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1H-Cycloprop[e]azulen-7-ol, decahydro-1,1,7-trimethyl-4-methylene-, [1ar-(1a«alpha»,4a«alpha»,7«beta»,7a«beta»,7b«alpha»)]-


Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5RTX-1HP-5 MSHP-5 MSDB-5
Column length (m) 30.60.30.30.35.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.250.250.20
Phase thickness (mum) 0.250.250.250.250.10
Tstart (C) 60.60.80.40.50.
Tend (C) 240.230.240.250.200.
Heat rate (K/min) 3.2.4.3.4.
Initial hold (min)   3.1. 
Final hold (min)  5.10.3. 
I 1578.1572.1570.1578.1576.
ReferenceRodriques, Amorim, et al., 2013Bendiabdellah, El Amine Dib, et al., 2012Dutra, Pittella, et al., 2012Jian-Yu, Zhu, et al., 2012Silva, Suzuki, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5 MSHP-5 MSHP-5DB-1
Column length (m) 35.30.30.30.30.
Carrier gas Helium HeliumHeliumHelium
Substrate      
Column diameter (mm) 0.200.250.250.250.25
Phase thickness (mum) 0.100.250.250.250.25
Tstart (C) 50.60.50.60.40.
Tend (C) 200.300.250.240.210.
Heat rate (K/min) 4.15.7.3.5.
Initial hold (min)  2.1.  
Final hold (min)  10.5.  
I 1598.1572.1578.1578.1578.
ReferenceSilva, Suzuki, et al., 2012Xu, Han, et al., 2012Zouari, Ayadi, et al., 2012Bertoli, Lepnardi, et al., 2011Fathi, Sahari, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5ZB-5ZB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumNitrogenNitrogenNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 50.60.40.40.60.
Tend (C) 180.240.200.200.250.
Heat rate (K/min) 2.3.5.5.4.
Initial hold (min)   5.5.1.
Final hold (min)    5.10.
I 1575.1576.1548.1548.1576.
ReferenceHammami, Kamoun, et al., 2011Karimi, Farmani, et al., 2011Vazques, Aimar, et al., 2011Vazquez, Demmel, et al., 2011Yousefzadi, Heidari, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5SPB-1HP-5 MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.2520.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.50.70.60.
Tend (C) 240.250.250.290.240.
Heat rate (K/min) 3.2.5.5.3.
Initial hold (min)   3.  
Final hold (min)   15.  
I 1574.1578.1563.1585.1576.
ReferenceCavar, Maksimovic, et al., 2010Ho, Wang, et al., 2010Lazarevic, Palic, et al., 2010Lazarevic, Radulovic, et al., 2010Magalhaes, Lima, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSDB-1DB-1BP-1HP-5 MS
Column length (m) 60.60.25. 30.
Carrier gas HeliumNitrogenNitrogenNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.25 0.25
Phase thickness (mum) 0.250.250.25 0.25
Tstart (C) 40.60.60.60.60.
Tend (C) 250.250.250.220.220.
Heat rate (K/min) 5.5.4.5.5.
Initial hold (min) 15. 1.10.10.
Final hold (min) 15. 10.30. 
I 1590.1563.1574.1569.1577.
ReferenceMesa-Arango, Betancur-Galvis, et al., 2010Meshkatalsadat, Safaei-Ghomi. J., et al., 2010Mirjalili, Salehi, et al., 2010Mishra, Chaudhary, et al., 2010Ogunwande, Flamini, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSHP-5HP-5 MSDB-1
Column length (m) 30.30.30.30.60.
Carrier gas HeliumHeliumHydrogenHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 100.70.70.70.60.
Tend (C) 220.290.290.290.250.
Heat rate (K/min) 2.5.5.5.4.
Initial hold (min)     1.
Final hold (min)  10. 10.10.
I 1573.1586.1587.1581.1570.
ReferencePripdeevech, Chumpolsri, et al., 2010Radulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Radulovic, Dordevic, et al., 2010, 2Safaei-Ghomi, Meshkatalsadat, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5 MSDB-5DB-1HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.40.50.50.
Tend (C) 240.240.240.220.250.
Heat rate (K/min) 3.3.3.4.7.
Initial hold (min)   1.2.1.
Final hold (min)    2.5.
I 1577.1572.1567.1580.1593.
ReferenceScherer, Wagner, et al., 2010Silva, Pott, et al., 2010de Souza, Lopes, et al., 2010Xu, Tang, et al., 2010Zouari, Zouari, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5VF-1 MSHP-5
Column length (m) 30.30.30.30.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.20
Phase thickness (mum) 0.250.250.250.250.33
Tstart (C) 60.35.70.60.60.
Tend (C) 240.220.240.280.240.
Heat rate (K/min) 3.3.5.4.3.
Initial hold (min)    5. 
Final hold (min)  40. 10.7.
I 1578.1563.1572.1569.1586.
ReferenceAlim, Goze, et al., 2009El-Massry, El-Ghorab, et al., 2009Lawal and Oyedelji, 2009Marchesini, Prada, et al., 2009Maridass, 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1RTX-1OV-1DB-5DB-5
Column length (m) 60.60.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.220.220.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.40.45.40.
Tend (C) 230.230.300.250.250.
Heat rate (K/min) 2.2.4.3.3.
Initial hold (min)   2.3.1.
Final hold (min) 30.30.10.5.10.
I 1560.1572.1542.1589.1576.
ReferenceMuseli, Pau, et al., 2009Museli, Pau, et al., 2009Nibret and Wink, 2009Porto, Decorti, et al., 2009Rahimi-Nasrabadi, Gholivand, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5HP-5MSHP-5 MS
Column length (m) 30.50.30.30.30.
Carrier gas NitrogenNitrogenHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.200.250.250.25
Phase thickness (mum) 0.250.320.250.250.25
Tstart (C) 40.60.40.50.60.
Tend (C) 230.220.240.240.300.
Heat rate (K/min) 2.5.3.5.15.
Initial hold (min)  3.1. 2.
Final hold (min)  5.  10.
I 1580.1578.1567.1576.1572.
ReferenceScrivanti, Anton, et al., 2009Shafaghat and Sadeghi, 2009de Souza, Lopes, et al., 2009Wannes, Mhamdi, et al., 2009Xu, Han, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSHP-5Ultra 2DB-5
Column length (m) 30.30.30.50.25.
