1H-Cycloprop[e]azulen-7-ol, decahydro-1,1,7-trimethyl-4-methylene-, [1ar-(1aα,4aα,7β,7aβ,7bα)]-


Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-WaxHP-InnowaxDB-WaxRTX-WaxHP-Innowax
Column length (m) 60.60.30.60.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.220.250.250.220.25
Phase thickness (μm) 0.250.250.250.250.52
Tstart (C) 60.60.40.60.35.
Tend (C) 230.220.230.230.205.
Heat rate (K/min) 2.5.4.2.3.
Initial hold (min)  1.2. 10.
Final hold (min) 5.5.4.530.10.
I 2091.2123.2138.2101.2144.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Feng, Cui, et al., 2011Zeng, Xie, et al., 2011Museli, Pau, et al., 2009Wannes, Mhamdi, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxRTX-WaxHP InnowaxPEG-20MHP-Innowax
Column length (m) 30.60.30.60.30.
Carrier gas NitrogenHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.220.320.250.25
Phase thickness (μm) 0.250.250.500.250.25
Tstart (C) 50.60.60.90.60.
Tend (C) 280.230.260.225.240.
Heat rate (K/min) 5.2.3.3.2.
Initial hold (min) 1.    
Final hold (min) 1.35. 15.20.
I 2125.2103.2128.2118.2108.
ReferenceBousaada, Ammar, et al., 2008Paolini, Tomi, et al., 2008Capetanos, Saroglou, et al., 2007Gil A., Van Baren C.M., et al., 2007Hachicha, Skanji, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBTC-FFAPCarbowax 20MDB-WaxSupelcowax-10
Column length (m) 30. 30.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.320.2
Phase thickness (μm) 0.250.250.250.250.2
Tstart (C) 40.60.60.70.70.
Tend (C) 220.220.230.220.220.
Heat rate (K/min) 3.3.3.4.3.
Initial hold (min) 1.    
Final hold (min) 2.30.  15.
I 2136.2130.2090.2133.2112.
ReferenceHymete, Rohloff, et al., 2007Kurose, Okamura, et al., 2007Limberger, Scopel, et al., 2007Pala-Paul, Brophy, et al., 2007Pinto, Salgueiro, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Supelcowax-10Supelcowax-10AT-WaxDB-Wax
Column length (m) 30.30.30.60.60.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.5
Tstart (C) 50.40.40.60.50.
Tend (C) 250.250.250.200.230.
Heat rate (K/min) 2.2.3.4.3.
Initial hold (min)   5. 2.
Final hold (min)  33.10.20.20.
I 2121.2125.2104.2150.2110.
ReferenceRaal, Orav, et al., 2007Sylvestre, Pichette, et al., 2007Vichi, Riu-Aumatell, et al., 2007Borges, Rojas, et al., 2006Cai, Lin, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10SupelcowaxNB-20MSupelcowax-10
Column length (m) 60.30.30.30.30.
Carrier gas N2 N2HeHe
Substrate      
Column diameter (mm) 0.250.250.320.20.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.40.50.50.50.
Tend (C) 230.210.200.250.220.
Heat rate (K/min) 2.2.5.2.4.
Initial hold (min) 2.2.  1.
Final hold (min) 20.33.  10.
I 2121.2124.2142.2126.2121.
ReferenceChoi, 2006Garneau F.X., Collin G., et al., 2006Martin, Joseph, et al., 2006Orav, Raal, et al., 2006Wong, Lim, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxDB-WaxHP-InnowaxCP-WaxDB-Wax
Column length (m) 50.30.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.320.25
Phase thickness (μm) 0.50.250.170.250.25
Tstart (C) 60.60.60.40.50.
Tend (C) 250.250.210.180.180.
Heat rate (K/min) 2.5.4.5.3.
Initial hold (min)   3.2. 
Final hold (min) 60.10.15. 40.
I 2093.2124.2153.2088.2120.
