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2-Hexenal, (E)-


Kovats' RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10DB-WaxDB-WaxDB-Wax
Column length (m) 60.60.60.60.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum)   0.250.250.25
Tstart (C) 40.35.40.40.40.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min) 2.5.5.5.5.
Final hold (min)  20.   
I 1216.1225.1219.1219.1218.
ReferenceUmano, Hagi, et al., 1994Wong and Teng, 1994Tatsuka, Suekane, et al., 1990Tatsuka, Suekane, et al., 1990Tatsuka, Suekane, et al., 1990
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxCarbowax 20MDB-WaxDB-WaxDB-Wax
Column length (m) 60.50.60.30.30.
Carrier gas He HeN2N2
Substrate      
Column diameter (mm) 0.250.220.250.250.25
Phase thickness (mum) 0.25    
Tstart (C) 40.80.40.60.60.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 3.2.2.2.2.
Initial hold (min) 5. 10.10.10.
Final hold (min)      
I 1219.1222.1212.1228.1222.
ReferenceTatsuka, Suekane, et al., 1990Nishimura, Yamaguchi, et al., 1989Umano and Shibamoto, 1987Umano, Shoji, et al., 1986Umano, Shoji, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 59.150.70.70.
Carrier gas  HeN2N2
Substrate     
Column diameter (mm) 0.250.640.280.28
Phase thickness (mum)     
Tstart (C) 70.50.80.80.
Tend (C) 190.170.200.200.
Heat rate (K/min) 1.1.2.2.
Initial hold (min)  30.  
Final hold (min)     
I 1234.1230.1205.1208.
ReferencePalma-Fleming and Kepner, 1983Buttery, Kamm, et al., 1982Yamaguchi and Shibamoto, 1981Yamaguchi and Shibamoto, 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Umano, Hagi, et al., 1994
Umano, K.; Hagi, Y.; Tamura, T.; Shoji, A.; Shibamoto, T., Identification of volatile compounds isolated from round kumquat (Fortunella japonica Swingle), J. Agric. Food Chem., 1994, 42, 9, 1888-1890, https://doi.org/10.1021/jf00045a011 . [all data]

Wong and Teng, 1994
Wong, K.C.; Teng, Y.E., Volatile Components of Mimusops elengi L. Flowers, J. Essent. Oil Res., 1994, 6, 5, 453-458, https://doi.org/10.1080/10412905.1994.9698425 . [all data]

Tatsuka, Suekane, et al., 1990
Tatsuka, K.; Suekane, S.; Sakai, Y.; Sumitani, H., Volatile constituents of kiwi fruit flowers: simultaneous distillation and extraction versus headspace sampling, J. Agric. Food Chem., 1990, 38, 12, 2176-2180, https://doi.org/10.1021/jf00102a015 . [all data]

Nishimura, Yamaguchi, et al., 1989
Nishimura, O.; Yamaguchi, K.; Mihara, S.; Shibamoto, T., Volatile Constituents of Guava Fruits (Psidium guajava L.) and Canned Puree, J. Agric. Food Chem., 1989, 37, 1, 139-142, https://doi.org/10.1021/jf00085a033 . [all data]

Umano and Shibamoto, 1987
Umano, K.; Shibamoto, T., Analysis of headspace volatiles from overheated beef fat, J. Agric. Food Chem., 1987, 35, 1, 14-18, https://doi.org/10.1021/jf00073a004 . [all data]

Umano, Shoji, et al., 1986
Umano, K.; Shoji, A.; Hagi, Y.; Shibamoto, T., Volatile constituents of peel of quince fruit, Cydonia oblonga Miller, J. Agric. Food Chem., 1986, 34, 4, 593-596, https://doi.org/10.1021/jf00070a003 . [all data]

Palma-Fleming and Kepner, 1983
Palma-Fleming, H.A.; Kepner, R.E., Volatile components of California live oak, Quercus agrifolia, Phytochemistry, 1983, 22, 6, 1503-1505, https://doi.org/10.1016/S0031-9422(00)84047-9 . [all data]

Buttery, Kamm, et al., 1982
Buttery, R.G.; Kamm, J.A.; Ling, L.C., Volatile components of alfalfa flowers and pods, J. Agric. Food Chem., 1982, 30, 4, 739-742, https://doi.org/10.1021/jf00112a028 . [all data]

Yamaguchi and Shibamoto, 1981
Yamaguchi, K.; Shibamoto, T., Volatile constituents of green tea, Gyokuro (Camellia sinensis L. var Yabukita), J. Agric. Food Chem., 1981, 29, 2, 366-370, https://doi.org/10.1021/jf00104a035 . [all data]


Notes

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