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1H-Cycloprop[e]azulen-7-ol, decahydro-1,1,7-trimethyl-4-methylene-, [1ar-(1a«alpha»,4a«alpha»,7«beta»,7a«beta»,7b«alpha»)]-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1CP-Sil PONA GBHP-5DB-5
Column length (m) 50.50.100.25.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.140.60.60.
Tend (C) 220.220.230.240.240.
Heat rate (K/min) 2.2.5.4.3.
Initial hold (min)   10.2. 
Final hold (min) 20.20.25.  
I 1569.1564.1603.1578.1577.
ReferenceBoti, Koukoua, et al., 2007Castilho, Liu, et al., 2007Cunicao, Lopes, et al., 2007Dehghan, Solaimanian, et al., 2007Flamini, Cioni, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSBP-1DB-5DB-5
Column length (m) 30.30.50.30.30.
Carrier gas N2HeHeHe 
Substrate      
Column diameter (mm) 0.250.250.220.250.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 220.280.220.240.240.
Heat rate (K/min) 5.3.2.3.3.
Initial hold (min) 10.   2.
Final hold (min)   20.  
I 1577.1578.1564.1577.1576.
ReferenceFlamini, Tebano, et al., 2007Kundakovic, Fokialakis, et al., 2007Lesueur, de Rocca Serra, et al., 2007Maccioni, Baldini, et al., 2007Martins, Santos, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeRTX-1RTX-1SPB-1HP-5MS
Column length (m) 30.60.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.220.220.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 80.60.60.50.60.
Tend (C) 220.230.230.250.280.
Heat rate (K/min) 2.2.2.5.4.
Initial hold (min)    3.5.
Final hold (min) 15.35.35.15. 
I 1574.1563.1565.1566.1577.
ReferenceMelo, Corrêa, et al., 2007Paolini J., Costa J., et al., 2007Paolini, Muselli, et al., 2007Radulovic, Lazarevic, et al., 2007Radulovic, Lazarevic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSDB-5ZB-5
Column length (m) 25.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.55.50.
Tend (C) 200.260.280.240.250.
Heat rate (K/min) 2.5.4.3.3.
Initial hold (min)   5.2. 
Final hold (min) 60.  15. 
I 1583.1594.1577.1575.1577.
ReferenceRout, Rao, et al., 2007Sabulal, Dan, et al., 2007Saroglou, Marin, et al., 2007Silva, Barbosa, et al., 2007Simoniatto, Bonani, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-5CP Sil 5 CBDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.50.60.
Tend (C) 240.280.250.200.240.
Heat rate (K/min) 3.3.3.5.3.
Initial hold (min)     2.
Final hold (min)   10.  
I 1576.1574.1575.1570.1576.
ReferenceTelascrea, de Araujo, et al., 2007Vagionas, Ngassapa, et al., 2007Yu, Liao, et al., 2007Andrianoelisoa H.S., Menut C., et al., 2006Batista-Pereira, Fernandes, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-5DB-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2N2N2
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.280.240.240.220.
Heat rate (K/min) 3.3.3.3.5.
Initial hold (min) 2. 3.3.10.
Final hold (min)   5.3. 
I 1576.1571.1575.1576.1578.
ReferenceBatista-Pereira, Fernandes, et al., 2006Chorianopoulos N., Evergets E., et al., 2006Dob, Dahmane, et al., 2006Dob, Dahmane, et al., 2006, 2Flamini, Tebano, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-5HP-5DB-1HP-5
Column length (m) 50.30.30.30.30.
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.50.60.
Tend (C) 220.260.250.220.250.
Heat rate (K/min) 2.3.3.4.10.
Initial hold (min)     2.
Final hold (min) 20.   10.
I 1568.1580.1576.1577.1590.
ReferenceGonny, Cavaleiro, et al., 2006Javidnia, Miri, et al., 2006Javidnia, Miri, et al., 2006, 2Kuiate, Bessière, et al., 2006Liu J.M., Nan P., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-5SPB-1SPB-1
Column length (m) 50.30.30.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.320.20.25
Phase thickness (mum) 0.320.250.250.20.25
Tstart (C) 60.60.60.70.50.
Tend (C) 220.280.280.220.250.
Heat rate (K/min) 5.3.3.3.5.
Initial hold (min) 3.   3.
Final hold (min) 5.  15.15.
I 1576.1548.1564.1553.1571.
ReferenceMasoudi, Esmaeili, et al., 2006Pavlovic, Kovacevic, et al., 2006Pavlovic, Tzakou, et al., 2006Pinto, Pina-Vaz, et al., 2006Radulovic, Mananjarasoa, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5HP-5MSHP-5MS
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.60.
Tend (C) 265.240.240.280.300.
Heat rate (K/min) 2.54.4.4.3.
Initial hold (min)    5. 
Final hold (min)      
I 1552.1583.1578.1575.1573.
ReferenceRamezani, Behravan, et al., 2006Rezazadeh, Hamedani, et al., 2006Rezazadeh, Hamedani, et al., 2006Saroglou, Dorizas, et al., 2006Silva-Brandão, Solferini, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSHP-5SPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.50.50.40.50.
Tend (C) 250.250.285.300.250.
Heat rate (K/min) 5.5.4.34.5.
Initial hold (min) 2.2. 5.3.
Final hold (min)     15.
I 1578.1578.1581.1575.1564.
ReferenceSu, Ho, et al., 2006Su, Ho, et al., 2006, 2Vujisic L., Vuckovic I., et al., 2006Vundac, Pfeifhofer, et al., 2006Boskovic, Radulovic, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-54HP-5DB-1DB-1
Column length (m) 30.50.30.30.30.
Carrier gas HeH2N2N2 
Substrate      
Column diameter (mm) 0.20.250.250.320.32
Phase thickness (mum) 0.250.270.250.250.25
Tstart (C) 50.50.60.50.50.
Tend (C) 250.300.220.260.250.
Heat rate (K/min) 5.5.5.2.2.
Initial hold (min) 3. 10.3.8.
Final hold (min) 15.  5. 
I 1575.1582.1578.1576.1541.