Carrier gas Helium NitrogenHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.250.200.22
Phase thickness (mum) 0.25 0.250.110.25
Tstart (C) 50.60.50.60.50.
Tend (C) 280.280.280.230.300.
Heat rate (K/min) 9.3.5.2.6.5
Initial hold (min) 3. 1.5.2.
Final hold (min) 3. 1.30.7.
I 1576.1577.1599.1576.1617.
ReferenceAicha, Ines, et al., 2008Baziou, Couladis, et al., 2008Bousaada, Ammar, et al., 2008Byun and Shin, 2008Chieng, Assim, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52VF-5MSHP-5SLB-5 MSZB-1
Column length (m) 50.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.240.100.50.45.
Tend (C) 280.320.240.250.230.
Heat rate (K/min) 3.20.5.3.3.
Initial hold (min)  1.2.2. 
Final hold (min) 20. 5.10. 
I 1590.1588.1576.1580.1561.
ReferenceDjarri, Medjroubi, et al., 2008Kowalski, 2008Lago, Romoff, et al., 2008Lo Presti, Sciarrone, et al., 2008Mierendorff, Stahl-Biskup, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSRTX-1HP-5 MSBPX-5HP-5
Column length (m) 30.60.30.7.525.
Carrier gas HeliumHeHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.220.250.100.25
Phase thickness (mum) 0.250.250.2510.0.25
Tstart (C) 50.60.50.60.60.
Tend (C) 300.230.240.240.240.
Heat rate (K/min) 5.2.3.3.4.
Initial hold (min) 5.   2.
Final hold (min) 5.35.   
I 1572.1563.1624.1580.1577.
ReferenceNoudogbessi, Yedomonhan, et al., 2008Paolini, Tomi, et al., 2008Sarikurkcu, Tepe, et al., 2008Shellie, 2008Verdian-rizi, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-5MSHP-5MSHP-5MS
Column length (m) 30.50.30.30.30.
Carrier gas HeliumNitrogenHeHeHe
Substrate      
Column diameter (mm) 0.250.200.250.250.25
Phase thickness (mum) 0.320.320.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 250.220.240.240.280.
Heat rate (K/min) 5.5.3.3.3.
Initial hold (min) 30.3.   
Final hold (min)  5.   
I 1575.1589.1577.1597.1562.
ReferenceYassa and Akhani, 2008Amiri, 2007Andrade, Oliveira, et al., 2007Argyropoulou, Daferera, et al., 2007Basta, Pavlovic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSHP-5 MSDB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeliumHe
Substrate      
Column diameter (mm) 0.250.260.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 280.240.280.280.240.
Heat rate (K/min) 3.3.3.4.3.
Initial hold (min)    5. 
Final hold (min)      
I 1557.1574.1576.1578.1578.
ReferenceBasta, Tzakou, et al., 2007Bos, Woerdenbag, et al., 2007Bozin B., Mlmica-Dukic N., et al., 2007Capetanos, Saroglou, et al., 2007Da Silva J.K.R., Sousa P.J.C., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5MSDB-15 % Phenyl methyl siloxane
Column length (m) 30.30.30.60.60.
Carrier gas HeliumHeliumHeNitrogenHe
Substrate      
Column diameter (mm) 0.260.250.250.250.25
Phase thickness (mum) 0.250.260.250.250.25
Tstart (C) 60.60.60.60.90.
Tend (C) 290.240.250.250.225.
Heat rate (K/min) 3.4.2.4.3.
Initial hold (min)  2.8.1. 
Final hold (min)  20.15.10.15.
I 1574.1583.1574.1576.1578.
ReferenceElfami, Bos, et al., 2007Farsam, Amanlou, et al., 2007Ferhat, Tigrine-Kordjani, et al., 2007Ghasempour, Shirinpour, et al., 2007Gil A., Van Baren C.M., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Col-Elite 5MSHP-1BP-1DB-5AT-5
Column length (m) 30.30. 30.60.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 30.60.60.60.60.
Tend (C) 246.240.220.300.260.
Heat rate (K/min) 3.2.5.3.4.
Initial hold (min)      
Final hold (min)  20.6.  
I 1598.1577.1564.1566.1580.
ReferenceGudaityte and Venskutonis R.P., 2007Hachicha, Skanji, et al., 2007Kiran, Devi, et al., 2007Limberger, Scopel, et al., 2007Meccia, Rojas, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-5DB-1DB-5DB-5DB-1
Column length (m) 30.30.30.30.50.
Carrier gas  HeliumHeliumHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.95.
Tend (C) 220.260.300.220.240.
Heat rate (K/min) 4.2.53.4.4.
Initial hold (min) 5.1.   
Final hold (min) 20.20.   
I 1577.1545.1548.1579.1576.
ReferenceMohottalage, Tabacchi, et al., 2007Monser-Esfahani, Karamkhani, et al., 2007Moreno, Lima, et al., 2007Morteza-Semnani, Saeedi, et al., 2007Pala-Paul, Brophy, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSSPB-1SPB-5DB-1HP-5
Column length (m) 25.30.30.60.30.
Carrier gas HeliumHeHeNitrogenHelium
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.250.20.250.250.25
Tstart (C) 100.70.50.60.40.
Tend (C) 280.220.250.250.260.
Heat rate (K/min) 4.3.2.4.4.
Initial hold (min) 3.  1. 
Final hold (min) 5.15. 10. 
I 1581.1553.1574.1576.1572.
ReferencePhutdhawong, Kawaree, et al., 2007Pinto, Salgueiro, et al., 2007Raal, Orav, et al., 2007Reza, Ebrahim, et al., 2007Ristic, Krivokuca-Dokic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1DB-5HP-5 MS
Column length (m) 30.30.60.30.30.
Carrier gas HeHeNitrogen Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.40.60.
Tend (C) 240.320.250.250.280.
Heat rate (K/min) 4.10.5.2.3.
Initial hold (min)      
Final hold (min)  4.10.33. 
I 1579.1575.1574.1573.1578.
ReferenceSefidkon, Abbasi, et al., 2007Smelcerovic, Spiteller, et al., 2007Sonboli, Kanani, et al., 2007Sylvestre, Pichette, et al., 2007Tsokou, Georgopoulos, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5MSHP-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.40.60.60.
