5MSDB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 50.60.60.60.50.
Tend (C) 265.240.220.280.265.
Heat rate (K/min) 2.55.3.4.2.5
Initial hold (min) 1. 4. 1.
Final hold (min) 30.   20.
I 1242.1262.1261.1263.1239.
ReferenceKhalighi-Sigaroodi, Hadijiakhoondi, et al., 2005Saeidnia, Gohari, et al., 2005Salehi, Sefidkon, et al., 2005Sadeghpour, Asghari, et al., 2004Sarkhail, Amin, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-5DB-5HP-5
Column length (m) 30.30.50.30.30.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.50.60.60.
Tend (C) 250.275.220.280.280.
Heat rate (K/min) 2.4.3.4.4.
Initial hold (min) 5. 2.10. 
Final hold (min) 20. 10.40. 
I 1263.1262.1267.1262.1262.
ReferenceSenatore, Rigano, et al., 2004Afsharypuor and Jahromy, 2003Juteau, Jerkovic, et al., 2003Pino, Marbot, et al., 2003Sajjadi and Mehregan, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5DB-1SPB-5HP-5
Column length (m) 60.30.60.50. 
Carrier gas HeN2N2He 
Substrate      
Column diameter (mm) 0.250.250.250.32 
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 40.60.75.60.40.
Tend (C) 280.220.220.240.210.
Heat rate (K/min) 4.5.4.3.2.
Initial hold (min) 5.10.1.  
Final hold (min)   8.20. 
I 1241.1263.1255.1223.1266.
ReferenceSefidkon, Jalili, et al., 2002Gallori, Flamini, et al., 2001Bailac, Dellacasa, et al., 1999Doneanu and Anitescu, 1998Collin, Deslauriers, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase HP-5
Column length (m)  
Carrier gas  
Substrate  
Column diameter (mm)  
Phase thickness (mum)  
Tstart (C) 40.
Tend (C) 210.
Heat rate (K/min) 2.
Initial hold (min)  
Final hold (min)  
I 1266.
ReferenceCollin, Deslauriers, et al., 1993
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zouari, Zouari, et al., 2010
Zouari, S.; Zouari, N.; Fakhfakh, N.; Bougatel, A.; Ayadi, M.A.; Neffati, M., Chemical composition and biological activities of a new essential oil chemotype of Tunisian Artemisia herba alba Asso, J. Medicinal Plants Res., 2010, 4, 10, 871-880. [all data]

Museli, Pau, et al., 2009
Museli, A.; Pau, M.; Desjobert, J.-M.; Foddai, M.; Usai, M.; Costa, J., Volatile constituents of Achllea ligustica All. by HS-SPME/GC/GC-MS. Comparison with essential oils obtained by hydrodistillation from Corsica and Sardinia, Chromatographia, 2009, 69, 5/6, 575-585, https://doi.org/10.1365/s10337-008-0939-1 . [all data]

Djarri, Medjroubi, et al., 2008
Djarri, L.; Medjroubi, K.; Akkai, S.; Elomri, A.; Seguin, E.; Groult, M.-L.; Verite, P., Variability of two essential olis of Kundmannia sicula (L.) DC., a traditional Algerian medicinal plant, Molecules, 2008, 13, 4, 812-817, https://doi.org/10.3390/molecules13040812 . [all data]

Basta, Pavlovic, et al., 2007
Basta, A.; Pavlovic, M.; Couladis, M.; Tzakou, O., Essential oil composition of the flowerheads of Chrysanthemum coronarium L. from Greece, Flavour Fragr. J., 2007, 22, 3, 197-200, https://doi.org/10.1002/ffj.1781 . [all data]

Gudaityte and Venskutonis R.P., 2007
Gudaityte, O.; Venskutonis R.P., Chemotypes of Achillea millefolium transferred from 14 different locations in Lithuania to the controlled environment, Biochem. Syst. Ecol., 2007, 35, 9, 582-592, https://doi.org/10.1016/j.bse.2007.03.016 . [all data]

