Humulene

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Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TR-5 MSDB-5RTX-1RTX-1Mega-5
Column length (m) 15.30.60.60.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.220.220.25
Phase thickness (μm) 0.250.250.250.250.25
Program 35 0C (3 min) 2 0C/min -> 60 0C (3 min) 2 0C/min -> 80 0C (3 min) 4 0C/min -> 120 0C (3 min) 5 0C/min -> 150 0C (3 min) 15 0C/min -> 240 0C (10 min)not specifiednot specifiednot specifiednot specified
I 1436.1452.1450.1450.1455.
ReferenceKurashov, Mitrukova, et al., 2014Rodriques, Amorim, et al., 2013Bendiabdellah, El Amine Dib, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Dell'Agli, Sanna, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSCBP-5Polydimethyl siloxane with 5 % Ph groupsHP-5DB-5 MS
Column length (m) 30.30.30.25.30.
Carrier gas HeliumHeliumHeliumHydrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.520.25
Program not specified60 0C 3 0C/min -> 240 0C 10 0C/min -> 280 0C (10 min)50 0C 4 0C/min -> 200 0C (5 min) 20 0C/min -> 280 0Cnot specified45 0C (5 min) 4 0C/min -> 150 0C (2 min) 5 0C/min -> 250 0C (5 min) 10 0C/min -> 275 0C (5 min)
I 1453.1454.1454.1456.1472.
ReferenceKotowska, Zalikowski, et al., 2012de Morais, Oliveira, et al., 2012da Silva, de Souza, et al., 2012Velickovic, Ristic, et al., 2012Arenas, Acevedo, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl polydimethyl siloxaneHP-5 MSHP-5 MSHP-5 MSCBP-5
Column length (m)  30.30.30.30.
Carrier gas  HeliumHeliumHeliumHelium
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Program not specified60 0C (1 min) 10 0C -> 180 0C (1 min) 20 0C/min -> 280 0C (15 min)not specifiednot specified60 0C 3 0C/min -> 246 0C 10 0C/min -> 270 0C (5 min)
I 1452.1454.1454.1454.1455.
ReferenceChaverri, Diaz, et al., 2011Chu, Liu, et al., 2011Feizbakhsh and Naeemy, 2011Feizbakhsh and Naeemy, 2011Fortes, Naves, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CBHP-5DB-5HP-5 MSHP-5 MS
Column length (m) 50.30.60.30. 
Carrier gas NitrogenHeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.320.320.250.25 
Phase thickness (μm) 1.200.251.000.25 
Program 36 0C 20 0C/min -> 85 0C 1 0C/min -> 145 0C 3 0C/min -> 250 0C (30 min)not specified40 0C 4 0C/min -> 230 0C 100 0C/min -> 260 0C (11.7 min)40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0Cnot specified
I 1469.1455.1499.1453.1455.
ReferenceGros, Nizet, et al., 2011Kahriman, Tosun, et al., 2011Miyazaki, Plotto, et al., 2011Nance and Setzer, 2011Payo, Colo, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSZB-5HP-5 MSHP-5 MSHP-5
Column length (m)  30.30.30.30.
Carrier gas  NitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Program not specifiednot specified70 0C (2 min) 10 0C/min -> 150 0C (15 min) 5 0C/min -> 240 0C50 0C (2 min) 3 0C/min -> 130 0C (2 min) 5 0C/min -> 270 0Cnot specified
I 1456.1433.1418.1438.1454.
ReferencePayo, Colo, et al., 2011Vazquez, Demmel, et al., 2011Bagci, Yazgin, et al., 2010Bamoniri, Mirjalili, et al., 2010Bi Kouame, Bedi, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1CP-Sil 8 CBHP-5DB-5DB-5
Column length (m) 60.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHydrogen
Substrate      
Column diameter (mm) 0.220.250.320.200.25
Phase thickness (μm) 0.250.250.250.320.25
Program not specifiedMulti-rise programnot specified60 0C (1 min) 3 0C/min -> 140 0C 50 0C/min -> 250 0C (3 min)35 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 280 0C
I 1451.1455.1455.1446.1450.
ReferenceDib, Djabou, et al., 2010Di Giusto, Bessiere, et al., 2010Kahriman, Tosun, et al., 2010Nezhadali and Parsa, 2010Pontes, Silva, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSDB-5DB-1-MSHP-5 MSDB-1
Column length (m) 10.30.60.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.100.250.250.250.25
Phase thickness (μm) 0.100.250.250.250.25
Program not specifiednot specifiednot specifiednot specifiednot specified
I 1454.1454.1472.1452.1456.