Tend (C) 280.250.260.300.300.
Heat rate (K/min) 3.3.4.3.3.
Initial hold (min)  5.   
Final hold (min)  10.   
I 1578.1571.1573.41567.1573.
ReferenceVagionas, Graikou, et al., 2007Vichi, Riu-Aumatell, et al., 2007Zizovic, Stamenic, et al., 2007Apel, Sobral, et al., 2006Apel, Sobral, et al., 2006, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBZB-5AT-5HP-5MS
Column length (m) 30.25.30.60.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.25 0.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 40.80.40.60.60.
Tend (C) 260.270.300.200.280.
Heat rate (K/min) 4.10.2.4.3.
Initial hold (min) 5.    
Final hold (min)    20. 
I 1574.1572.1556.1574.1578.
ReferenceAskari and Sefidkon, 2006Ayoub, Al-Azizi, et al., 2006Biondi, Sari, et al., 2006Borges, Rojas, et al., 2006Bozin, Mimicá-Dukic, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSDB-5HP-5HP-1
Column length (m) 30.30.30.30.50.
Carrier gas He HeliumHeHe
Substrate      
Column diameter (mm) 0.320.250.260.250.2
Phase thickness (mum) 0.250.250.250.250.33
Tstart (C) 60.60.60.50.60.
Tend (C) 246.280.290.300.250.
Heat rate (K/min) 3.4.3.5.2.
Initial hold (min)    5. 
Final hold (min)    5.40.
I 1578.1574.1574.1578.1557.
ReferenceCoronel, Cerda-Garcia-Rojas, et al., 2006Ebrahim Sajjadi and Mehregan, 2006Elfami, Komar, et al., 2006Figuérédo, Cabassu, et al., 2006Filippi, Lanfranchi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-1HP-5
Column length (m) 30.30.30.60.30.
Carrier gas  HeHe He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 210.240.240.250.240.
Heat rate (K/min) 2.5.5.5.4.
Initial hold (min) 2.2.2.  
Final hold (min) 33.  10. 
I 1573.1575.1575.1577.1576.
ReferenceGarneau F.X., Collin G., et al., 2006Gohari, Hadjiakhoondi, et al., 2006Gohari A.R., Hadjiakhoondi A., et al., 2006Hadian, Sonboli, et al., 2006Ibañez and Usubillaga, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5BP-1Methyl SiliconeHP-5
Column length (m) 30.30. 25.30.
Carrier gas HeHeliumHeliumHeHelium
Substrate      
Column diameter (mm) 0.250.25 0.250.32
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.60.60.90.60.
Tend (C) 260.260.220.220.260.
Heat rate (K/min) 4.3.5.7.5.
Initial hold (min)    2.2.
Final hold (min)   6. 13.
I 1576.1580.1564.1563.1580.
ReferenceIbanez and Usubillaga, 2006Javidnia, Miri, et al., 2006Kiran, Bhavani, et al., 2006Kitchlu, Bakshi, et al., 2006Kucuk, Gulec, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-1HP-5CP Sil 5 CBCP Sil 5 CB5 % Phenyl methyl siloxane
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2N2Helium
Substrate      
Column diameter (mm) 0.320.250.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.100.50.50.60.
Tend (C) 300.240.300.200.280.
Heat rate (K/min) 4.5.4.5.3.
Initial hold (min)  2.   
Final hold (min)  5.  30.
I 1568.1576.1568.1578.1543.
ReferenceKula, Izydorczyk, et al., 2006Lago, Soares, et al., 2006Lis and Milczarek, 2006Martin, Joseph, et al., 2006Marongiu, Piras, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 220.220.260.220.265.
Heat rate (K/min) 4.4.4.4.2.5
Initial hold (min)  5.4.5.0.5
Final hold (min)      
I 1579.1580.1579.1581.1607.
ReferenceMorteza-Semnani, Akbarzadeh, et al., 2006Morteza-Semnani K., Akbarzadeh M., et al., 2006Morteza-Semnani, Saeedi, et al., 2006Morteza-Semnani K., Saeedi M., et al., 2006Nickavar B., Kamalinejad M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30DB-5DB-1HP-5MSHP-5
Column length (m) 30.25.50.30.30.
Carrier gas HeN2N2HeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.250.150.250.250.25
Tstart (C) 50.50.95.40.60.
Tend (C) 250.200.240.260.220.
Heat rate (K/min) 2.4.4.4.5.
Initial hold (min)  3.  10.
Final hold (min)      
I 1568.1575.1599.1583.1570.
ReferenceOrav, Raal, et al., 2006Ouamba, Ouabonzi, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006Petrovic, Ristic, et al., 2006Pintore G., Chessa M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSHP-5HP-5MS
Column length (m) 30.30.30.25.30.
Carrier gas HydrogenHydrogenHeH2 
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.70.60.60.50.
Tend (C) 280.280.280.240.250.
Heat rate (K/min) 4.4.3.3.10.
Initial hold (min) 4.4.  5.
Final hold (min)      
I 1576.1576.1545.1581.1590.
ReferencePino, Marbot, et al., 2006Pino, Marbot, et al., 2006Pitarokili, Tzakou, et al., 2006Potzernheim, Bizzo, et al., 2006Robinson, 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSDB-5DB-1DB-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.25 0.25
Tstart (C) 60.60.40.40.40.
Tend (C) 200.280.240.250.260.
Heat rate (K/min) 2.4.4.4.2.
Initial hold (min)     5.
Final hold (min) 60.   20.
I 1576.1579.1576.1560.1572.
ReferenceRout, Naik, et al., 2006Sajjadi, 2006Sefidkon and Jamzad, 2006Sefidkon, Jamzad, et al., 2006Senatore, Landolfi, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1SPB-5CP Sil 5 CBMethyl SiliconeHP-5
Column length (m) 60. 25.25.25.
Carrier gas HeliumHeH2N2H2
Substrate      
Column diameter (mm) 0.25 0.250.30.32
Phase thickness (mum) 0.25  0.150.52
Tstart (C) 60.50.50.50.50.
Tend (C) 250.250.230.210.280.