Heravi and Sereshti, 2007
Heravi, M.J.; Sereshti, H., Determination of Essential Oil Components of Artemisia haussknechtii Boiss. using Simultaneous Hydrodistillation-Static Headspace Liquid Phase Microextraction - Gas Chromatography Mass Spectrometry, J. Chromatogr. A, 2007, 1160, 1-2, 81-89, https://doi.org/10.1016/j.chroma.2007.05.096 . [all data]

Pala-Paul, Brophy, et al., 2007
Pala-Paul, J.; Brophy, J.J.; Perez-Alonso, M.J.; Usano, J.; Soria, S.C., Essential oil composition of the different parts of Eryngium corniculatum Lam. (Apiaceae) from Spain, J. Chromatogr. A, 2007, 1175, 2, 289-293, https://doi.org/10.1016/j.chroma.2007.10.061 . [all data]

Sefidkon, Abbasi, et al., 2007
Sefidkon, F.; Abbasi, K.; Jamzad, Z.; Ahmadi, S., The effect of distillation methods and stage of plant growth on the essential oil content and composition of Satureja rechingeri Jamzad, Food Chem., 2007, 100, 3, 1054-1058, https://doi.org/10.1016/j.foodchem.2005.11.016 . [all data]

Sereshti and Samadi, 2007
Sereshti, H.; Samadi, S., Comparison of hydrodistillation-headspace liquid phase microextraction techniques with hydrodistillation in determination of essential oils in Artemisia Haussknechtii Boiss, JSUT, 2007, 33, 2, 7-17. [all data]

Ebrahim Sajjadi and Mehregan, 2006
Ebrahim Sajjadi, S.; Mehregan, I., Volatile constituents of flowers and leaves of Anthemis hyalina, Chem. Nat. Compd. (Engl. Transl.), 2006, 42, 5, 531-533, https://doi.org/10.1007/s10600-006-0207-2 . [all data]

Filippi, Lanfranchi, et al., 2006
Filippi, J.-J.; Lanfranchi, D.-A.; Prado, S.; Baldovini, N.; Meierhenrich, U.J., Composition, Enantiomeric Distribution, and Antibacterial Activity of the Essential Oil of Achillea ligustica All. from Corsica, J. Agric. Food Chem., 2006, 54, 17, 6308-6313, https://doi.org/10.1021/jf060752y . [all data]

Orav, Raal, et al., 2006
Orav, A.; Raal, A.; Arak, E.; Müürisepp, M.; Kailas, T., Composition of the essential oil of Artemisia absinthium L. of different geographical origin, Proc. Est. Acad. Sci. Chem., 2006, 55, 3, 155-165. [all data]

Sebastián, Urzúa, et al., 2006
Sebastián, B.; Urzúa, A.M.; Vines, M., Analysis of surface and volatile compounds of flower heads of introduced plants of Chrysanthemum coronarium L. growing wild in Chile, Flavour Fragr. J., 2006, 21, 5, 783-785, https://doi.org/10.1002/ffj.1712 . [all data]

Gauvin and Smadja, 2005
Gauvin, A.; Smadja, J., Essential oil composition of four Psiadia species from Reunion Island: A chemotaxonomic study, Biochem. Syst. Ecol., 2005, 33, 7, 705-714, https://doi.org/10.1016/j.bse.2004.12.013 . [all data]

Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005
Khalighi-Sigaroodi, F.; Hadijiakhoondi, A.; Shahverdi, A.R.; Mozaffarian, V.-A.; Shafiee, A., Chemical composition and antimicrobial activity of the essential oil of Ferulago Bernardii Tomk. and M.Pimen., DARU, 2005, 13, 3, 100-104. [all data]

Saeidnia, Gohari, et al., 2005
Saeidnia, S.; Gohari, A.R.; Yassa, N.; Shafiee, A., Composition of the volatile oil of Achillea conferta DC. from Iran, DARU, 2005, 13, 1, 34-36. [all data]

Salehi, Sefidkon, et al., 2005
Salehi, P.; Sefidkon, F.; Bazzaz Tolami, L.; Sonboli, A., Essential oil composition of Salvia palaestina Benth. from Iran, Flavour Fragr. J., 2005, 20, 5, 525-527, https://doi.org/10.1002/ffj.1448 . [all data]

