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1H-Cycloprop[e]azulen-7-ol, decahydro-1,1,7-trimethyl-4-methylene-, [1ar-(1a«alpha»,4a«alpha»,7«beta»,7a«beta»,7b«alpha»)]-


Normal alkane RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-WaxHP-InnowaxDB-WaxRTX-WaxHP-Innowax
Column length (m) 60.60.30.60.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.220.250.250.220.25
Phase thickness (mum) 0.250.250.250.250.52
Tstart (C) 60.60.40.60.35.
Tend (C) 230.220.230.230.205.
Heat rate (K/min) 2.5.4.2.3.
Initial hold (min)  1.2. 10.
Final hold (min) 5.5.4.530.10.
I 2091.2123.2138.2101.2144.
ReferenceBendiabdellah, El Amine Dib, et al., 2012Feng, Cui, et al., 2011Zeng, Xie, et al., 2011Museli, Pau, et al., 2009Wannes, Mhamdi, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxRTX-WaxHP InnowaxPEG-20MHP-Innowax
Column length (m) 30.60.30.60.30.
Carrier gas NitrogenHeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.220.320.250.25
Phase thickness (mum) 0.250.250.500.250.25
Tstart (C) 50.60.60.90.60.
Tend (C) 280.230.260.225.240.
Heat rate (K/min) 5.2.3.3.2.
Initial hold (min) 1.    
Final hold (min) 1.35. 15.20.
I 2125.2103.2128.2118.2108.
ReferenceBousaada, Ammar, et al., 2008Paolini, Tomi, et al., 2008Capetanos, Saroglou, et al., 2007Gil A., Van Baren C.M., et al., 2007Hachicha, Skanji, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBTC-FFAPCarbowax 20MDB-WaxSupelcowax-10
Column length (m) 30. 30.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.320.2
Phase thickness (mum) 0.250.250.250.250.2
Tstart (C) 40.60.60.70.70.
Tend (C) 220.220.230.220.220.
Heat rate (K/min) 3.3.3.4.3.
Initial hold (min) 1.    
Final hold (min) 2.30.  15.
I 2136.2130.2090.2133.2112.
ReferenceHymete, Rohloff, et al., 2007Kurose, Okamura, et al., 2007Limberger, Scopel, et al., 2007Pala-Paul, Brophy, et al., 2007Pinto, Salgueiro, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10Supelcowax-10Supelcowax-10AT-WaxDB-Wax
Column length (m) 30.30.30.60.60.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.5
Tstart (C) 50.40.40.60.50.
Tend (C) 250.250.250.200.230.
Heat rate (K/min) 2.2.3.4.3.
Initial hold (min)   5. 2.
Final hold (min)  33.10.20.20.
I 2121.2125.2104.2150.2110.
ReferenceRaal, Orav, et al., 2007Sylvestre, Pichette, et al., 2007Vichi, Riu-Aumatell, et al., 2007Borges, Rojas, et al., 2006Cai, Lin, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10SupelcowaxNB-20MSupelcowax-10
Column length (m) 60.30.30.30.30.
Carrier gas N2 N2HeHe
Substrate      
Column diameter (mm) 0.250.250.320.20.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.40.50.50.50.
Tend (C) 230.210.200.250.220.
Heat rate (K/min) 2.2.5.2.4.
Initial hold (min) 2.2.  1.
Final hold (min) 20.33.  10.
I 2121.2124.2142.2126.2121.
ReferenceChoi, 2006Garneau F.X., Collin G., et al., 2006Martin, Joseph, et al., 2006Orav, Raal, et al., 2006Wong, Lim, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxDB-WaxHP-InnowaxCP-WaxDB-Wax
Column length (m) 50.30.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.320.25
Phase thickness (mum) 0.50.250.170.250.25
Tstart (C) 60.60.60.40.50.
Tend (C) 250.250.210.180.180.
Heat rate (K/min) 2.5.4.5.3.
Initial hold (min)   3.2. 
Final hold (min) 60.10.15. 40.
I 2093.2124.2153.2088.2120.
ReferenceBendimerad and Bendiab, 2005Fakhari A.R., Sonboli A., et al., 2005Ferretti, Maggi, et al., 2005Ka, Choi, et al., 2005Lee, Umano, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10Supelcowax-10DB-WaxSupelcowax-10
Column length (m) 60.30.30.60.30.