Heat rate (K/min) 5.5.3.2.2.5
Initial hold (min)  3. 5.5.
Final hold (min) 10.15.   
I 1570.1576.1567.1600.1583.
ReferenceSonboli, Mirjalili, et al., 2006Stojanovic, Palic, et al., 2006Tesso, König, et al., 2006Tonzibo, Coffy, et al., 2006Wang, Kong, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-1DB-5DB-5HP-1
Column length (m) 30.50.30.30.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.2
Phase thickness (mum) 0.250.330.250.250.5
Tstart (C) 60.50.40.60.60.
Tend (C) 250.220.250.210.250.
Heat rate (K/min) 10.4.4.3.2.
Initial hold (min) 2.1. 5. 
Final hold (min) 10.10.  60.
I 1595.1558.1562.1574.1564.
ReferenceWang, Yang, et al., 2006Wong, Lim, et al., 2006Yadegarinia, Gachkar, et al., 2006Askari and Sefidkon, 2005Bendimerad and Bendiab, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5CP Sil 8 CBDB-1
Column length (m) 50.30.25.30.60.
Carrier gas  HeHeHeN2
Substrate      
Column diameter (mm) 0.30.250.20.250.25
Phase thickness (mum) 0.250.250.330.250.25
Tstart (C) 60.60.60.80.60.
Tend (C) 240.240.240.200.250.
Heat rate (K/min) 2.3.3.3.5.
Initial hold (min)    5. 
Final hold (min)   7.5.10.
I 1579.1577.1572.1577.1578.
ReferenceChagonda and Chalchat, 2005Chaverri and Cicció, 2005Duarte, Figueira, et al., 2005Facey, Porter, et al., 2005Fakhari A.R., Sonboli A., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5CP Sil 5 CBCP Sil 5 CB
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeN2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.60.60.
Tend (C) 300.30.300.250.250.
Heat rate (K/min) 3.4.5.5.5.
Initial hold (min) 3.3.5.  
Final hold (min)  15.5.10.10.
I 1573.1577.1578.1578.1580.
ReferenceFerraz, Limberger, et al., 2005Ferretti, Maggi, et al., 2005Figuérédo, Cabassu, et al., 2005Jassbi, Mehrdad, et al., 2005Jassbi, Mehrdad, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1DB-1DB-5DB-5
Column length (m) 25.30.30.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.320.32
Phase thickness (mum) 0.520.250.25  
Tstart (C) 40.50.50.60.60.
Tend (C) 240.265.265.240.240.
Heat rate (K/min) 4.2.52.53.3.
Initial hold (min)  1.1.  
Final hold (min)  20.30.  
I 1571.1562.1553.1571.1573.
ReferenceJovanovic, Kitic, et al., 2005Khanavi, Ghasemian, et al., 2005Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005Khayyat and Karimi, 2005Khayyat and Karimi, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5MS
Column length (m) 30.30.30.30.30.
Carrier gas He HeliumHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 60.35.35.60.60.
Tend (C) 240.280.280.230.280.
Heat rate (K/min) 3.4.4.3.3.
Initial hold (min)  2.2. 30.
Final hold (min)      
I 1579.1588.1588.1569.1545.
ReferenceKhayyat and Karimi, 2005Kowalski and Wolski, 2005Kowalski, 2005Limberger, Sobral, et al., 2005Marongiu, Piras, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5CP Sil 5 CBCP Sil 5 CBHP-5
Column length (m) 30.30.25.25.30.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.150.150.25
Tstart (C) 60.60.50.50.70.
Tend (C) 220.220.230.230.240.
Heat rate (K/min) 4.4.3.3.5.
Initial hold (min) 5.5.   
Final hold (min)      
I 1578.1578.1579.1573.1577.
ReferenceMorteza-Semnani, Akbarzadeh, et al., 2005Morteza-Semnani, Akbarzadeh, et al., 2005, 2Ogunwande, Olawore, et al., 2005Olawore, Ogunwande, et al., 2005Oyedeji, Yani, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5MSHP-5HP-5MS
Column length (m) 50.50.30.30.30.
Carrier gas N2N2 HeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.25  0.25
Tstart (C) 95.95.60.60.60.
Tend (C) 240.240.280.240.220.
Heat rate (K/min) 4.4.3.5.6.
Initial hold (min)     3.
Final hold (min)      
I 1576.1576.1578.1575.1596.
ReferencePalá-Paúl, Pérez-Alonso, et al., 2005Pala-Paul, Perez-Alonso, et al., 2005Petrakis, Roussis, et al., 2005Saeidnia, Gohari, et al., 2005Safaei-Ghomi, Bamoniri, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSHP-5MSDB-5DB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.50.
Tend (C) 280.275.280.220.265.
Heat rate (K/min) 4.4.4.3.2.5
Initial hold (min)    4.1.
Final hold (min)     20.
I 1578.1578.1576.1580.1543.
ReferenceSajjadi S.E. and Eskandari B., 2005Sajjadi and Ghannadi, 2005Sajjadi, 2005Salehi, Sefidkon, et al., 2005Sarkhail, Amin, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5HP-5MSDB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 240.260.280.300.300.
Heat rate (K/min) 4.2.3.3.3.
Initial hold (min)  5.5.  
Final hold (min)  20.   
I 1575.1572.1576.1571.1571.
ReferenceSefidkon and Jamzad, 2005Senatore, Apostolides Arnold, et al., 2005Setzer, Noletto, et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005Simoes-Pires C.A., Debenedetti S., et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSRTX-1DB-1DB-5
Column length (m) 30.30.60.60.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.40.
Tend (C) 300.280.25.250.210.
Heat rate (K/min) 3.3.5.5.2.
Initial hold (min)     2.
Final hold (min)   10.10.33.
I 1572.1572.1574.1571.1578.
ReferenceSimoes-Pires C.A., Debenedetti S., et al., 2005Slavkovska, Couladis, et al., 2005Sonboli, Salehi, et al., 2005Sonboli, Salehi, et al., 2005, 2Stevanovic, Garneau, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBHP-5 MSHP-5MSDB-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum)  0.500.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 290.260.280.280.240.
Heat rate (K/min) 3.3.3.3.3.
Initial hold (min) 5.    
Final hold (min)  20.   
I 1567.1579.1543.1558.1578.