Sadeghpour, Asghari, et al., 2004
Sadeghpour, O.; Asghari, G.; Ardekani, M.R.S., Composition of essential oil of Artemisia persica Boiss. from Iran, Iran. J. Pharm. Res., 2004, 3, 65-67. [all data]

Sarkhail, Amin, et al., 2004
Sarkhail, P.; Amin, G.; Shafiee, A., Composition of the essential oil of Phlomis persica Boiss and Phlomis chorassanica Bunge from Iran, Flavour Fragr. J., 2004, 19, 6, 538-540, https://doi.org/10.1002/ffj.1338 . [all data]

Senatore, Rigano, et al., 2004
Senatore, F.; Rigano, D.; de Fusco, R.; Bruno, M., Composition of the essential oil from flowerheads of Chrysanthemum coronarium L. (Asteraceae) growing wild in Southern Italy, Flavour Fragr. J., 2004, 19, 2, 149-152, https://doi.org/10.1002/ffj.1285 . [all data]

Afsharypuor and Jahromy, 2003
Afsharypuor, S.; Jahromy, M.M., Constituents of the essential oil from Tanacetum lingulatum (Boiss.) Bornm., J. Essent. Oil Res., 2003, 15, 2, 74-76, https://doi.org/10.1080/10412905.2003.9712069 . [all data]

Juteau, Jerkovic, et al., 2003
Juteau, F.; Jerkovic, I.; Masotti, V.; Milos, M.; Mastelic, J.; Bessière, J.-M.; Viano, J., Composition and antimicrobial activity of the essential oil of Artemisia absinthium from Croatia and France, Planta Medica, 2003, 69, 2, 158-161, https://doi.org/10.1055/s-2003-37714 . [all data]

Pino, Marbot, et al., 2003
Pino, J.A.; Marbot, R.; Fuentes, V., Characterization of volatiles in Bullock's heart (Annona reticulata L.) fruit cultivars from Cuba, J. Agric. Food Chem., 2003, 51, 13, 3836-3839, https://doi.org/10.1021/jf020733y . [all data]

Sajjadi and Mehregan, 2003
Sajjadi, S.E.; Mehregan, I., Chemical composition of the essential oil of Prangos Asperula Boiss. subsp. haussknechtii (Boiss.) Hernst. et Heyn fruits, 2003, retrieved from http://www1.tums.ac.ir/daru/daru2%2020003/Dr%20Sajadi.PDF. [all data]

Sefidkon, Jalili, et al., 2002
Sefidkon, F.; Jalili, A.; Mirhaji, T., Essential oil composition of three Artemisia spp. from Iran, Flavour Fragr. J., 2002, 17, 2, 150-152, https://doi.org/10.1002/ffj.1063 . [all data]

Gallori, Flamini, et al., 2001
Gallori, S.; Flamini, G.; Bilia, A.R.; Morelli, I.; Landini, A.; Vincieri, F.F., Chemical composition of some traditional herbal drug preparations: essential oil and aromatic water of costmary (Balsamita suaveolens Pers.), J. Agric. Food Chem., 2001, 49, 12, 5907-5910, https://doi.org/10.1021/jf0107656 . [all data]

Bailac, Dellacasa, et al., 1999
Bailac, P.N.; Dellacasa, A.D.; Duschatzky, C.B.; Firpo, N.; Ponzi, M.I., Composicion del aceite esencial y actividad antimicrobiana de Aloysia gratissima de San Luis - Argentina, An. Asoc. Quim. Argent., 1999, 87, 3/4, 149-153. [all data]

Doneanu and Anitescu, 1998
Doneanu, C.; Anitescu, G., Supercritical carbon dioxide extraction of Angelica archangelica L. root oil, J. Supercrit. Fluids, 1998, 12, 1, 59-67, https://doi.org/10.1016/S0896-8446(97)00040-5 . [all data]

Collin, Deslauriers, et al., 1993
Collin, G.J.; Deslauriers, H.; Pageau, N.; Gagnon, M., Essential oil of Tansy (Tanacetum vulgare L.) of Canadian origin, J. Essent. Oil Res., 1993, 5, 6, 629-638, https://doi.org/10.1080/10412905.1993.9698296 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References