ReferenceBoskovic, Radulovic, et al., 2005Brantner, Pfeifhofer, et al., 2005Celik, Gokturk, et al., 2005Dob T., Berramdane T., et al., 2005Dob, Dahmane, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase MDN-5DB-1DB-1HP-5DB-1
Column length (m) 30.30.30.30.25.
Carrier gas HeHeHeN2 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.40.40.60.60.
Tend (C) 250.250.260.220.180.
Heat rate (K/min) 3.3.2.5.3.
Initial hold (min)   5.10.10.
Final hold (min)  20.20. 10.
I 1624.1561.1564.1577.1575.
ReferenceDugo, Mondello, et al., 2005Fanciullino, Gancel, et al., 2005de Feo, Urrunaga Soria, et al., 2005Flamini, Luigi Cioni, et al., 2005bin Jantan, Yalvema, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-1DB-5DB-5MSSE-54
Column length (m) 30.60.30.60.25.
Carrier gas HeHeHeHeH2
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (mum) 0.250.250.250.250.2
Tstart (C) 60.60.40.40.50.
Tend (C) 260.230.260.200.250.
Heat rate (K/min) 3.2.2.2.4.
Initial hold (min)   5.  
Final hold (min)  35.20.20. 
I 1579.1563.1576.1581.1579.
ReferenceJavidnia, Miri, et al., 2005Paolini, Costa, et al., 2005Senatore, Napolitano, et al., 2005Seo and Baek, 2005Simionatto, Porto, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1BP-1HP-5MSSPB-1HP-5
Column length (m) 30.50.30.30.30.
Carrier gas N2HeHeHeN2
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.70.60.
Tend (C) 200.230.280.220.220.
Heat rate (K/min) 5.2.3.3.5.
Initial hold (min)     10.
Final hold (min)  35. 15. 
I 1571.1565.1574.1552.1578.
ReferenceTchoumbougnang, Zollo, et al., 2005Vellutini, Baldovini, et al., 2005Aligiannis, Kalpoutzakis, et al., 2004Antunes, Sevinate-Pinto, et al., 2004Bertoli, Menichini, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-1HP-5HP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2He HeN2
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.250.20.250.250.25
Tstart (C) 60.70.60.60.60.
Tend (C) 220.220.220.280.240.
Heat rate (K/min) 5.3.5.3.3.
Initial hold (min) 10. 10.  
Final hold (min)  15.   
I 1578.1551.1575.1571.1577.
ReferenceBertoli, Pistelli, et al., 2004Cavaleiro, Salgueiro, et al., 2004Ceccarini, Macchia, et al., 2004Chorianopoulos, Kalpoutzakis, et al., 2004Flamini, Cioni, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-5HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 60.60.40.60.60.
Tend (C) 220.280.250.260.260.
Heat rate (K/min) 5.4.3.3.3.
Initial hold (min) 10.5.   
Final hold (min)      
I 1578.1577.1575.1580.1579.
ReferenceFlamini, Luigi Cioni, et al., 2004Grujic-Jovanovic, Skaltsa, et al., 2004Isidorov, Krajewska, et al., 2004Javidnia, Miri, et al., 2004Javidnia, Miri, et al., 2004, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1SPB-5HP-5MSHP-5HP-5MS
Column length (m) 30.30.30.25.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.20.25
Phase thickness (mum) 0.20.250.250.330.25
Tstart (C) 70.60.50.60.60.
Tend (C) 220.250.250.240.280.
Heat rate (K/min) 3.4.3.3.3.
Initial hold (min)  2.   
Final hold (min) 15.20. 7. 
I 1552.1576.1580.1580.1557.
ReferenceMoldão-Martins, Beirão-da-Costa, et al., 2004Pino, Marbot, et al., 2004Salido, Valenzuela, et al., 2004Sartoratto, Machado, et al., 2004Tzakou, Vagias, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima 5DB-5MSDB-5BPX-5DB-5
Column length (m) 25.30.25.30.30.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.75.75.60.
Tend (C) 280.200.210.210.240.
Heat rate (K/min) 3.4.3.3.3.
Initial hold (min)  5.10.10. 
Final hold (min) 20.20.1.1.30.
I 1563.1584.1580.1578.1577.
ReferenceVérité, Nacer, et al., 2004Yu, Kim, et al., 2004bin Ahmad and bin Jantan, 2003bin Ahmad and bin Jantan, 2003, 2Bader, Caponi, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1HP-5HP-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeN2N2N2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.60.
Tend (C) 240.200.220.220.220.
Heat rate (K/min) 3.5.5.5.5.
Initial hold (min)   10.10.10.
Final hold (min)  0.   
I 1578.1574.1577.1577.1578.
ReferenceBader, Flamini, et al., 2003Boyom, Assembe, et al., 2003Dural, Bagci, et al., 2003Ertugrul, Dural, et al., 2003Flamini, Luigi Cioni, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5DB-5DB-5HP-5
Column length (m) 30.30.30.25.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.25 0.25 0.25
Tstart (C) 40.25.75.60.60.
Tend (C) 250.150.230.260.280.
Heat rate (K/min) 3.3.3.4.4.
Initial hold (min)  5.10. 5.
Final hold (min) 20. 20.  
I 1560.1577.1572.1578.1576.
ReferenceGancel, Ollitrault, et al., 2003Isidorov, Vinogorova, et al., 2003Jantan, Ling, et al., 2003Javidnia, Miri, et al., 2003Karioti, Skaltsa, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-1BPX-5RTX-5HP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.330.250.250.25
Tstart (C) 60.40.60.45.60.
Tend (C) 280.260.240.250.280.
Heat rate (K/min) 3.2.3.3.4.
Initial hold (min)  5.2.6.5.
Final hold (min)  20.   
I 1576.1572.1579.1586.1577.
ReferenceNgassapa, Runyoro, et al., 2003Senatore, Rigano, et al., 2003Shellie, Marriott, et al., 2003Shellie, Marriott, et al., 2003, 2Skaltsa, Demetzos, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5SPB-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (mum) 0.250.250.250.200.25
Tstart (C) 60.60.60.70.50.
Tend (C) 280.280.280.220.280.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min)     5.
Final hold (min)    15. 
I 1578.1578.1579.1552.1576.