ReferenceSuárez, Vásquez, et al., 2005Topçu, Barla, et al., 2005Tzakou, Bazos, et al., 2005Tzakou and Constantinidis, 2005Urdampilleta, Amat, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-5CP Sil 5 CBDB-1
Column length (m) 30.30.30.30.30.
Carrier gas  HeH2N2N2
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.50.50.50.
Tend (C) 220.260.290.200.200.
Heat rate (K/min) 3.5.4.5.5.
Initial hold (min) 5.2.   
Final hold (min) 10.13.   
I 1571.1579.1576.1574.1574.
ReferenceVichi, Riu-Aumatell, et al., 2005Yayli, Yasar, et al., 2005Abreu, Reis, et al., 2004Agnaniet, Menut, et al., 2004Fekam Boyom, Fotio, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5DB-5RTX-1
Column length (m) 30.25.25.60.30.
Carrier gas N2 NitrogenHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.40.60.
Tend (C) 230.180.240.280.300.
Heat rate (K/min) 2.3.3.4.4.
Initial hold (min)  10. 4. 
Final hold (min)  10.   
I 1576.1575.1577.1577.1568.
ReferenceGonzález, Guerra, et al., 2004bin Jantan, Ayop, et al., 2004JAvidnia, Mojab, et al., 2004Kalvandi, Sefidkon, et al., 2004Kalemba and Thiem, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-5DB-5MSDB-5RTX-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 260.300.240.300.300.
Heat rate (K/min) 2.3.3.3.4.
Initial hold (min) 5.    
Final hold (min)      
I 1568.1556.1576.1572.1567.
ReferenceKilic, Hafizoglu, et al., 2004Lago, de Ávila, et al., 2004paz Lima, Silva, et al., 2004Limberger, Sobral, et al., 2004Lis, Boczek, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSHP-5MSHP-5MSBP-1
Column length (m) 30.30.30.30.25.
Carrier gas  HeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.60.60.
Tend (C) 210.280.280.280.220.
Heat rate (K/min) 2.3.3.3.5.
Initial hold (min) 2.    
Final hold (min) 33.    
I 1574.1586.1573.1574.1572.
ReferenceLopez Arze, Collin, et al., 2004Malencic, Couladis, et al., 2004Malencic, Couladis, et al., 2004Malencic, Couladis, et al., 2004Mallavarapu, Kulkarni, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-1DB-5DB-1
Column length (m) 30.30.60.30.50.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (mum) 0.250.150.250.250.25
Tstart (C) 60.60.50.35.70.
Tend (C) 275.220.270.220.220.
Heat rate (K/min) 4.3.4.3.4.
Initial hold (min)  3.   
Final hold (min)      
I 1590.1575.1560.1579.1568.
ReferenceMehrabani, Asadipour, et al., 2004Mevy, Bessiere, et al., 2004Nik, Mirza, et al., 2004Palá-Paúl, Brophy, et al., 2004Palá-Paúl, García-Jiménez, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase NB-30DB-5HP-5MSDB-5HP-1
Column length (m) 50.30.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.200.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.33
Tstart (C) 50.35.60.50.40.
Tend (C) 250.220.280.250.260.
Heat rate (K/min) 2.2.54.3.2.
Initial hold (min)    5.5.
Final hold (min)  6.  20.
I 1572.1578.1578.1576.1574.
ReferenceRaal, Paaver, et al., 2004Rohloff, Mordal, et al., 2004Sajjadi and Shahpiri, 2004Sefidkon, Jamzad, et al., 2004Senatore, Napolitano, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5CP Sil 5 CBBPX-5DB-5
Column length (m) 30.30.20.25.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.220.25
Phase thickness (mum) 0.250.250.251.0.25
Tstart (C) 40.60.100.60.60.
Tend (C) 250.300.270.250.240.
Heat rate (K/min) 2.3.8.3.4.
Initial hold (min) 5. 2.5. 
Final hold (min) 20.  10. 
I 1575.1567.1575.1612.1570.
ReferenceSenatore, Rigano, et al., 2004Suyenaga, Apel, et al., 2004Thappa, Bakshi, et al., 2004Vilaseca, Guy, et al., 2004Cabanillas, Lopez, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSDB-1HP-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 100.60.50.60.60.
Tend (C) 240.220.200.275.280.
Heat rate (K/min) 5.5.5.4.4.
Initial hold (min) 2.20.   
Final hold (min) 5.20.   
I 1576.1582.1551.1580.1576.
ReferenceChaves, Lago, et al., 2003Feizbaksh, Saber Tehrani, et al., 2003Fekam Boyom, Ngouana, et al., 2003Ghannadi, Aghazari, et al., 2003Ghasemi, Asghari, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5Methyl SiliconeRSL-200RSL-200
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeH2H2
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.40.
Tend (C) 280.275.250.280.280.
Heat rate (K/min) 4.4.2.6.6.
Initial hold (min)   2.5.5.
Final hold (min)   5.5.5.
I 1568.1586.1555.1573.1562.
ReferenceGhassemi, Sajjadi, et al., 2003Ghannadi and Zolfaghari, 2003Jayaprakasha, Rao, et al., 2003Jirovetz, Buchbauer, et al., 2003Jirovetz, Buchbauer, et al., 2003, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CP Sil 5 CBCP Sil 5 CBDB-5DB-5
Column length (m) 50.25.25.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum) 0.250.250.390.250.25
Tstart (C) 50.35.60.60.60.
Tend (C) 220.280.220.280.250.
Heat rate (K/min) 3.5.5.5.3.
Initial hold (min) 2.2.5   
Final hold (min) 10.    
I 1575.1557.1568.1568.1573.
ReferenceJuteau, Jerkovic, et al., 2003Kanjilal, Kotoky, et al., 2003Khanavi, Hadjiakhoondi, et al., 2003Lago, de Ávila, et al., 2003Limberger, Simões-Pires, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5CP Sil 5 CBZB-1DB-1
Column length (m) 30.50.25.30.60.
Carrier gas HeHe N2He
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.250.250.390.250.25
Tstart (C) 60.50.60.45.50.
Tend (C) 240.220.220.230.270.
Heat rate (K/min) 3.3.5.3.4.
Initial hold (min)  2.   