Carrier gas He  N2N2
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.40.40.70.40.
Tend (C) 220.210.220.230.230.
Heat rate (K/min) 3.2.3.2.2.
Initial hold (min)  2.5.2. 
Final hold (min)  33.10.20. 
I 2133.2115.2104.2121.2110.
ReferencePalá-Paúl, Pérez-Alonso, et al., 2005Stevanovic, Garneau, et al., 2005Vichi, Riu-Aumatell, et al., 2005Choi, 2004González, Guerra, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10Innowax FSCBP-20DB-Wax
Column length (m) 60.30.60.25.60.
Carrier gas He HeliumN2He
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum)  0.25 0.250.25
Tstart (C) 60.40.60.60.35.
Tend (C) 220.210.220.220.220.
Heat rate (K/min) 2.2.4.5.3.
Initial hold (min) 4.2.10.  
Final hold (min)  33.   
I 2121.2123.2144.2101.2132.
ReferenceJiang and Kubota, 2004Lopez Arze, Collin, et al., 2004Lourens, Reddy, et al., 2004Mallavarapu, Kulkarni, et al., 2004Palá-Paúl, Brophy, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxSW-10DB-WaxDB-WaxBP-20
Column length (m) 50.50.60.60.25.
Carrier gas HeHe NitrogenH2
Substrate      
Column diameter (mm) 0.20.200.250.250.33
Phase thickness (mum) 0.20.250.250.250.5
Tstart (C) 70.50.70.70.80.
Tend (C) 220.230.230.230.220.
Heat rate (K/min) 4.2.2.2.5.
Initial hold (min)   2.2. 
Final hold (min)   20.  
I 2127.2104.2133.2133.2136.
ReferencePalá-Paúl, García-Jiménez, et al., 2004Raal, Paaver, et al., 2004Sawamura, Son, et al., 2004Sawamura, Sou, et al., 2004Dunlop, Bignell, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TC-WaxDB-WaxCarbowax 20MSW-10Supelcowax-10
Column length (m) 60.60.50.50.30.
Carrier gas  HeliumN2HeN2
Substrate      
Column diameter (mm) 0.250.250.250.200.25
Phase thickness (mum)   0.250.250.25
Tstart (C) 80.70.90.50.40.
Tend (C) 240.210.220.250.230.
Heat rate (K/min) 3.2.3.2.2.
Initial hold (min)      
Final hold (min)  60.   
I 2110.2125.2126.2100.2110.
ReferenceMiyazawa, Yamafuji, et al., 2003Mookdasanit, Tamura, et al., 2003Priestap, van Baren, et al., 2003Raal, Arak, et al., 2003Rotman, Ahumada, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-InnowaxInnowaxCarbowax 20MHP-WaxDB-Wax
Column length (m) 50.60.25.50.60.
Carrier gas  HeN2N2He
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.2 0.250.250.25
Tstart (C) 50.60.50.75.45.
Tend (C) 220.220.250.220.240.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min) 5.10. 4. 
Final hold (min)  10.10.  
I 2150.2144.2140.2127.2121.
ReferenceStashenko, Jaramillo, et al., 2003Suleimenov, Atazharova, et al., 2003Zrira, Elamrani, et al., 2003Priestap, van Baren, et al., 2002Christoph, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PEG-20MCP-Wax 52CBBP-20BP-20HP Innowax FSP
Column length (m) 50.50.25.25.60.
Carrier gas HeHeNitrogen He
Substrate      
Column diameter (mm) 0.20.300.500.330.25
Phase thickness (mum)  0.250.250.50.25
Tstart (C) 70.40.60.80.60.
Tend (C) 250.220.200.220.220.
Heat rate (K/min) 2.3.5.5. 
Initial hold (min)  5.  10.
Final hold (min)     10.
I 2100.2097.2098.2136.2144.
ReferenceOrav, Kailas, et al., 2001Chagonda, Makanda, et al., 2000Mallavarapu, Rao, et al., 2000Dunlop, Bignell, et al., 1999Kaya, Baser, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase InnowaxHP-InnowaxHP-InnowaxHP-InnowaxSupelcowax-10
Column length (m) 60.60.60.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 60.60.60.60.60.