ReferenceBendimerad and Bendiab, 2005Fakhari A.R., Sonboli A., et al., 2005Ferretti, Maggi, et al., 2005Ka, Choi, et al., 2005Lee, Umano, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10Supelcowax-10DB-WaxSupelcowax-10
Column length (m) 60.30.30.60.30.
Carrier gas He  N2N2
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.40.40.70.40.
Tend (C) 220.210.220.230.230.
Heat rate (K/min) 3.2.3.2.2.
Initial hold (min)  2.5.2. 
Final hold (min)  33.10.20. 
I 2133.2115.2104.2121.2110.
ReferencePalá-Paúl, Pérez-Alonso, et al., 2005Stevanovic, Garneau, et al., 2005Vichi, Riu-Aumatell, et al., 2005Choi, 2004González, Guerra, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10Innowax FSCBP-20DB-Wax
Column length (m) 60.30.60.25.60.
Carrier gas He HeliumN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm)  0.25 0.250.25
Tstart (C) 60.40.60.60.35.
Tend (C) 220.210.220.220.220.
Heat rate (K/min) 2.2.4.5.3.
Initial hold (min) 4.2.10.  
Final hold (min)  33.   
I 2121.2123.2144.2101.2132.
ReferenceJiang and Kubota, 2004Lopez Arze, Collin, et al., 2004Lourens, Reddy, et al., 2004Mallavarapu, Kulkarni, et al., 2004Palá-Paúl, Brophy, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxSW-10DB-WaxDB-WaxBP-20
Column length (m) 50.50.60.60.25.
Carrier gas HeHe NitrogenH2
Substrate      
Column diameter (mm) 0.20.200.250.250.33
Phase thickness (μm) 0.20.250.250.250.5
Tstart (C) 70.50.70.70.80.
Tend (C) 220.230.230.230.220.
Heat rate (K/min) 4.2.2.2.5.
Initial hold (min)   2.2. 
Final hold (min)   20.  
I 2127.2104.2133.2133.2136.
ReferencePalá-Paúl, García-Jiménez, et al., 2004Raal, Paaver, et al., 2004Sawamura, Son, et al., 2004Sawamura, Sou, et al., 2004Dunlop, Bignell, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TC-WaxDB-WaxCarbowax 20MSW-10Supelcowax-10
Column length (m) 60.60.50.50.30.
Carrier gas  HeliumN2HeN2
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (μm)   0.250.250.25
Tstart (C) 80.70.90.50.40.
Tend (C) 240.210.220.250.230.
Heat rate (K/min) 3.2.3.2.2.
Initial hold (min)      
Final hold (min)  60.   
I 2110.2125.2126.2100.2110.
ReferenceMiyazawa, Yamafuji, et al., 2003Mookdasanit, Tamura, et al., 2003Priestap, van Baren, et al., 2003Raal, Arak, et al., 2003Rotman, Ahumada, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxInnowaxCarbowax 20MHP-WaxDB-Wax
Column length (m) 50.60.25.50.60.
Carrier gas  HeN2N2He
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.2 0.250.250.25
Tstart (C) 50.60.50.75.45.
Tend (C) 220.220.250.220.240.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min) 5.10. 4. 
Final hold (min)  10.10.  
I 2150.2144.2140.2127.2121.
ReferenceStashenko, Jaramillo, et al., 2003Suleimenov, Atazharova, et al., 2003Zrira, Elamrani, et al., 2003Priestap, van Baren, et al., 2002Christoph, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PEG-20MCP-Wax 52CBBP-20BP-20HP Innowax FSP
Column length (m) 50.50.25.25.60.
Carrier gas HeHeNitrogen He
Substrate      
Column diameter (mm) 0.20.300.500.330.25
Phase thickness (μm)  0.250.250.50.25
Tstart (C) 70.40.60.80.60.
Tend (C) 250.220.200.220.220.
Heat rate (K/min) 2.3.5.5. 
Initial hold (min)  5.  10.
Final hold (min)     10.
I 2100.2097.2098.2136.2144.