ReferenceScandinaro, Tranchida, et al., 2010Scherer, Wagner, et al., 2010Takeoka, Hobbs, et al., 2010Vedernikov and Roschin, 2010Xu, Tang, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5HP-5HP-5
Column length (m) 30.30.25.25.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm) 0.250.250.170.170.17
Program 50 0C m6 0C/min -> 140 0C 5 0C/min -> 160 0C (1 min) 10 0C/min -> 200 0C50 0C m6 0C/min -> 140 0C 5 0C/min -> 160 0C (1 min) 10 0C/min -> 200 0C60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C (15 min)60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C (15 min)60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C (15 min)
I 1462.1433.1447.1447.1454.
ReferenceCourtois, Paine, et al., 2009Courtois, Paine, et al., 2009Custer, 2009Custer, 2009Custer, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5DB-1Optima-5MS
Column length (m) 25.25.25.60.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.320.320.250.32
Phase thickness (μm) 0.170.170.170.250.25
Program not specifiednot specifiednot specified50 0C (5 min) 3 0C/min -> 120 0C 5 0C/min -> 250 0C (3 min) 15 0C/min -> 300 0C (20 min)40 0C (5 min) 5 0C/min -> 230 0C 30 0C/min -> 280 0C (5 min)
I 1454.1454.1454.1469.1449.
ReferenceCuster, 2009Custer, 2009Custer, 2009Delort and Jaquier, 2009HEuskin, Godin, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneElite-5 MSElite-5 MSRTX-5RTX-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumNitrogenNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 50 0C (2 min) 10 0C/min -> 150 0C 15 0C/min -> 300 0C (10 min)60 0C (1 min) 1.5 0C/min -> 185 0C (1 min) 9 0C/min -> 275 0C (2 min)60 0C (1 min) 1.5 0C/min -> 185 0C (1 min) 9 0C/min -> 275 0C (2 min)60 0C 95 min) 110 0C 3 0C/min -> 200 0C 5 0C/min -> 220 0C 95 min)not specified
I 1450.1443.1451.1458.1455.
ReferenceHuang, Qin, et al., 2009Kapoor, Singh, et al., 2009Kapoor, Singh, et al., 2009Leela, Vipin, et al., 2009Leela, Vipin, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSDB-1DB-1HP-5
Column length (m) 25.30.30.30.30.
Carrier gas HeliumHeliumHydrogenHydrogen 
Substrate      
Column diameter (mm) 0.320.250.250.250.32
Phase thickness (μm) 0.170.250.250.25 
Program 60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0C40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)not specified
I 1450.1455.1447.1447.1454.
ReferenceMaggi, Bilek, et al., 2009Mancini, Arnold, et al., 2009Mendes, Trindade, et al., 2009Mendes, Trindade, et al., 2009, 2Riahi, Pourbasheer, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSHP-1HP-5 MSHP-5 MSDB-5
Column length (m) 30.25.30.30.30.
Carrier gas Helium HeliumHeliumHydrogen
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.170.250.250.25
Program not specifiednot specified32 0C (1 min) 50 0C/min -> 115 0C 1.5 0C/min -> 145 0C 12 0C/min -> 240 0C (10 min)32 0C (1 min) 50 0C/min -> 115 0C 1.5 0C/min -> 145 0C 12 0C/min -> 240 0C (10 min)35 0C 4 0C/min -> 180 0C 17 0C/min -> 280 0C (10 min)
I 1453.1447.1421.1455.1455.
ReferenceSu, Wang, et al., 2009Wetwiayaklung, Thavanapong, et al., 2009Zellner, Amorim, et al., 2009Zellner, Amorim, et al., 2009de Albuquerque, Alves, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m) 25.30.30.30.30.
Carrier gas NitrogenHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specified35 0C 1 0C/min -> 60 0C 3 0C/min -> 170 0C 8 0C/min -> 200 0C 15 0C/min -> 280 0C (5 min)35 0C 1 0C/min -> 60 0C 3 0C/min -> 170 0C 8 0C/min -> 200 0C 15 0C/min -> 280 0C (5 min)35 0C 1 0C/min -> 60 0C 3 0C/min -> 170 0C 8 0C/min -> 200 0C 15 0C/min -> 280 0C (5 min)not specified
I 1467.1444.1445.1448.1454.
ReferenceChieng, Assim, et al., 2008Gazim, Rezende, et al., 2008Gazim, Rezende, et al., 2008Gazim, Rezende, et al., 2008Gazim, Rezende, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5CB-1CB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specifiednot specifiednot specified40 0C (2 min) 4 0C/min -> 180 0C 20 0C/min -> 220 0C (1 min)not specified
I 1454.1454.1454.1418.1421.
ReferenceGazim, Rezende, et al., 2008Gazim, Rezende, et al., 2008Isidorov, Lech, et al., 2008Kannaste, Vongvanich, et al., 2008Kannaste, Vongvanich, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBCP Sil 8 CBSLB-5 MSHP-5MSDB-1
Column length (m) 30.50.30.30.30.