ReferenceTsiri, Kretsi, et al., 2003Tsiri, Kretsi, et al., 2003Tzakou, Couladis, et al., 2003Cavaleiro, Salgueiro, et al., 2002Demetzos, Angelopoulou, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-5 MSSE-30DB-5DB-5
Column length (m) 30.30.25.25.30.
Carrier gas N2HeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.25 0.25
Tstart (C) 60.45.60.70.60.
Tend (C) 220.180.180.275.260.
Heat rate (K/min) 5.2.53.4.4.
Initial hold (min) 10.10.10.  
Final hold (min)   10.  
I 1578.1577.1569.1576.1576.
ReferenceFlamini, Cioni, et al., 2002Hudaib, Speroni, et al., 2002bin Jantan, Ayop, et al., 2002Javidnia, Miri, et al., 2002Javidnia, Miri, et al., 2002, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-5CP Sil 5 CBCP Sil 5 CBCP Sil 5 CB
Column length (m) 25.30.25.30.50.
Carrier gas HeHeN2H2He
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum)  0.250.250.250.4
Tstart (C) 70.45.60.60.60.
Tend (C) 260.300.280.280.280.
Heat rate (K/min) 4.3.4.2.3.
Initial hold (min)  6.6.10.10.
Final hold (min)  10. 40.60.
I 1576.1585.1557.1563.1563.
ReferenceMiri, Ramezani, et al., 2002Mondello, Zappia, et al., 2002Pino, Marbot, et al., 2002Pino, Marbot, et al., 2002, 2Pino, Marbot, et al., 2002, 3
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5RTX-5RTX-5HP-5
Column length (m) 50.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.45.45.60.
Tend (C) 220.280.250.250.280.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min)   6.6.5.
Final hold (min) 20.    
I 1567.1560.1576.1586.1575.
ReferencePintore, Usai, et al., 2002Pitarokili, Couladis, et al., 2002Shellie, Mondello, et al., 2002Shellie, Mondello, et al., 2002Aligiannis, Kalpoutzakis, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5HP-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.500.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.260.380.280.280.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min) 5.   5.
Final hold (min)  10.   
I 1573.1577.1570.1579.1576.
ReferenceAligiannis, Kalpoutzakis, et al., 2001, 2Couladis, Baziou, et al., 2001Couladis, Tsortanidou, et al., 2001Couladis, Tzakou, et al., 2001Giamakis, Kretsi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSRTX-5 MSBP-1DB-5HP-5MS
Column length (m) 30.30.50.30.30.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.70.60.60.50.
Tend (C) 210.210.220.240.250.
Heat rate (K/min) 4.4.2.3.3.
Initial hold (min) 10.10.   
Final hold (min) 10.10.   
I 1583.1583.1557.1580.1580.
ReferenceHudaib, Grazia Bellardi, et al., 2001Hudaib, Grazia Bellardi, et al., 2001Lota, Serra, et al., 2001Nogueira, Bittrich, et al., 2001Salido, Altarejos, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 280.200.240.240.240.
Heat rate (K/min) 4.2.3.3.3.
Initial hold (min) 5.5.2.2.2.
Final hold (min)  20.   
I 1577.1581.1575.1575.1575.
ReferenceSkaltsa, Mavrommati, et al., 2001Kim, Thuy, et al., 2000Maia, de Paula, et al., 2000Maia, de Paula, et al., 2000Maia, de Paula, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101CBP-1DB-1HP-5
Column length (m) 30.25.30.60.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.25   0.25
Tstart (C) 60.50.60.60.50.
Tend (C) 240.200.240.230.280.
Heat rate (K/min) 3.5.4.3.4.
Initial hold (min) 2.   5.
Final hold (min)    5. 
I 1575.1573.1570.1568.1576.
ReferenceMaia, de Paula, et al., 2000Menut, Bessiere, et al., 2000Zunino, Lopez, et al., 2000Javidnia and Shafiee, 1999Lazari, Skaltsa, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1DB-1OV-1OV-1
Column length (m) 25.60.30.25.25.
Carrier gas N2He  H2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)  0.250.250.30.3
Tstart (C) 50.50.50.50.50.
Tend (C) 200.220.220.200.200.
Heat rate (K/min) 5.4.3.3.3.
Initial hold (min)   3.1.1.
Final hold (min)    20.20.
I 1569.1581.1547.1544.1542.
ReferenceMenut, Bessiere, et al., 1999Mirza and Sefidkon, 1999Muselli, Hoi, et al., 1999Bicchi, Rubiolo, et al., 1998Bicchi, Fresia, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1DB-5Methyl SiliconeDB-5
Column length (m) 50.50.60.25.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.240.20.32
Phase thickness (mum) 0.250.25 0.31.
Tstart (C) 60.60.50.40.40.
Tend (C) 230.230.280.200.220.
Heat rate (K/min) 2.2.5.2.3.
Initial hold (min)   3.  
Final hold (min) 35.35.   
I 1566.1557.1572.1596.1601.
ReferenceMariotti, Costa, et al., 1997Mariotti, Tomi, et al., 1997Tzakou, Roussis, et al., 1997Píry, Príbela, et al., 1995Le Quere and Latrasse, 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Boti, Koukoua, et al., 2007
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Paolini, Muselli, et al., 2007
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Sabulal, Dan, et al., 2007
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Saroglou, Marin, et al., 2007
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Silva, Barbosa, et al., 2007
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Simoniatto, Bonani, et al., 2007
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Telascrea, de Araujo, et al., 2007
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Vagionas, Ngassapa, et al., 2007
Vagionas, K.; Ngassapa, O.; Runyoro, D.; Graikou, K.; Gortzi, O.; Chinou, I., Chemical analysis of edible aromatic plants growing in Tanzania, Food Chem., 2007, 105, 4, 1711-1717, https://doi.org/10.1016/j.foodchem.2007.05.029 . [all data]