Final hold (min)      
I 1581.1574.1570.1561.1560.
ReferenceMaia, Taveira, et al., 2003Masotti, Juteau, et al., 2003Mazloomifar, Saber-Tehrani, et al., 2003Mierendorff, Stahl-Biskup, et al., 2003Mirza and Nik, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5DB-5DB-5HP-5
Column length (m) 60.30.30.30.30.
Carrier gas HeHeliumH2H2He
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 50.70.60.60.60.
Tend (C) 270.210.280.280.280.
Heat rate (K/min) 4.2.4.4.3.
Initial hold (min)   10.10. 
Final hold (min)  60.40.40. 
I 1560.1575.1576.1576.1557.
ReferenceMirza, Nik, et al., 2003Mookdasanit, Tamura, et al., 2003Pino, Marbot, et al., 2003Pino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5NB-30DB-1DB-5Methyl Silicone
Column length (m) 30.50.60.30. 
Carrier gas HeHeHeN2He
Substrate      
Column diameter (mm) 0.20.20.250.25 
Phase thickness (mum) 0.250.50.250.25 
Tstart (C) 75.50.40.40.35.
Tend (C) 220.250.220.230.180.
Heat rate (K/min) 3.2.4.2.4.
Initial hold (min) 4.    
Final hold (min)      
I 1578.1570.1568.1576.1556.
ReferencePriestap, van Baren, et al., 2003Raal, Arak, et al., 2003Rasooli and Mirmostafa, 2003Rotman, Ahumada, et al., 2003Santos and Cordeiro, 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5Cross-Linked MethylsiliconeHP-5
Column length (m) 60.30.60.25.25.
Carrier gas HeHe HeHelium
Substrate      
Column diameter (mm) 0.250.250.250.20.32
Phase thickness (mum) 0.250.250.250.330.53
Tstart (C) 40.60.40.70.40.
Tend (C) 260.240.250.250.280.
Heat rate (K/min) 4.3.5.4.4.
Initial hold (min) 5. 15.  
Final hold (min)      
I 1558.1580.1576.1556.1573.
ReferenceSefidkon, Naderi Nik, et al., 2003da Silva, Luz, et al., 2003Stashenko, Jaramillo, et al., 2003Velasco-Negueruela, Pérez-Alonso, et al., 2003Velickovic, Ristic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5DB-5DB-5
Column length (m) 25.25.30.30.25.
Carrier gas HeliumHeliumHeHeN2
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (mum) 0.530.530.320.250.25
Tstart (C) 40.40.60.60.50.
Tend (C) 280.280.250.240.250.
Heat rate (K/min) 4.4.5.3.4.
Initial hold (min)   30.  
Final hold (min)     10.
I 1574.1578.1581.1579.1576.
ReferenceVelickovic, Ristic, et al., 2003Velickovic, Ristic, et al., 2003Yassa, Akhani, et al., 2003Zoghbi, Andrade, et al., 2003Zrira, Elamrani, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1CP Sil 5 CBOV-101DB-55 % Phenyl methyl siloxane
Column length (m) 60.25.25.30.30.
Carrier gas HeN2 HeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.4 0.250.25
Tstart (C) 50.60.50.60.75.
Tend (C) 280.260.200.280.200.
Heat rate (K/min) 4.5.5.3.3.
Initial hold (min)     4.
Final hold (min)  40. 30.8.
I 1560.1563.1573.1563.1578.
ReferenceAhmadi, Mirza, et al., 2002Azaz. D., Demirci, et al., 2002Boyom, Keumedjio, et al., 2002Caredda, Marongiu, et al., 2002Cicció and Gómez-Laurito, 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1DB-5HP-5DB-5DB-1
Column length (m) 25.30.30.30.30.
Carrier gas N2N2N2HeH2
Substrate      
Column diameter (mm) 0.500.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.50.60.40.
Tend (C) 220.250.250.240.245.
Heat rate (K/min) 5.4.4.3.3.
Initial hold (min)   5. 20.
Final hold (min) 10.    
I 1570.1576.1576.1578.1560.
ReferenceDas, Ram, et al., 2002Farah, Fechtal, et al., 2002Farah, Fechtal. M., et al., 2002Flamini, Ertugrul, et al., 2002Gancel, Ollé, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PTE-5SE-30RSL-200RSL-200CP Sil 8 CB
Column length (m) 60.50.30.30.30.
Carrier gas H2HeH2H2He
Substrate      
Column diameter (mm) 0.320.250.320.320.25
Phase thickness (mum) 0.300.250.250.250.25
Tstart (C) 60.70.40.50.50.
Tend (C) 285.240.280.280.220.
Heat rate (K/min) 4.34.6.6.3.
Initial hold (min)   5.5.2.
Final hold (min)   5.5. 
I 1576.1571.1619.1619.1575.
ReferenceGudzic, Djokovic, et al., 2002Iñigo, Palá-Paúl, et al., 2002Jirovetz, Buchbauer, et al., 2002Jirovetz, Ngassoum, et al., 2002Juteau, Masotti, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5OV-101DB-5HP-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.35.50.60.60.
Tend (C) 240.280.200.250.275.
Heat rate (K/min) 3.3.5.3.4.
Initial hold (min)  2.  4.
Final hold (min)  15.   
I 1577.1588.1574.1573.1571.
ReferenceKobaisy, Tellez, et al., 2002Krauze-Baranowska, Mardarowicz, et al., 2002Kuiate, Bessière, et al., 2002Limberger, Simões-Pires, et al., 2002Lockwood, Asghari, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5MSCP Sil 5 CBDB-5HP-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.390.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 240.240.220.220.240.
Heat rate (K/min) 3.3.5.4.3.
Initial hold (min)    5. 
Final hold (min)      
I 1579.1578.1565.1578.1585.
ReferenceMaia, da Silva, et al., 2002Maia, Zoghbi, et al., 2002Mojab, Rustaiyan, et al., 2002Morteza-Semnani, Saeedi, et al., 2002Novak, Langbehn, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1HP-1DB-5DB-1
Column length (m) 30.50.50.25.60.
Carrier gas  N2N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.20.25
Phase thickness (mum) 0.250.250.25  
Tstart (C) 60.80.90.60.40.
Tend (C) 240.225.220.220.250.