Tend (C) 220.220.220.220.240.
Heat rate (K/min)     4.
Initial hold (min) 10.10.10.10. 
Final hold (min)      
I 2144.2144.2144.2144.2110.
ReferenceKaya, Baser, et al., 1999, 2Kaya, Baser, et al., 1999, 3Kaya, Baser, et al., 1999, 3Kaya, Baser, et al., 1999, 3Labuckas, Zygadlo, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxBP-20Supelcowax-10DB-Wax
Column length (m) 60.60.25.30.30.
Carrier gas HeN2H2HeN2
Substrate      
Column diameter (mm) 0.25 0.330.250.25
Phase thickness (mum) 0.250.250.5 0.25
Tstart (C) 60.60.80.60.45.
Tend (C) 240.220.220.240.220.
Heat rate (K/min) 4.5.5.4.3.
Initial hold (min)      
Final hold (min)      
I 2129.2147.2136.2149.2128.
ReferenceNgassoum, Yonkeu, et al., 1999Weyerstahl, Marschall, et al., 1999Bignell, Dunlop, et al., 1998Lamarque, Maestri, et al., 1998Molleken U., Sinnwell V., et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-Innowax FSCDB-WaxHP-Innowax FSCBP-20BP-20
Column length (m) 60.30.60.25.25.
Carrier gas HeHeHeH2H2
Substrate      
Column diameter (mm) 0.250.320.250.330.33
Phase thickness (mum) 0.25  0.50.5
Tstart (C) 60.60.60.80.80.
Tend (C) 220.250.240.220.220.
Heat rate (K/min) 4.3.4.5.5.
Initial hold (min) 10. 10.  
Final hold (min) 10. 10.  
I 2144.2151.2144.2136.2136.
ReferenceTümen, Baser, et al., 1998Abreu and Noronha, 1997Baser, Kirimer, et al., 1997Bignell, Dunlop, et al., 1997Bignell, Dunlop, et al., 1997, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20BP-20BP-20BP-20Supelcowax-10
Column length (m) 25.25.25.25.30.
Carrier gas H2H2 H2 
Substrate      
Column diameter (mm) 0.330.330.330.330.25
Phase thickness (mum) 0.50.50.50.5 
Tstart (C) 80.80.80.80.60.
Tend (C) 220.220.220.220.240.
Heat rate (K/min) 5.5.5.5.4.
Initial hold (min)      
Final hold (min)      
I 2136.2136.2136.2136.2118.
ReferenceBignell, Dunlop, et al., 1997, 3Bignell, Dunlop, et al., 1997, 4Bignell, Dunlop, et al., 1997, 5Bignell, Dunlop, et al., 1997, 6Zunino, Novillo-Newton, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10SP-1000Supelcowax-10Carbowax 20MDB-Wax
Column length (m) 0.85.60.45.30.
Carrier gas HeHeHeHydrogen 
Substrate      
Column diameter (mm) 0.250.500.250.320.32
Phase thickness (mum)   0.251.0 
Tstart (C) 40.65.40.60.70.
Tend (C) 240.225.200.200.200.
Heat rate (K/min) 3.3.3.2.4.
Initial hold (min)   3.5.2.
Final hold (min)   30.  
I 2149.2136.2149.2103.2145.
ReferenceZygadlo, Ariza-Espinar, et al., 1997Brophy, Goldsack, et al., 1996Wong and Lai, 1996Kollmannsberger, Nitz, et al., 1992Wyllie, Brophy, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase FFAP
Column length (m) 50.
Carrier gas  
Substrate  
Column diameter (mm)  
Phase thickness (mum)  
Tstart (C) 50.
Tend (C) 180.
Heat rate (K/min) 10.
Initial hold (min) 1.
Final hold (min)  
I 2152.
ReferenceBrophy, Davies, et al., 1989
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bendiabdellah, El Amine Dib, et al., 2012
Bendiabdellah, A.; El Amine Dib, M.; Djabou, N.; Allali, H.; Tabti, B.; Costa, J.; Myseli, A., Biological activities and volatile cinstituents of Daucus muricatus L. from Algeria, Chem. Centr. J., 2012, 6, 48, 1-22. [all data]

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Bendimerad and Bendiab, 2005
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Notes

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