Yu, Liao, et al., 2007
Yu, J.Q.; Liao, Z.X.; Cai, X.Q.; Lei, J.C.; Zou, G.L., Composition, antimicrobial activity and cytotoxicity of essential oils from Aristolochia mollissima, Environmental Toxicology and Pharmacology, 2007, 23, 2, 162-167, https://doi.org/10.1016/j.etap.2006.08.004 . [all data]

Andrianoelisoa H.S., Menut C., et al., 2006
Andrianoelisoa H.S.; Menut C.; de Chatelperron P.C.; Saracco J.; Ramanoelina P.; Danthu P., Intraspecific chemical variability and highlighting of chemotypes of leaf essential oils from Ravensara aromatica Sonnerat a tree endemic to Madagascar, Flavour Fragr. J., 2006, 21, 5, 833-838, https://doi.org/10.1002/ffj.1735 . [all data]

Batista-Pereira, Fernandes, et al., 2006
Batista-Pereira, L.G.; Fernandes, J.B.; Correa, A.G.; da Silva, M.F.G.F.; Vieira, P.C., Electrophysiological responses of eucalyptus brown looper Thyrinteina arnobia to essential oils of seven Eucalyptus species, J. Braz. Chem. Soc., 2006, 17, 3, 555-561, https://doi.org/10.1590/S0103-50532006000300019 . [all data]