ReferenceOrav, Kailas, et al., 2001Chagonda, Makanda, et al., 2000Mallavarapu, Rao, et al., 2000Dunlop, Bignell, et al., 1999Kaya, Baser, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxHP-InnowaxHP-InnowaxHP-InnowaxSupelcowax-10
Column length (m) 60.60.60.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.60.60.60.60.
Tend (C) 220.220.220.220.240.
Heat rate (K/min)     4.
Initial hold (min) 10.10.10.10. 
Final hold (min)      
I 2144.2144.2144.2144.2110.
ReferenceKaya, Baser, et al., 1999, 2Kaya, Baser, et al., 1999, 3Kaya, Baser, et al., 1999, 3Kaya, Baser, et al., 1999, 3Labuckas, Zygadlo, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxBP-20Supelcowax-10DB-Wax
Column length (m) 60.60.25.30.30.
Carrier gas HeN2H2HeN2
Substrate      
Column diameter (mm) 0.25 0.330.250.25
Phase thickness (μm) 0.250.250.5 0.25
Tstart (C) 60.60.80.60.45.
Tend (C) 240.220.220.240.220.
Heat rate (K/min) 4.5.5.4.3.
Initial hold (min)      
Final hold (min)      
I 2129.2147.2136.2149.2128.
ReferenceNgassoum, Yonkeu, et al., 1999Weyerstahl, Marschall, et al., 1999Bignell, Dunlop, et al., 1998Lamarque, Maestri, et al., 1998Molleken U., Sinnwell V., et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCDB-WaxHP-Innowax FSCBP-20BP-20
Column length (m) 60.30.60.25.25.
Carrier gas HeHeHeH2H2
Substrate      
Column diameter (mm) 0.250.320.250.330.33
Phase thickness (μm) 0.25  0.50.5
Tstart (C) 60.60.60.80.80.
Tend (C) 220.250.240.220.220.
Heat rate (K/min) 4.3.4.5.5.
Initial hold (min) 10. 10.  
Final hold (min) 10. 10.  
I 2144.2151.2144.2136.2136.
ReferenceTümen, Baser, et al., 1998Abreu and Noronha, 1997Baser, Kirimer, et al., 1997Bignell, Dunlop, et al., 1997Bignell, Dunlop, et al., 1997, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20BP-20BP-20BP-20Supelcowax-10
Column length (m) 25.25.25.25.30.
Carrier gas H2H2 H2 
Substrate      
Column diameter (mm) 0.330.330.330.330.25
Phase thickness (μm) 0.50.50.50.5 
Tstart (C) 80.80.80.80.60.
Tend (C) 220.220.220.220.240.
Heat rate (K/min) 5.5.5.5.4.
Initial hold (min)      
Final hold (min)      
I 2136.2136.2136.2136.2118.
ReferenceBignell, Dunlop, et al., 1997, 3Bignell, Dunlop, et al., 1997, 4Bignell, Dunlop, et al., 1997, 5Bignell, Dunlop, et al., 1997, 6Zunino, Novillo-Newton, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10SP-1000Supelcowax-10Carbowax 20MDB-Wax
Column length (m) 0.85.60.45.30.
Carrier gas HeHeHeHydrogen 
Substrate      
Column diameter (mm) 0.250.500.250.320.32
Phase thickness (μm)   0.251.0 
Tstart (C) 40.65.40.60.70.
Tend (C) 240.225.200.200.200.
Heat rate (K/min) 3.3.3.2.4.
Initial hold (min)   3.5.2.
Final hold (min)   30.  
I 2149.2136.2149.2103.2145.
ReferenceZygadlo, Ariza-Espinar, et al., 1997Brophy, Goldsack, et al., 1996Wong and Lai, 1996Kollmannsberger, Nitz, et al., 1992Wyllie, Brophy, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase FFAP
Column length (m) 50.
Carrier gas  
Substrate  
Column diameter (mm)  
Phase thickness (μm)  
Tstart (C) 50.
Tend (C) 180.
Heat rate (K/min) 10.
Initial hold (min) 1.
Final hold (min)  
I 2152.
ReferenceBrophy, Davies, et al., 1989
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Notes

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