Heat rate (K/min) 3.4.3.3.4.
Initial hold (min)      
Final hold (min)      
I 1587.1557.1570.1574.1555.
ReferenceNovak, Langbehn, et al., 2002Palá-Paúl, Pérez-Alonso, et al., 2002Priestap, van Baren, et al., 2002Schwob, Bessière, et al., 2002Sefidkon, Dabiri, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-5MSDB-5DB-1
Column length (m) 60.60.30.30.60.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.248
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 280.280.270.240.220.
Heat rate (K/min) 4.4.3.3.3.
Initial hold (min) 5.5.  5.
Final hold (min)     22.
I 1562.1562.1577.1578.1579.
ReferenceSefidkon, Jalili, et al., 2002Sefidkon, 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2Bailac, Dellacasa, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSSPB-5HP-5BP-1Optima-5
Column length (m) 30.60.30.30.30.
Carrier gas HeHeN2N2He
Substrate      
Column diameter (mm) 0.250.320.250.250.2
Phase thickness (mum) 0.25 0.250.25 
Tstart (C) 60.40.60.60.50.
Tend (C) 240.220.220.220.250.
Heat rate (K/min) 3.3.5.5.3.
Initial hold (min)  5.10. 3.
Final hold (min)  15.   
I 1567.1585.1577.1571.1584.
ReferenceCherchi, Deidda, et al., 2001Cornu, Carnat, et al., 2001Gallori, Flamini, et al., 2001Gupta, Mallavarapu, et al., 2001Jacquemond-Collet, Bessière, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200RTX-1CBP-1DB-5MSDB-1
Column length (m) 30.30.25.30.60.
Carrier gas H2N2NitrogenHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.50.60.50.
Tend (C) 280.300.210.240.270.
Heat rate (K/min) 6.4.3.3.4.
Initial hold (min) 5. 2.  
Final hold (min) 5.  30. 
I 1618.1569.1615.1565.1559.
ReferenceJirovetz L., Buchbauer G., et al., 2001Kalemba, Marschall, et al., 2001Ly, Yamauchi, et al., 2001Marongiu, Porcedda, et al., 2001Mirza, Ahmadi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5DB-1DB-1PTE-5
Column length (m) 50.30.30.30.60.
Carrier gas HeHeN2HeH2
Substrate      
Column diameter (mm) 0.20.250.250.20.32
Phase thickness (mum) 0.50.250.25 0.3
Tstart (C) 50.60.80.60.60.
Tend (C) 250.270.225.240.285.
Heat rate (K/min) 2.3.4.3.4.3
Initial hold (min)      
Final hold (min)      
I 1558.1580.1545.1577.51576.
ReferenceOrav, Kailas, et al., 2001Palmeira, Conserva, et al., 2001Palá-Paúl, Pérez-Alonso, et al., 2001Santos, Moreira, et al., 2001Stojanovic, Palic, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1DB-1HP-1BP-1
Column length (m) 25.60.25.60.25.
Carrier gas  N2NitrogenHeN2
Substrate      
Column diameter (mm) 0.250.250.500.250.33
Phase thickness (mum) 0.150.250.250.251.0
Tstart (C) 50.60.60.60.60.
Tend (C) 230.220.220.200.275.
Heat rate (K/min) 3.3.5.4.4.
Initial hold (min)  5. 5. 
Final hold (min)  22. 25. 
I 1579.1581.1570.1587.1575.
ReferenceAsekun and Ekundayo, 2000Bailac, Dellacasa, et al., 2000Mallavarapu, Rao, et al., 2000Meccia, Rojas, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5OV-101DB-1RTX-1
Column length (m) 30.30.25.60.30.
Carrier gas HeHeN2N2N2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 60.40.50.75.60.
Tend (C) 275.240.200.220.300.
Heat rate (K/min) 4.3.5.4.4.
Initial hold (min)  5. 1. 
Final hold (min)    8. 
I 1572.1582.1573.1579.1568.
ReferenceMohagheghzadeh, Shams-Ardakani, et al., 2000, 2Novak, Novak, et al., 2000Ayedoun, Adéoti, et al., 1999Bailac, Dellacasa, et al., 1999Kalemba, 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CBP-1CP Sil 5 CBDB-1DB-5CP Sil 5 CB
Column length (m) 25.25.50.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.30.250.250.250.25
Phase thickness (mum)   0.250.250.39
Tstart (C) 60.50.70.40.60.
Tend (C) 240.230.240.250.220.
Heat rate (K/min) 4.3.4.2.5.
Initial hold (min)    5.5.
Final hold (min)    60.20.
I 1570.1550.1545.1553.1569.
ReferenceLabuckas, Zygadlo, et al., 1999Oyedeji, Olawore, et al., 1999Palá-Paúl, Pérez-Alonso, et al., 1999Porta, Porcedda, et al., 1999Rustaiyan, Masoudi, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-5CP Sil 5 CB
Column length (m) 60.60.60.30.25.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.320.25 
Phase thickness (mum) 0.250.25 0.250.39
Tstart (C) 40.50.60.60.60.
Tend (C) 280.220.230.240.220.
Heat rate (K/min) 4.4.3.3.5.
Initial hold (min) 5.    
Final hold (min)   5.  
I 1571.1568.1568.1575.1571.
ReferenceSefidkon, Dabiri, et al., 1999Sefidkon and Mirza, 1999Shafiee, Javidnia, et al., 1999Tellez, Canel, et al., 1999Weyerstahl, Marschall, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SPB-5DB-5OV-1CBP-1
Column length (m) 30.50.30.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.320.25
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 60.60.60.50.60.
Tend (C) 240.240.240.250.240.
Heat rate (K/min) 3.3.3.10.4.
Initial hold (min)    5. 
Final hold (min)  20. 20. 
I 1576.1587.1576.1567.1576.
ReferenceZoghbi, Andrade, et al., 1999Doneanu and Anitescu, 1998El-Sakhawy, El-Tantawy, et al., 1998Kökdil, Kurucu, et al., 1998Lamarque, Maestri, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5OV-101DB-5DB-5
Column length (m) 30.30.25.30.30.
Carrier gas HeHelium HeHelium
Substrate      
Column diameter (mm) 0.250.250.320.320.25
Phase thickness (mum) 0.250.25  0.25
Tstart (C) 60.60.50.60.60.