Carrier gas  HeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 60C => 2.5C/min => 170C => 10C/min => 250C (5min)not specifiednot specified40 0C (2 min) 3 0C/min -> 180 0C (2 min) 15 0C -> 280 0C45C => 3C/min => 175C => 15C/min => 300C (10min)
I 1454.1455.1457.1432.1447.
ReferenceKristiawan, Sobolik, et al., 2008Kupcinskiene, Stikliene, et al., 2008Lo Presti, Sciarrone, et al., 2008Ning, Zheng, et al., 2008Nogueira, Marcelo-Curto, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 8CB-MSHP-5HP-5Elite-1DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.25 
Program 50 0C(3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 260 0C40 0C (3 min) 3 0C/min -> 160 0C (2 min) 8 0C/min -> 220 0C (3 min)not specifiednot specified80 0C (2 min) 3 0C/min -> 180 0C 10 0C/min -> 300 0C (10 min)
I 1458.1455.1454.1455.1459.
ReferenceProfitt, Schatz, et al., 2008Qiao, Xie, et al., 2008Qiao, Xie, et al., 2008Raj, Baby, et al., 2008Santos, Costa, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BPX-5DB-5 MSRTX-5RTX-5
Column length (m) 30.7.530.30.30.
Carrier gas HeliumHelium HeliumHelium
Substrate      
Column diameter (mm) 0.250.100.250.250.25
Phase thickness (μm)  10.0.250.250.25
Program not specifiednot specified80 0C (1.5 min) 4 pC/min -> 180 0C 10 0C/min -> 300 0C (10 min)60 0C (5 min) 5 0C/min -> 110 0C 3 0C/min -> 220 0C (5 min)not specified
I 1455.1454.1457.1460.1455.
ReferenceSantos, Costa, et al., 2008Shellie, 2008Silva, Doria, et al., 2008Zachariah, Leela, et al., 2008Zachariah, Leela, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase 5 % Phenyl methyl siloxaneDB-5DB-5DB-1DB-5
Column length (m)  30.30.30.30.
Carrier gas  HeHeHeHelium
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (μm)  0.10.250.10.25
Program not specified35C => 4C/min => 180C => 10C/min => 250C35C => 4C/min => 180C => 10C/min => 250C35C => 4C/min => 180C => 10C/min => 250C35 0C 4 0C/min -> 180 0C 10 0C/min -> 250 0C
I 1492.1456.1455.1455.1455.
ReferenceAgabriel, Cornu, et al., 2007Albuquerque M.R.J.R., Costa S.M.O., et al., 2007Albuquerque, Lemos, et al., 2007Albuquerque, Vasconcelos Silva, et al., 2007Arriaga, Rodrigues, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSCBP-5HP-5MSHP-5MSSPB-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 60C => 1C/min => 65C => 3C/min => 120C => 5C/min => 180C(5min) => 5C/min => 250C (20min)60C(2min) => 3C/min => 240C => 10C/min => 300C40C => 3C/min => 100C => 5C/min => 230C(2min)40C(10min) => 3C/min => 200C => 2C/min => 220C70C(3min) => 4C/min => 120C => 8C/min => 250C(5min)
I 1453.1414.1447.1454.1457.
ReferenceBarra A., Coroneo V., et al., 2007Cheriti, Saad, et al., 2007Chokeprasert P., Charles A.L., et al., 2007Cole, Haber, et al., 2007Díaz-Maroto, Castillo, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSDB-1HP-5 MSDB-1
Column length (m) 30.30.30.30.30.
Carrier gas  HeliumHeHeliumH2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 75C(4min) => 5C/min => 135C => 1C/min => 220C => 10C/min => 280C40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C45C => 3C/min => 175C => 15C/min => 300C (10min)40 0C (5 min) 2 0C/min -> 250 0C (15 min) 10 0C/min -> 270 0C45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min)
I 1455.1454.1447.1455.1447.
ReferenceDuschatzky, Almeida, et al., 2007Eason and Setzer, 2007Ferreira, Meireles de Sousa, et al., 2007Formisano, Rigano, et al., 2007Kamatou, Viljoen, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSCP Sil 8 CBHP-1CP Sil 8 CB
Column length (m)  30.30.30.50.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm)  0.250.250.20.32
Phase thickness (μm)  0.250.250.330.25
Program not specified40C(3min) => 8C/min => 160C => 15C/min => 300C (10min)50C(3min) => 3C/min => 100C => 2.7C/min => 140C => 2.4C/min => 180C => 6C/min => 250C60C(5min) => 3C/min => 180C => 20C/min => 280C(10min)60 0C (2 min) 5 0C/min -> 160 0C 5 0C/min -> 250 0C (10 min)
I 1443.1455.1453.1453.1455.