Chorianopoulos N., Evergets E., et al., 2006
Chorianopoulos N.; Evergets E.; Mallouchos A.; Kalpoutzakis E.; Nychas G.J.; Haroutounian S.A., Characterization of the essential oil volatiles of Satureja thymbra and Satureja parnassica: Influence of harvesting time and antimicrobial activity, J. Agric. Food Chem., 2006, 54, 8, 3139-3145, https://doi.org/10.1021/jf053183n . [all data]

Dob, Dahmane, et al., 2006
Dob, T.; Dahmane, D.; Chelghoum, C., Essential oil composition of Juniperus oxycedrus growing in Algeria, Pharm. Biol., 2006, 44, 1, 1-6, https://doi.org/10.1080/13880200500530922 . [all data]

Dob, Dahmane, et al., 2006, 2
Dob, T.; Dahmane, D.; Agli, M.; Chelghoum, C., Essential oil composition of Lavandula stoechas from Algeria, Pharm. Biol., 2006, 44, 1, 60-64, https://doi.org/10.1080/13880200500496421 . [all data]

Flamini, Tebano, et al., 2006
Flamini, G.; Tebano, M.; Cioni, P.L.; Bagci, Y.; Dural, H.; Ertugrul, K.; Uysal, T.; Savran, A., A multivariate statistical approach to Centaurea classification using essential oil composition data of some species from Turkey, Pl. Syst. Evol., 2006, 261, 1-4, 217-228, https://doi.org/10.1007/s00606-006-0448-3 . [all data]

Gonny, Cavaleiro, et al., 2006
Gonny, M.; Cavaleiro, C.; Salgueiro, L.; Casanova, J., Analysis of Juniperus communis subsp. alpina needle, berry, wood and root oils by combination of GC, GC/MS and 13C-NMR, Flavour Fragr. J., 2006, 21, 1, 99-106, https://doi.org/10.1002/ffj.1527 . [all data]

