1H-Cycloprop[e]azulen-7-ol, decahydro-1,1,7-trimethyl-4-methylene-, [1ar-(1aα,4aα,7β,7aβ,7bα)]-


Normal alkane RI, polar column, custom temperature program

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Innowax FSCInnowax FSCHP-InnowaxHP InnowaxInnowax
Column length (m) 60.60.60.30.60.
Carrier gas HeliumHeliumHeliumNitrogen 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.33
Program 60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 oC/min -> 240 0C60 0C (10 min) 4 0C/min -> 220 0C 1 0C/min -> 240 0Cnot specified35 0C (10 min) 3 0C/min -> 205 0C 10 0C/min -> 225 0Cnot specified
I 2144.2144.2144.2125.2150.
ReferenceAkin, Saracoglu, et al., 2012Bardakci, Demirci, et al., 2012Feng, Cui, et al., 2011Laribi, Kouki, et al., 2011Noorizadeh, Farmany, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxHP InnowaxInnowax FSCInnowax FSCHP Innowax
Column length (m) 30.60.60.60.50.
Carrier gas Helium HeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.20
Phase thickness (μm) 0.250.330.250.250.25
Program not specifiednot specified60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C40 0C (5 min) 2 0C/min -> 270 0C -> 260 0C (20 min)
I 2135.2150.2144.2144.2150.
ReferenceZeng, Xie, et al., 2011Noorizadeh and Farmany, 2010Polatoglu, Demirci, et al., 2010Baser, Demirci, et al., 2009Mancini, Arnold, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP Innowax FSPHP-20MInnowaxHP-InnowaxInnowax FSC
Column length (m) 60.25.30.50.60.
Carrier gas HeliumHeliumHeliumHeNitrogen
Substrate      
Column diameter (mm) 0.250.200.250.20.25
Phase thickness (μm) 0.250.200.250.20.25
Program 60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C (20 min)30 0C (1 min) 50 0C/min -> 110 0C 1.5 0C/min -> 145 0C 4 0C/min -> 220 0C (10 min)not specified40C(5min) => 2C/min => 250C(15min) => 10C/min => 270C60 0C (10 min) 1 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C
I 2144.2129.2136.2150.2144.
ReferenceWedge, Klun, et al., 2009Zellner, Amorim, et al., 2009Aicha, Ines, et al., 2008Formisano, Mignola, et al., 2007Kaya, Benirci, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MDB-WaxHP-Innowax FSCInnowax FSCHP Innowax FSP
Column length (m) 30.60.60.60.60.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Program 60C(5min) => 3C/min => 180C => 20C/min => 280C(10min)40C(3min) => 2C/min => 150C => 4C/min => 200C (20min)60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 2111.2136.2144.2144.2144.
ReferenceMerle, Verdeguer, et al., 2007Seo, Kim, et al., 2007Tabanca N., Demirci B., et al., 2007Tabanca, Demirci, et al., 2007Tabanca N., Demirci B., et al., 2007, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Innowax FSCInnowax FSCInnowax FSCHP-Innowax FSCInnowax FSC
Column length (m) 60.60.60.60.60.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min >220C (10min) => 1C/min => 240C60C(10min) => 4C/min >220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 2144.2144.2144.2144.2144.
ReferenceBaser K.H.C., Ozek G., et al., 2006Baser, Özek, et al., 2006Baser, Özek, et al., 2006Demirci B., Baser K.H.C., et al., 2006Iscan, Kirimer, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCHP-InnowaxHP-Innowax FSCHP-Innowax FSCHP-Innowax FSC
Column length (m) 60.50.60.60.60.
Carrier gas HeHeHe N2
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (μm) 0.250.20.250.250.25
Program 60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C40C(5min) => 2C/min => 250C (15min) => 10C/min => 270C60(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C => (10min) => 1C/min => 240C
I 2144.2150.2144.2144.2144.
ReferenceKürkçüoglu, Hüsnü Can Baser, et al., 2006Senatore, Apostolides Arnold, et al., 2006Suleimenov Y.M., Atazhanova G.A., et al., 2006Tabanca, Demirci, et al., 2006Tabanca, Demirci, et al., 2006, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxHP-Innowax FSCDB-WaxHP-Innowax FSCHP-Innowax FSC
Column length (m) 60.60. 60.60.
Carrier gas N2N2N2HeHe
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (μm) 0.250.25 0.250.25
Program 60C(10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C (10min) => 1C/min => 240Cnot specified60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 2144.2144.2133.2144.2144.