ReferenceLiolios, Laouer, et al., 2007Liu, Song, et al., 2007Meekijjaroenroj, Bessière, et al., 2007Merle, Verdeguer, et al., 2007Mockute, Bernotiene, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSHP-5MSDB-5DB-5MS
Column length (m) 30.30.30.50.30.
Carrier gas HeliumHeliumHeHelium 
Substrate      
Column diameter (mm) 0.250.250.250.32 
Phase thickness (μm) 0.250.250.250.25 
Program 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C40C(10min) => 3C/min => 200C => 2C/min => 220C60 0C (1 min) 5 0C/min -> 160 0C 10 0C/min -> 250 0Cnot specified
I 1453.1454.1454.1455.1464.
ReferenceMoriarity, Bansal, et al., 2007Moriarity, Bansal, et al., 2007Moronkola, Ogunwande, et al., 2007Nivinsliene, Butkiene, et al., 2007Polzin, Stanfill, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-SilCP-SilCP-SilCP Sil 8 CBHP-5
Column length (m) 30.30.30.50.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.250.250.250.250.25
Program 50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C50 0C (3 min) 3 0C/min -> 100 0C 2.7 0C/min -> 140 0C 2.4 0C/min -> 180 0C 6 0C/min -> 250 0C60 0C (2 min) 5 0C/min -> 160 0C (1 min) 10 0C/min -> 280 0C (3 min)not specified
I 1440.1458.1458.1455.1455.
ReferenceProffit, 2007Proffit, 2007Proffit, 2007Radusiene, Judzentiene, et al., 2007Ristic, Krivokuca-Dokic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-55 % Phenyl methylsiloxaneHP-5 MSDB-5
Column length (m) 30.30. 30.30.
Carrier gas HeHydrogen HeliumHelium
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (μm) 0.250.25  0.50
Program 45C => 3C/min => 175C => 15C/min => 300C(10min)35 0C 4 0C/min -> 180 0C 17 0C/min -> 280 0C (10 min)not specified40 0C (10 min) 3 oC/min -> 200 0C 2 0C/min -> 220 0C35 0C (6 min) 5 0C/min -> 50 0C 2 0C/min -> 70 0C 3 0C/min -> 150 0C 5 0C/min -> 200 0C
I 1447.1455.1489.1454.1453.
ReferenceRodrigues, Antunes, et al., 2007Santos, Santiago, et al., 2007Serrano, Cornu, et al., 2007Setzer, Stokes, et al., 2007Soares, Pereira, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSOV-1HP-5MSPolydimethyl siloxaneHP-5MS
Column length (m)  30.30. 30.
Carrier gas  HeliumHe He
Substrate      
Column diameter (mm)  0.250.25 0.25
Phase thickness (μm)  0.25  0.25
Program not specified40 0C (2 min) 6 0C/min -> 130 0C 10 0C/min -> 300 0C40C(10min) => 3C/min => 200C => 2C/min => 220Cnot specified40C(3min) => 6C/min => 160C => 10C/min => 300C (10min)
I 1453.1447.1454.1451.1420.
ReferenceStokes, Cole, et al., 2007Suschke, Sporer, et al., 2007Takaku, Haber, et al., 2007Werka, Boehme, et al., 2007Yu, Huang, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5Ultra-2HP-5MSHP-5MSHP-5
Column length (m) 30.25.30.30.30.
Carrier gas HeH2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.330.250.250.25
Program 35C => 4C/min => 180C => 10C/min => 250Cnot specified40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C50C(3min) => 3C/min => 150C(10min) => 10C/min => 250C60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C
I 1454.1454.1455.1486.1457.
ReferenceAlbuquerque, Canuto, et al., 2006Ceva-Antunes, Bizzo, et al., 2006Formisano C., Senatore F., et al., 2006Güllüce, Özer, et al., 2006Jordan, Martinez, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBHP-5 MSHP-5 MSHP-5 MSHP-5
Column length (m) 50.30.30.30.30.
Carrier gas HeHGeliumHGeliumHGeliumHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.32
Phase thickness (μm) 0.250.250.250.250.25
Program 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (5min)40 0C (3 min) 10 0C/min -> 108 0C 3 0C/min -> 188 0C 4 0C/min -> 280 0C (5 min)40 0C (3 min) 10 0C/min -> 108 0C 3 0C/min -> 188 0C 4 0C/min -> 280 0C (5 min)40 0C (3 min) 10 0C/min -> 108 0C 3 0C/min -> 188 0C 4 0C/min -> 280 0C (5 min)not specified
I 1455.1456.1457.1460.1457.