Tend (C) 240.240.200.250.240.
Heat rate (K/min) 3.3.5.3.3.
Initial hold (min)      
Final hold (min)      
I 1579.1579.1573.1577.1576.
ReferenceMaia, Zohhbi, et al., 1998Santos, Andrade, et al., 1998Zollo, Biyiti, et al., 1998Abreu and Noronha, 1997Tellez, Estell, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5CBP-1DB-5DB-5SPB-1
Column length (m) 30.25.30.30.50.
Carrier gas HeHe  He
Substrate      
Column diameter (mm) 0.250.220.250.250.2
Phase thickness (mum)   0.25 0.33
Tstart (C) 60.60.60.40.40.
Tend (C) 240.240.300.210.200.
Heat rate (K/min) 4.5.4.2.3.
Initial hold (min)   2.2.3.
Final hold (min)   5.33.30.
I 1570.1570.1576.71574.1563.
ReferenceZunino, Novillo-Newton, et al., 1997Zygadlo, Ariza-Espinar, et al., 1997Gawdzik, Mardarowicz, et al., 1996Sohounhloue, Dangou, et al., 1996Wong and Lai, 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-101SE-54DB-1CP Sil 8 CBBP-1
Column length (m) 50.30.30.25.50.
Carrier gas H2HydrogenN2 H2
Substrate      
Column diameter (mm) 0.320.25 0.200.30
Phase thickness (mum) 0.30.25   
Tstart (C) 65.60.80.60.40.
Tend (C) 300.250.220.230.250.
Heat rate (K/min) 2.2.4.3.10.
Initial hold (min) 5.5. 10.1.
Final hold (min)  2.   
I 1556.1569.1595.1589.1573.
ReferenceDemarne and van der Walt, 1993Kollmannsberger, Nitz, et al., 1992Velasco-Negueruela, Pérez Alonso, et al., 1991Jantan and Goh, 1990Brophy, Davies, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase DB-1
Column length (m) 10.
Carrier gas H2
Substrate  
Column diameter (mm) 0.25
Phase thickness (mum) 0.25
Tstart (C) 50.
Tend (C) 250.
Heat rate (K/min) 5.
Initial hold (min)  
Final hold (min)  
I 1555.
ReferencePerry, Baxter, et al., 1986
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Maia, Zoghbi, et al., 2002
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Sefidkon, 2002
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Bailac, P.N.; Dellacasa, A.D.; Bernasconi, H.O.; Ponzi, M.I.; Firpo, N.H., Essential oil of female plants of Baccharis coridifolia De Candole, J. Essent. Oil Res., 2001, 13, 1, 23-24, https://doi.org/10.1080/10412905.2001.9699593 . [all data]

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Cornu, A.; Carnat, A.-P.; Martin, B.; Coulon, J.-B.; Lamaison, J.-L.; Berdagué, J.-L., Solid-phase microextraction of volatile components from natural grassland plants, J. Agric. Food Chem., 2001, 49, 1, 203-209, https://doi.org/10.1021/jf0008341 . [all data]

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Gallori, S.; Flamini, G.; Bilia, A.R.; Morelli, I.; Landini, A.; Vincieri, F.F., Chemical composition of some traditional herbal drug preparations: essential oil and aromatic water of costmary (Balsamita suaveolens Pers.), J. Agric. Food Chem., 2001, 49, 12, 5907-5910, https://doi.org/10.1021/jf0107656 . [all data]

Gupta, Mallavarapu, et al., 2001
Gupta, R.; Mallavarapu, G.R.; Banerjee, S.; Kumar, S., Characteristics of an isomenthone-rich somaclonal mutant isolated in a geraniol-rich rose-scented geranium accession of Pelargonium graveolens, Flavour Fragr. J., 2001, 16, 5, 319-324, https://doi.org/10.1002/ffj.1002 . [all data]

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Jacquemond-Collet, I.; Bessière, J.-M.; Hannedouche, S.; Bertrand, C.; Fourasté, I.; Moulis, C., Identification of the alkaloids of Galipea officinalis by gas chromatography-mass spectrometry, Phytochem. Anal., 2001, 12, 5, 312-319, https://doi.org/10.1002/pca.594 . [all data]

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Jirovetz L.; Buchbauer G.; Shafi P.M.; Rosamma M.K.; Geissler M., Analysis of the composition and aroma of the essential leaf oil of Syzygium travancoricum from South India by GC-FID, GC-MS, and olfactometry. Seasonal changes of composition, Chromatographia Sup., 2001, 53, S1, s372-s374, https://doi.org/10.1007/BF02490359 . [all data]

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Kalemba, D.; Marschall, H.; Bradesi, P., Constituents of the essential oil of Solidago gigantea Ait. (giant goldenrod), Flavour Fragr. J., 2001, 16, 1, 19-26, https://doi.org/10.1002/1099-1026(200101/02)16:1<19::AID-FFJ940>3.0.CO;2-U . [all data]

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Ly, T.N.; Yamauchi, R.; KAto, K., Volatile components of the essential oils in Galanga (Alpina officinarum Hance) from Vietnam, Food Sci. Technol. Res., 2001, 7, 4, 303-306, https://doi.org/10.3136/fstr.7.303 . [all data]

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Mirza, M.; Ahmadi, L.; Tayebi, M., Volatile constituents of Hymenocrater incanus Bunge, an Iranian endemic species, Flavour Fragr. J., 2001, 16, 4, 239-240, https://doi.org/10.1002/ffj.983 . [all data]

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Palmeira, Conserva, et al., 2001
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Santos, P.R.; Moreira, D.L.; Guimaraes, E.F.; Kaplan, M.A.C., Essential oil analysis of 10 piperaceae species from the Brazilian Atlantic forest, Phytochemistry, 2001, 58, 4, 547-551, https://doi.org/10.1016/S0031-9422(01)00290-4 . [all data]

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Asekun and Ekundayo, 2000
Asekun, O.T.; Ekundayo, O., Essential oil constituents of Hyptis suaveolens (L.) Poit. (Bush tea) leaves from Nigeria, J. Essent. Oil Res., 2000, 12, 227-230. [all data]

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Notes

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