ReferenceDemirci, Demirci, et al., 2005Demirci, Demirci, et al., 2005, 2Pala-Paul, Perez-Alonso, et al., 2005Tabanca, Demirci, et al., 2005Viljoen, Subramoney, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP Innowax FSPHP-Innowax FSCHP-Innowax FSCHP-Innowax FSCHP-Innowax
Column length (m) 60.60.60.60.50.
Carrier gas N2HeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (μm) 0.250.250.250.250.2
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240Cnot specified
I 2144.2144.2144.2144.2150.
ReferenceAltintas, Kose, et al., 2004Demirci, Paper, et al., 2004Kivcak, Akay, et al., 2004Kivcak, Akay, et al., 2004Senatore, Apostolides Arnold, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MHP Innowax FSPHP-Innowax FSCHP-Innowax FSCHP-Innowax FSC
Column length (m)  60.60.60.60.
Carrier gas  HeHeN2He
Substrate      
Column diameter (mm)  0.250.250.250.25
Phase thickness (μm)  0.250.250.250.25
Program not specified60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C (10min) => 4C/min => 220C (10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C(40min)
I 2144.2144.2144.2144.2144.
ReferenceVinogradov, 2004Baser, Demirci, et al., 2003Demirci, Baser, et al., 2003Kaya, Demirci, et al., 2003Kürkcüoglu, Demirci, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxHP-InnowaxInnowax FSCInnowaxHP-Innowax
Column length (m) 60.60.60.60.60.
Carrier gas  HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C
I 2144.2144.2144.2144.2144.
ReferenceViljoen, van Vuuren, et al., 2003Baser, Demirci, et al., 2002Baser, Demirei, et al., 2002Baser, Nuriddinov, et al., 2002Demirci, Baser, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCHP-InnowaxHP-InnowaxHP-InnowaxHP-Innowax FSC
Column length (m) 60.30.60.60.60.
Carrier gas N2H2HeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.250.50.250.250.25
Program 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C40C (8min) => 3C/min => 180C => 20C/min => 240C60 0C (10 min) 10 K/min -> 220 0C (10 min) 1K/min -> 240 0C60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 2144.2147.2144.2144.2144.
ReferenceHüsnü Can Baser, Demirci, et al., 2002Paroul, Rota, et al., 2002Baser, Demirci, et al., 2001Gören, Demirci, et al., 2001Kirimer N., Tabanea N., et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxInnowax FSCHP-Innowax FSCHP-WaxInnowax
Column length (m) 60.60.60.60.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.25 
Program 60C(10min) => 4C/min => 200C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C50 0C 3 K/min -> 200 0C 8 K/min -> 280 0C60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C
I 2144.2144.2144.2155.2144.
ReferenceÖzcan, Akgül, et al., 2001Tabanca N., Demirci F., et al., 2001Tabanca, Kirimer, et al., 2001Usubillaga, Aparicio, et al., 2001Ahmed, Choudhary, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxInnowax FSCSupelcowax-10Innowax FSCInnowax
Column length (m) 60.60. 60.60.
Carrier gas HeHe Helium 
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (μm) 0.250.25 0.250.25
Program 60 0C (10 min) 4 K/min -> 220 0C (10 min) 1 K/min -> 240 0C60C(10 min) => 4C/min => 220C(10min) => 1C/min => 240Cnot specified60 0C (10 min) 4 0C/min -> 220 0C (10 min) 1 0C/min -> 240 0C60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C
I 2144.2144.2110.2144.2144.
ReferenceBaser, Özek, et al., 2000Kirimer, Tabanca, et al., 2000Zunino, Lopez, et al., 2000Kirimer, Tabanca, et al., 1999Baser, Kürkcüoglu, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase FFAPDB-WaxNB-351NB-351
Column length (m) 25.60.25.25.
Carrier gas H2N2 He
Substrate     
Column diameter (mm) 0.2 0.320.32
Phase thickness (μm) 0.330.250.20.2
Program 40C(5min) => 4C/min => 170C => 8C/min => 240C (12min)not specified40C(5min) => 4C/min => 170C => 8C/min => 240C (12min)35C(5min) => 2.5C/min => 150C => 5C/min => 240C (20min)
I 2125.2142.2137.2132.
ReferenceReddy, Angers, et al., 1998Weyerstahl, Marschall, et al., 1998Kerrola, Galambosi, et al., 1994Kerrola and Kallio, 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Akin, Saracoglu, et al., 2012
Akin, M.; Saracoglu, H.T.; Demirci, B.; Baser, K.H.C., Chemical composition and antibacterial activity of essential oils from different parts of Buplerum rotundifolium L., Rec. Nat. Prod., 2012, 6, 3, 316-320. [all data]