ReferenceJudzentiene and Buzelyte, 2006Kawaree, Phutdhawong, et al., 2006Kawaree, Phutdhawong, et al., 2006Kawaree, Phutdhawong, et al., 2006Kucuk, Gulec, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-1SE-52HP-5CP Sil 8 CB
Column length (m) 30.30.25.30.50.
Carrier gas HeHeH2 He
Substrate      
Column diameter (mm) 0.250.250.320.250.32
Phase thickness (μm) 0.25 0.420.250.25
Program 40C(1min) => 8C/min => 160C => 12C/min => 300C(5min)35C => 4C/min => 180C => 10C/min => 250C60C(8min) => 3C/min => 180C => 20C/min => 250C (10min)not specified60 0C (2 min) 5 0C/min -> 160 0C 10 0C/min -> 250 0C (5 min)
I 1454.1455.1449.1457.1454.
ReferenceLi, Deng, et al., 2006de Lima, Maia, et al., 2006Lorenzo, Loayza, et al., 2006Martinez, Madrid, et al., 2006Mockute, Bernotiene, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5HP-5 MSDB-5HP-5 MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas Helium HeHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.100.250.250.250.25
Program 40 0C (1 min) 10 0C/min -> 120 0C 0.5 0C/min -> 150 0C 20 0C/min -> 280 0C (5 min)40 0C (3 min) 2 0C/min -> 150 0C 20 0C/min -> 220 0C (5 min)35C => 4C/min => 180C => 10C/min => 250C40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C
I 1454.1453.1464.1453.1454.
ReferenceNavickiene, Morandim, et al., 2006Pyun and Shin, 2006Santos, Nunes, et al., 2006Schmidt, Noletto, et al., 2006Schmidt, Noletto, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5MSHP-5MSHP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.250.250.25
Program 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C60C => 1.5C/min => 185C(1min) => 9C/min => 275C(2min)60C(1min) => 1.5C => 185C => 9C/min => 275C (2min)60C => 2C/min => 100C => 3C/min => 160C => 5C/min => 280C
I 1453.1455.1456.1458.1453.
ReferenceSchmidt, Noletto, et al., 2006Senatore, Apostolides Arnold, et al., 2006Singh, Marimuthu, et al., 2006Singh G., Maurya S., et al., 2006Srivastava, Mallavarapu, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52DB-5MSDB-1DB-5MSDB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.150.250.250.250.25
Program 45C => 1C/min => 100C => 5C/min => 250C (10min)60C => 3C/min => 180C => 250C (2min)35C => 2C/min => 200C => 5C/min => 240C70C(2min) => 10C/min => 150C(15min) => 5C/min => 240C45C => 3C/min => 175C => 15C/min => 300C(10min)
I 1455.1450.1428.1439.1447.
ReferenceTognolini, Barocelli, et al., 2006Tuberoso, Barra, et al., 2006Al-Burtamani, Fatope, et al., 2005Bagci and Baser, 2005Belhattab, Larous, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBDB-5DB-1HP-5MSDB-5
Column length (m) 50.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)35C => 4C/min => 180C => 10C/min => 250C45C => 3C/min => 175C => 15C/min => 300C (10min)not specified40C(1min) => 9C/min => 130C => 2C/min => 230C
I 1455.1452.51447.1454.1454.
ReferenceButkienë, Nivinskienë, et al., 2005Cysne, Canuto, et al., 2005Faleio, Miguel, et al., 2005Grombone-Guaratini, Silva-Brandão, et al., 2005Hamm, Bleton, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BPX-5BPX-5CP Sil 8 CBPolydimethyl siloxane with 5 % Ph groupsCP Sil 8 CB
Column length (m) 30.30.50. 50.
Carrier gas  HeHe He
Substrate      
Column diameter (mm) 0.250.320.32 0.32
Phase thickness (μm) 0.250.50.25 0.25
Program 60C(0.2min) => 3K/min => 186C => 10C/min => 240C (5min)60C(1min) => 3.5C/min => 180C => 20C/min => 280C(2min)60C(1min) => 5C/min => 160C => 5C/min => 250C(3min)not specified60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (3min)
I 1454.1454.1454.1455.1454.
ReferenceJudzentiene and Mockute, 2005Koutsoudaki, Krsek, et al., 2005Nivinskienë, Butkienë, et al., 2005Pino, Marbot, et al., 2005Radudienë, Judpintienë, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5CP Sil 8 CB
Column length (m) 30.30.30.30.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.10.10.250.10.25
Program 35C => 4C/min => 180C => 10C/min => 250C35C => 4C/min => 180C => 10C/min => 250C35C => 4C/min => 180C => 10C/min => 280C35C => 4C/min => 180C => 20C/min => 280C50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)
I 1430.1431.1454.1454.1455.