Javidnia, Miri, et al., 2006
Javidnia, K.; Miri, R.; Banani, A., Volatile oil constituents of Haplophyllum tuberculatum (Forssk.) A. Juss. (Rutaceae) from Iran, J. Essent. Oil Res., 2006, 18, 4, 355-356, https://doi.org/10.1080/10412905.2006.9699111 . [all data]

Javidnia, Miri, et al., 2006, 2
Javidnia, K.; Miri, R.; Kamalinejad, M.; Khazraii, H., Chemical composition of the volatile oil of aerial parts of Valeriana sisymbriifolia Vahl. grown in Iran, Flavour Fragr. J., 2006, 21, 3, 516-518, https://doi.org/10.1002/ffj.1660 . [all data]

Kuiate, Bessière, et al., 2006
Kuiate, J.R.; Bessière, J.M.; Vilarem, G.; Amvam Zollo, P.H., Chemical composition and antidermatophytic properties of the essential oils from leaves, flowers and fruits of Cupressus lusitanica Mill. from Cameroon, Flavour Fragr. J., 2006, 21, 4, 693-697, https://doi.org/10.1002/ffj.1686 . [all data]

Liu J.M., Nan P., et al., 2006
Liu J.M.; Nan P.; Tsering Q.; Tsering T.; Bai Z.K.; Wang L.; Liu Z.J.; Zhong Y., Volatile constituents of the leaves and flowers of Salvia przewalskii Maxim. from Tibet, Flavour Fragr. J., 2006, 21, 3, 435-438, https://doi.org/10.1002/ffj.1607 . [all data]

Masoudi, Esmaeili, et al., 2006
Masoudi, S.; Esmaeili, A.; Khalilzadeh, M.A.; Rustaiyan, A.; Moazami, N.; Akhgar, M.R.; Varavipoor, M., Volatile constituents of Dorema aucheri Boiss., Seseli libanotis (L.) W. D. Koch var. armeniacum bordz. and Conium maculatum L. three Umbelliferae herbs growing wild in Iran, Flavour Fragr. J., 2006, 21, 5, 801-804, https://doi.org/10.1002/ffj.1722 . [all data]

Pavlovic, Kovacevic, et al., 2006
Pavlovic, M.; Kovacevic, N.; Tzakou, O.; Couladis, M., Essential oil composition of Anthemis triumfetti (L.) DC., Flavour Fragr. J., 2006, 21, 2, 297-299, https://doi.org/10.1002/ffj.1592 . [all data]

Pavlovic, Tzakou, et al., 2006
Pavlovic, M.; Tzakou, O.; Petrakis, P.V.; Couladis, M., The essential oil of Hypericum perforatum L., Hypericum tetrapterum Fries and Hypericum olympicum L. growing in Greece, Flavour Fragr. J., 2006, 21, 1, 84-87, https://doi.org/10.1002/ffj.1521 . [all data]

Pinto, Pina-Vaz, et al., 2006
Pinto, E.; Pina-Vaz, C.; Salgueiro, L.; Goncalves, M.J.; Costa-de-Oliveira, S.; Cavaleiro, C.; Palmeira, A.; Rodrigues, A.; Martinez-de-Oliveira, J., Antifuncal activity of the essential oil Thymus pulegioides on Candida, Aspergillus and dermatophyte species, Journal of Medical Microbiology, 2006, 55, 10, 1367-1373, https://doi.org/10.1099/jmm.0.46443-0 . [all data]

Radulovic, Mananjarasoa, et al., 2006
Radulovic, N.; Mananjarasoa, E.; Harinantenaina, L.; Yoshinori, A., Essential oil composition of four Croton species from Madagascar and their chemotaxonomy, Biochem. Syst. Ecol., 2006, 34, 8, 648-653, https://doi.org/10.1016/j.bse.2006.02.005 . [all data]

Ramezani, Behravan, et al., 2006
Ramezani, M.; Behravan, J.; Yazdinezhad, A., Composition and antimicrobial activity of the volatile oil of Artemisia kopetdaghensis Krasch., M.Pop. Linecz ex Poljak from Iran, Flavour Fragr. J., 2006, 21, 6, 869-871, https://doi.org/10.1002/ffj.1644 . [all data]