Bardakci, Demirci, et al., 2012
Bardakci, H.; Demirci, B.; Yesilada, E.; Kirmizibekmez, H.; Naser, K.H.C., Chemical composition of the essential oil of the subterranean parts of Valeriana alliariifolia, Rec. Nat. Prod., 2012, 6, 1, 89-92. [all data]

Feng, Cui, et al., 2011
Feng, T.; Cui, J.-J.; Xiao, Z.-B.; Tian, H.-X.; Yi, F.-P.; Ma, X., Chemical composition od essential oil from the peel of Chinese Torreya grandis Frt, Org. Chem. International, 2011, 2011, 1-5, https://doi.org/10.1155/2011/187372 . [all data]

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Laribi, B.; Kouki, K.; Sahli, A.; Mougou, A.; Marzouk, B., Essential oil fatty acids composition of a Tunisian caraway (Carum carvi L.) seed ecotype cultivated under water deficit, Adv. Environ. Biol., 2011, 1-15, retrieved from http://www.thefreelibrary.com//print/PrintArticle.aspx?id=253057768. [all data]

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Noorizadeh, H.; Farmany, A.; Noorizadeh, M., Quantitative structure-retention relationships analysis of retention index of essential oils, Quim. Nova, 2011, 34, 2, 242-249, https://doi.org/10.1590/S0100-40422011000200014 . [all data]

Zeng, Xie, et al., 2011
Zeng, Z.; Xie, R.; Zhang, T.; Zhang, H.; Chen, J.Y., Analysis of volatile compositions of Magnolia biondii Pamp by steam distillation and Headspace solid phase micro-extraction, J. Oleo Sci., 2011, 60, 12, 591-596, https://doi.org/10.5650/jos.60.591 . [all data]

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Noorizadeh, H.; Farmany, A., Exploration of linear and nonlinear modeling techniques to predict of retention index of essential oils, J. Chin. Chem. Soc., 2010, 1268-1277. [all data]

Polatoglu, Demirci, et al., 2010
Polatoglu, K.; Demirci, F.; Demirci, B.; Goren, N.; Baser, K.H.C., Antimicrobial activity and essential oil composition of a new T. argyrophyllum (C. Koch) Tvzel var. argyrophyllium chemotype, J. Oleo Sci., 2010, 59, 6, 307-313, https://doi.org/10.5650/jos.59.307 . [all data]

Baser, Demirci, et al., 2009
Baser, K.H.C.; Demirci, B.; Kurkcuoglu, M.; Satin, F.; Tumen, G., Comparative morphological and phytochemical charactertization of Salvia cadmica and S. smyrnaea, Pak. J. Bot., 2009, 41, 4, 1545-1555. [all data]

Mancini, Arnold, et al., 2009
Mancini, E.; Arnold, N.A.; De Martino, L.; De Feo, V.; Formisano, C.; Rigano, D.; Senatore, F., Chemical composition and phytotoxic effects of essential oils of Salvia hierosolymitana Boiss. and Salvia multicaulis Vahl. var. simplicifolia Boiss. growing wild in Lebanon, Molecules, 2009, 14, 11, 4725-4736, https://doi.org/10.3390/molecules14114725 . [all data]

Wedge, Klun, et al., 2009
Wedge, D.E.; Klun, J.A.; Tabanca, N.; Demirci, B.; Ozek, T.; Baser, K.H.C.; Liu, Z.; Zhang, S.; Cantrell, C.L.; Zhang, J., Bioactivity-guided fractionation and GC/MS fingerprinting of Amgelica sinensis and Angelica archangelica root components for antifungal and mosquito deterrent activity, J. Agric. Food Chem., 2009, 57, 2, 464-470, https://doi.org/10.1021/jf802820d . [all data]

Zellner, Amorim, et al., 2009
Zellner, B.D.; Amorim, A.C.L.; de Miranda A.L.P.; Alves, R.J.V.; Barbosa, J.P.; da Costa, G.L.; Rezende, C.M., Screening of the odor-activity and bioactiovity of the essential oils of leaves and flowers of Hyptis Passerina Mart. from the Brazilian Cerrado, J. Braz. Chem. Soc., 2009, 20, 2, 322-332, https://doi.org/10.1590/S0103-50532009000200018 . [all data]

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Formisano, Mignola, et al., 2007
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Kaya, Benirci, et al., 2007
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Merle, Verdeguer, et al., 2007
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Seo, Kim, et al., 2007
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Tabanca N., Demirci B., et al., 2007, 2
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Baser K.H.C., Ozek G., et al., 2006
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Iscan, Kirimer, et al., 2006
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Senatore, Apostolides Arnold, et al., 2006
Senatore, F.; Apostolides Arnold, N.; Piozzi, F.; Formisano, C., Chemical composition of the essential oil of Salvia microstegia Boiss. et Balansa growing wild in Lebanon, J. Chromatogr. A, 2006, 1108, 2, 276-278, https://doi.org/10.1016/j.chroma.2006.01.066 . [all data]

Suleimenov Y.M., Atazhanova G.A., et al., 2006
Suleimenov Y.M.; Atazhanova G.A.; Ozek T.; Demirci B.; Kulyyasov A.T.; Adekenov S.M.; Baser K.H.C., Essential oil composition of three species of Achillea from Kazakhstan, Chem. Nat. Compd. (Engl. Transl.), 2006, 37, 5, 447-450, https://doi.org/10.1023/A:1014471326724 . [all data]

Tabanca, Demirci, et al., 2006
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Notes

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