ReferenceAlbuquerque, Silveira, et al., 2004Albuquerque, Souza, et al., 2004de Andrade, Bezerra, et al., 2004Barros-Filho, Nunes, et al., 2004Butkienë, Nivinskienë, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeOV-1DB-5CP Sil 8 CBCP Sil 8 CB
Column length (m)  30.30.50.50.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm)  0.250.250.320.32
Phase thickness (μm)  0.250.25 0.25
Program not specified45 0C (4 min) 3 0C/min -> 75 0C 4 0C/min -> 115 0C 6 0C/min -> 312 0C40C(1min) => 9C/min => 130C => 2C/min => 230C60C(2min) => 5C/min => 160C (1min) => 10C/min => 250C (2min)60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (5min)
I 1438.1443.1454.1454.1454.
ReferenceCouladis, Özcan, et al., 2004Hafez and Abdel-Salam, 2004Hamm, Bleton, et al., 2004Judpentienë and Mockutë, 2004Judpentienë and Mockutë, 2004, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1CP Sil 8 CBCP Sil 8 CBHP-5MS
Column length (m) 30.30.50.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (μm) 0.250.25 0.250.25
Program 60C(4min) => 6C/min => 240 => 10C/min => 280C45C => 3C/min => 175C => 15C/min => 300C (10min)50 0C (2 min) 3 0C/min -> 180 0C (1 min) 20 0C/min -> 250 0C (2 min)50C(2min) => 3C/min => 180C(1min) => 20C/min => 250C (2min)50C(3min) => 3C/min => 150C(10min) => 10C/min => 250C
I 1455.1447.1454.1454.1455.
ReferenceLetchamo, Ward, et al., 2004Miguel, Simões, et al., 2004Mockutë, Bernotienë, et al., 2004Mockutë, Judbentienë, et al., 2004Sahin, Gulluce, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-1DB-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas  HeliumHeliumHelium 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C35 0C 4 0C/min -> 180 0C 10 0C/min -> 250 0C35 0C 4 0C/min -> 180 0C 10 0C/min -> 250 0C35 0C 4 0C/min -> 180 0C 10 0C/min -> 250 0C60C(1min) => 1.5C/min => 185C(1min) => 9C/min => 275C(2min)
I 1455.1455.1445.1455.1458.
ReferenceSenatore, Apostolides Arnold, et al., 2004Silva, Matos, et al., 2004Silva, Matos, et al., 2004Silva, Matos, et al., 2004Singh, Marimuthu, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-5SE-30SE-30
Column length (m) 30.30.   
Carrier gas HeHe   
Substrate      
Column diameter (mm) 0.250.25   
Phase thickness (μm) 0.250.25   
Program 60C(4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C50C (3min) => 3C/min => 150C (10min) => 10C/min => 250Cnot specifiednot specifiednot specified
I 1457.1455.1454.1449.1448.
ReferenceSotomayor, Martínez, et al., 2004Tepe, Donmez, et al., 2004Vilaseca, Guy, et al., 2004Vinogradov, 2004Vinogradov, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1HP-5SE-54CP-Sil 8CB-MS
Column length (m) 30.30.30.25.50.
Carrier gas HeHeHeH2 
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (μm) 0.250.10.250.25 
Program 40C (1min) => 9C/min => 130C => 2C/min => 230C40C (2min) => 20C/min => 80C => 3C/min => 145C => 45C/min => 225C (3min)60C (4min) => 1C/min => 64C => 2.5C/min => 155C => 5C/min => 250C110C(2min) => 3C/min => 130C => 8.5C => 290C60C(1min) => 3C/min => 70C => 15C/min => 170C(8min) => 5C/min => 250C
I 1454.1421.81457.1457.1454.
ReferenceHamm, Lesellier, et al., 2003Helmig, Revermann, et al., 2003Jordán, Martínez, et al., 2003Lima, Veiga, et al., 2003Mockute, Bernotiene, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 8CB-MSCP Sil 8 CBCP Sil 8 CBDB-1DB-1
Column length (m) 50.50.50.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm)  0.250.250.10.1
Program 50C(2min) => 3C/min => 180C(1min) => 20C/min => 250C(2min)70C(5min) => 3C/min => 100C (1min) => 25C/min => 250C (10min)60C(1min) => 5C/min => 160C => 10C/min => 250C(5min)35C => 4C/min => 180C => 10C/min => 250C35C => 4C/min => 180C => 10C/min => 250C
I 1454.1454.1454.1449.1443.