Rezazadeh, Hamedani, et al., 2006
Rezazadeh, S.; Hamedani, M.P.; Dowlatabadi, R.; Yazdani, D.; Shafiee, A., Chemical composition of the essential oils of Stachys schtschegleevii Sosn. and Stachys balansae Boiss Kotschy from Iran, Flavour Fragr. J., 2006, 21, 2, 290-293, https://doi.org/10.1002/ffj.1587 . [all data]

Saroglou, Dorizas, et al., 2006
Saroglou, V.; Dorizas, N.; Kypriotakis, Z.; Skaltsa, H.D., Analysis of the essential oil composition of eight Anthemis species from Greece, J. Chromatogr. A, 2006, 1104, 1-2, 313-322, https://doi.org/10.1016/j.chroma.2005.11.087 . [all data]

Silva-Brandão, Solferini, et al., 2006
Silva-Brandão, K.L.; Solferini, V.N.; Trigo, J.R., Chemical and phylogenetic relationships among Aristolochia L. (Aristolochiaceae) from southeastern Brazil, Biochem. Syst. Ecol., 2006, 34, 4, 291-302, https://doi.org/10.1016/j.bse.2005.10.011 . [all data]

Su, Ho, et al., 2006
Su, Y.C.; Ho, C.L.; Wang, E.I.C., Analysis of leaf essential oils from the indigenous five conifers of Taiwan, Flavour Fragr. J., 2006, 21, 3, 447-452, https://doi.org/10.1002/ffj.1685 . [all data]

Su, Ho, et al., 2006, 2
Su, Y.-C.; Ho, C.-L.; Wang, E.I.-C.; Chang, S.-T., Antifungal activities and chemical compositions of essential oils from leaves of four eucalypts, Taiwan J. For. Sci., 2006, 21, 1, 49-61. [all data]

Vujisic L., Vuckovic I., et al., 2006
Vujisic L.; Vuckovic I.; Tesevic V.; Dokovic D.; Ristic M.S.; Janackovic P.; Milosavljevic S., Comparative examination of the essential oils of Anthemis ruthenica and A-arvensis wild-growing in Serbia, Flavour Fragr. J., 2006, 21, 3, 458-461, https://doi.org/10.1002/ffj.1681 . [all data]

Vundac, Pfeifhofer, et al., 2006
Vundac, V.B.; Pfeifhofer, H.W.; Brantner, A.H.; Males, Z.; Plazibat, M., Essential oils of seven Stachys taxa from Croatia, Biochem. Syst. Ecol., 2006, 34, 12, 875-881, https://doi.org/10.1016/j.bse.2006.04.010 . [all data]

Boskovic, Radulovic, et al., 2005
Boskovic, Z.; Radulovic, N.; Stojanovic, G., Essential oil composition of four Achillea species from the balkans and its chemotaxonomic significance, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 6, 674-678, https://doi.org/10.1007/s10600-006-0009-6 . [all data]

Brantner, Pfeifhofer, et al., 2005
Brantner, A.H.; Pfeifhofer, H.W.; Ercegovac, O.; Males, Z.; Plazibat, M., Essential oil composition and antioxidant activity of Thymus bracteosus Vis. ex Benth., Flavour Fragr. J., 2005, 20, 6, 596-600, https://doi.org/10.1002/ffj.1494 . [all data]

Celik, Gokturk, et al., 2005
Celik, S.; Gokturk, R.S.; Flamini, G.; Cioni, P.L.; Morelli, I., Essential oils of Phlomis leucophracta, Phlomis chimerae and Phlomis grandiflora var. grandiflora from Turkey, Biochem. Syst. Ecol., 2005, 33, 6, 617-623, https://doi.org/10.1016/j.bse.2004.11.010 . [all data]

Dob T., Berramdane T., et al., 2005
Dob T.; Berramdane T.; Chelghoum C., Analysis of essential oil from the needles of Pinus pinaster growing in Algeria, Chem. Nat. Compd. (Engl. Transl.), 2005, 41, 5, 545-548, https://doi.org/10.1007/s10600-005-0202-z . [all data]

Dob, Dahmane, et al., 2005
Dob, T.; Dahmane, D.; Berramdane, T.; Chelghoum, C., Chemical composition of the essential oil of Artemisia campestris L. from Algeria, Pharm. Biol., 2005, 43, 6, 512-514, https://doi.org/10.1080/13880200500220664 . [all data]