ReferenceMockute, Bernotiene, et al., 2003, 2Mockute and Judzentiene, 2003Mockute, Nivinskiene, et al., 2003Silva, Matos, et al., 2003Bezerra, Andrade-Neto, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54CP Sil 8 CBCP Sil 8 CBDB-5DB-5MS
Column length (m)  50.50.30.30.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm)  0.320.320.250.32
Phase thickness (μm)    0.10.25
Program not specified60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (2min)60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C(2min)35C => 4C/min => 180C => 10C/min => 250Cnot specified
I 1436.1454.1454.1458.1450.
ReferenceKilic, 2002Mockute and Judzentiene, 2002Mockute and Judzentiene, 2002, 2Pessoa, Morais, et al., 2002Phutdhawong, Korth, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBHP-5MSHP-5DB-5DB-1
Column length (m)  30.30. 30.
Carrier gas  He   
Substrate      
Column diameter (mm)  0.250.25 0.25
Phase thickness (μm)  0.250.25 0.25
Program not specified40C (10min) => 3C/min => 120C => 10C/min => 250C (5min)not specifiednot specified45 0C 3 K/min -> 175 0C 15 K/min -> 300 0C (10 min)
I 1455.1458.1450.1437.1447.
ReferenceSchwob, Bessière, et al., 2002Ansorena, Gimeno, et al., 2001Aparicio, Romero, et al., 2001Ferreira, Costantin, et al., 2001Figueiredo, Miguel, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5HP-1DB-5
Column length (m)  30.30.12. 
Carrier gas  HeHeHe 
Substrate      
Column diameter (mm)  0.250.250.20 
Phase thickness (μm)  0.250.250.33 
Program not specified50 0C 3 K/min -> 200 0C 8 K/min -> 280 0C40C => 2C/min => 60C => 4C/min => 260C40 0C 6.7 0C/min -> 87 0C (9 min) 10 0C/min -> 187 0Cnot specified
I 1450.1446.1456.1443.1488.
ReferencePetrakis, Tsitsimpikou, et al., 2001Usubillaga, Aparicio, et al., 2001Andrade, Maia, et al., 2000Betts, 2000Dittmann and Nitz, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CBP-1BP-1DB-1HP-5MS
Column length (m) 30. 50.30.30.
Carrier gas H2  H2He
Substrate      
Column diameter (mm) 0.25 0.220.250.25
Phase thickness (μm) 0.25 0.250.250.25
Program 40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min)not specifiednot specified40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min)not specified
I 1447.1452.1453.1447.1462.
ReferenceDorman, Figueiredo, et al., 2000Juliani, Biurrun, et al., 2000Muselli, Bighelli, et al., 2000da Silva, Pedro, et al., 2000Bouwmeester, Wallaart, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SE-30DB-1CP Sil 5 CBCP Sil 5 CB
Column length (m) 30.30.30.25.25.
Carrier gas HeHeliumHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.390.39
Phase thickness (μm) 0.250.200.25  
Program 45C => 3C/min => 170C => 15C/min => 300C(10min)not specified45C => 3C/min => 175C => 15C/min => 300C(10min)not specifiednot specified
I 1447.1467.1447.1460.1447.
ReferencePedro, da Silva, et al., 1999Prikhod'ko, Klyuev, et al., 1999Santos, Figueiredo, et al., 1999Weyerstahl, Marschall, et al., 1999Weyerstahl, Marschall, et al., 1999, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBOV-1CP Sil 5 CBDB-5
Column length (m) 30.50.50.25.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.320.32 0.25
Phase thickness (μm) 0.251.20.25 0.25
Program 45C => 3C/min => 175C => 15C/min => 240C (10min)30C => 55C/min => 85C => 1C/min => 145C => 3C/min => 250C1)50C(1min) => 4C/min => 180C => 2C/min => 250C(10min) 2)50C(1min) => 6C/min => 200C => 12C/min => 250C(5min)not specified45C(5min) => 2C/min => 200C => 5C/min => 250C
I 1447.1463.1454.1459.1452.
ReferenceBaratta, Dorman, et al., 1998Guyot, Bouseta, et al., 1998Kökdil, 1998Phan, Van, et al., 1998Sanda, Koba, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBCP Sil 5 CBCP Sil 5 CBDB-5
Column length (m) 30.25.25.25.30.
Carrier gas H2N2N2N2He
Substrate      
Column diameter (mm) 0.25   0.25
Phase thickness (μm) 0.250.390.39 0.25
Program 45C => 3C/min => 175C => 15C => 240C(10min)not specifiednot specifiednot specified60C => 3C/min => 240C => 30C/min => 300C
I 1447.1454.1452.1453.1451.
Referenceda Silva, Figueiredo, et al., 1998Weyerstahl, Marschall, et al., 1998Weyerstahl, Marschall, et al., 1998, 2Weyerstahl, Marschall, et al., 1998, 3Yusuf, Begum, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-1SPB-SulfurCP Sil 5 CB
Column length (m) 15.30.30.30.25.
Carrier gas HeH2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.32 
Phase thickness (μm) 0.250.250.254. 
Program 40C(5min) => 5C/min => 120C(10min) => 4C/min => 250C(4min) => 5C/min => 280C45C => 3C/min => 175C => 15C/min => 240C(10min)45C => 3C/min => 175C => 15C/min => 280Cnot specifiednot specified
I 1463.1447.1447.1449.1454.
ReferenceAnitescu, Doneanu, et al., 1997Figueiredo, Barroso, et al., 1997Gaspar, Palma, et al., 1997Mariaca, Berger, et al., 1997Weyerstahl, Marschall, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1HP-1DB-1Methyl Silicone
Column length (m) 30.30.24.30. 
Carrier gas N2H2 Helium 
Substrate      
Column diameter (mm) 0.250.250.320.25 
Phase thickness (μm)  0.250.25  
Program not specified45 0C 3 0C/min -> 175 0C 15 0C/min -> 240 0C (10 min)60C(2min) => 4C/min => 120C => 2C/min => 220C (20min)35 0C 4 0C/min -> 180 0C 10 0C/min -> 250 0Cnot specified
I 1453.1447.1437.1439.1447.
ReferenceWeyerstahl, Marschall, et al., 1997, 2Barroso, Figueiredo, et al., 1996Dung, Thanh, et al., 1996de Morais, Craveiro, et al., 1996Zenkevich, 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30SE-30OV-101DB-1DB-1
Column length (m)    60.60.
Carrier gas     He
Substrate      
Column diameter (mm)    0.320.32
Phase thickness (μm)     0.25
Program not specifiednot specifiednot specifiednot specified-80 C (20 min; during thermal desorption) 50-200 C at 4 C/min 200-320 C at 10 C/min
I 1448.1448.1456.1448.1448.
ReferenceDavis and Essenberg, 1995Davis and Essenberg, 1995Menut, Lamaty, et al., 1994Binder and Flath, 1989Miller, Bills, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-1DB-1OV-101
Column length (m) 60.  
Carrier gas He  
Substrate    
Column diameter (mm) 0.32  
Phase thickness (μm) 0.25  
Program -80 C (20 min; during thermal desorption) 50-200 C at 4 C/min 200-320 C at 10 C/minnot specifiednot specified
I 1450.1487.1465.
ReferenceMiller, Bills, et al., 1989MacLeod and Snyder, 1988Shibamoto, 1987
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kurashov, Mitrukova, et al., 2014
Kurashov, E.A.; Mitrukova, G.G.; Krylova, Yu.V., Variations in the component composition of essential oil of Ceratophyllum demersum (Ceratophyllaceae) during vegetation (in press), Plant Resources (Rastitel'nye Resursy), 2014, 1, 000-000. [all data]

Rodriques, Amorim, et al., 2013
Rodriques, K.A. da.F.; Amorim, L.V.; de Oliveira, J.M.G.; Dias, C.N.; Moraes, D.F.C.; Andrade, E.H. deA.; Maia, J.G.S.; Carneiro, S.M.P.; Carvalho, F.A. deA., Eugenia uniflora L. essential oil as a potential anti-Leishmania agent: effect on Leishmania amazonensis and possible mechanism of action, Evidence-Based Complementary and Alternative Medicine, 2013, 2013, 1-10, https://doi.org/10.1155/2013/279726 . [all data]

Bendiabdellah, El Amine Dib, et al., 2012
Bendiabdellah, A.; El Amine Dib, M.; Djabou, N.; Allali, H.; Tabti, B.; Costa, J.; Myseli, A., Biological activities and volatile cinstituents of Daucus muricatus L. from Algeria, Chem. Centr. J., 2012, 6, 48, 1-22. [all data]

Dell'Agli, Sanna, et al., 2012
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Miller, R.L.; Bills, D.D.; Buttery, R.G., Volatile components from Barlett and Bradford pear leaves, J. Agric. Food Chem., 1989, 37, 6, 1476-1479, https://doi.org/10.1021/jf00090a005 . [all data]

MacLeod and Snyder, 1988
MacLeod, A.J.; Snyder, C.H., Volatile components of mango preserved by deep freezing, J. Agric. Food Chem., 1988, 36, 1, 137-139, https://doi.org/10.1021/jf00079a035 . [all data]

Shibamoto, 1987
Shibamoto, T., Retention Indices in Essential Oil Analysis in Capillary Gas Chromatography in Essential Oil Analysis, Sandra, P.; Bicchi, C., ed(s)., Hutchig Verlag, Heidelberg, New York, 1987, 259-274. [all data]


Notes

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