Dugo, Mondello, et al., 2005
Dugo, P.; Mondello, L.; Favoino, O.; Cicero, L.; Rodriguez Zenteno, N.A.; Dugo, G., Characterization of cold-pressed Mexican dancy tangerine oils, Flavour Fragr. J., 2005, 20, 1, 60-66, https://doi.org/10.1002/ffj.1367 . [all data]

Fanciullino, Gancel, et al., 2005
Fanciullino, A.-L.; Gancel, A.-L.; Froelicher, Y.; Luro, F.; Ollitrault, P.; Brillouet, J.-M., Effects of Nucleo-cytoplasmic Interactions on Leaf Volatile Compounds from Citrus Somatic Diploid Hybrids, J. Agric. Food Chem., 2005, 53, 11, 4517-4523, https://doi.org/10.1021/jf0502855 . [all data]

de Feo, Urrunaga Soria, et al., 2005
de Feo, V.; Urrunaga Soria, E.; Urrunaga Soria, R.; Pizza, C., Composition and in vitro toxicity of the essential oil of Tagetes terniflora HBK. (Asteraceae), Flavour Fragr. J., 2005, 20, 1, 89-92, https://doi.org/10.1002/ffj.1379 . [all data]

Flamini, Luigi Cioni, et al., 2005
Flamini, G.; Luigi Cioni, P.; Morelli, I.; Celik, S.; Gokturk, R.S.; Unal, O., Essential oil of Stachys aleurites from Turkey, Biochem. Syst. Ecol., 2005, 33, 1, 61-66, https://doi.org/10.1016/j.bse.2004.05.013 . [all data]

bin Jantan, Yalvema, et al., 2005
bin Jantan, I.; Yalvema, M.F.; Ahmad, N.W.; Jamal, J.A., Insecticidal activities of the leaf oils of eight Cinnamomum species against Aedes aegypti and Aedes albopictus, Pharm. Biol., 2005, 43, 6, 526-532, https://doi.org/10.1080/13880200500220771 . [all data]

Javidnia, Miri, et al., 2005
Javidnia, K.; Miri, R.; Mehregan, I.; Sadeghpour, H., Volatile constituents of the essential oil of Nepeta ucrainica L. ssp. kopetdaghensis from Iran, Flavour Fragr. J., 2005, 20, 2, 219-221, https://doi.org/10.1002/ffj.1381 . [all data]

Paolini, Costa, et al., 2005
Paolini, J.; Costa, J.; Bernardini, A., Analysis of the essential oil from aerial parts of Eupatorium cannabinum subsp. corsicum (L.) by gas chromatography with electron impact and chemical ionization mass spectrometry, J. Chromatogr. A, 2005, 1076, 1-2, 170-178, https://doi.org/10.1016/j.chroma.2005.03.131 . [all data]

Senatore, Napolitano, et al., 2005
Senatore, F.; Napolitano, F.; Arnold, N.A.; Bruno, M.; Herz, W., Composition and antimicrobial activity of the essential oil of Achillea falcata L. (Asteraceae), Flavour Fragr. J., 2005, 20, 3, 291-294, https://doi.org/10.1002/ffj.1411 . [all data]

Seo and Baek, 2005
Seo, W.H.; Baek, H.H., Identification of characteristic aroma-active compounds from water dropword (Oenanthe javanica DC.), J. Agric. Food Chem., 2005, 53, 17, 6766-6770, https://doi.org/10.1021/jf050150z . [all data]

Simionatto, Porto, et al., 2005
Simionatto, E.; Porto, C.; da Silva, U.F.; Squizani, A.; Dalcol, I.I.; Morel, A.F., Composition and antimicrobial activity of the essential oil from Aloysia sellowii, J. Braz. Chem. Soc., 2005, 16, 6B, 1458-1462, https://doi.org/10.1590/S0103-50532005000800028 . [all data]

Tchoumbougnang, Zollo, et al., 2005
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Pintore, G.; Usai, M.; Bradesi, P.; Juliano, C.; Boatto, G.; Tomi, F.; Chessa, M.; Cerri, R.; Casanova, J., Chemical composition and antimicrobial activity of Rosmarinus officinalis L. oils from Sardinia and Corsica, Flavour Fragr. J., 2002, 17, 1, 15-19, https://doi.org/10.1002/ffj.1022 . [all data]

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Notes

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