Hexanal
- Formula: C6H12O
- Molecular weight: 100.1589
- IUPAC Standard InChI: InChI=1S/C6H12O/c1-2-3-4-5-6-7/h6H,2-5H2,1H3
- IUPAC Standard InChIKey: JARKCYVAAOWBJS-UHFFFAOYSA-N
- CAS Registry Number: 66-25-1
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: n-Caproaldehyde; n-Hexanal; Caproaldehyde; Caproic aldehyde; Capronaldehyde; Hexaldehyde; n-C5H11CHO; 1-Hexanal; n-Hexaldehyde; n-Caproylaldehyde; Aldehyde C-6; Kapronaldehyd; UN 1207; Hexylaldehyde; n-Capronaldehyde; Hexan-1-al; Hexanaldehyde; NSC 2596
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Van Den Dool and Kratz RI, polar column, temperature ramp
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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax Etr | DB-Wax | HP-Innowax | DB-FFAP |
| Column length (m) | 30. | 30. | 60. | 60. | 30. |
| Carrier gas | He | He | He | ||
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.5 |
| Tstart (C) | 40. | 40. | 40. | 40. | 35. |
| Tend (C) | 200. | 250. | 200. | 250. | 225. |
| Heat rate (K/min) | 4. | 5. | 4. | 4. | 4. |
| Initial hold (min) | 1. | 3. | 1. | 2. | 5. |
| Final hold (min) | 10. | 15. | 10. | 10. | 30. |
| I | 1097. | 1080. | 1097. | 1081. | 1087. |
| Reference | Cho, Namgung, et al., 2008 | Aubert and Chanforan, 2007 | Cho I.H., Lee S.M., et al., 2007 | Hashizume M., Gordon M.H., et al., 2007 | Jarunrattanasri, Theerakulkait, et al., 2007 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-FFAP | FFAP | FFAP | FFAP | DB-Wax |
| Column length (m) | 30. | 30. | 30. | 30. | 30. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.32 |
| Phase thickness (μm) | 0.5 | 0.25 | 0.25 | 0.25 | 0.5 |
| Tstart (C) | 35. | 35. | 35. | 35. | 40. |
| Tend (C) | 225. | 225. | 225. | 225. | 240. |
| Heat rate (K/min) | 4. | 10. | 10. | 10. | 7. |
| Initial hold (min) | 5. | 5. | 5. | 5. | |
| Final hold (min) | 30. | 25. | 25. | 25. | 5. |
| I | 1089. | 1095. | 1095. | 1069. | 1088. |
| Reference | Jarunrattanasri, Theerakulkait, et al., 2007 | Lozano P.R., Drake M., et al., 2007 | Lozano P.R., Drake M., et al., 2007 | Lozano P.R., Miracle E.R., et al., 2007 | Mahattanatawee K., Perez-Cacho P.R., et al., 2007 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | HP-Innowax | DB-Wax | DB-FFAP |
| Column length (m) | 30. | 30. | 60. | 30. | 30. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | 0.32 |
| Phase thickness (μm) | 0.5 | 0.5 | 0.25 | 0.5 | 0.24 |
| Tstart (C) | 40. | 40. | 50. | 40. | 40. |
| Tend (C) | 250. | 250. | 220. | 240. | 240. |
| Heat rate (K/min) | 4. | 4. | 4. | 7. | 6. |
| Initial hold (min) | 5. | 5. | 4. | 2. | |
| Final hold (min) | 15. | 15. | 10. | 5. | 10. |
| I | 1077. | 1089. | 1084. | 1090. | 1074. |
| Reference | Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 2007 | Pozo-Bayon M.A., Ruiz-Rodriguez A., et al., 2007 | Quijano, Linares, et al., 2007 | Ruiz Perez-Cacho, Mahattanatawee, et al., 2007 | Scheidig, Czerny, et al., 2007 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | FFAP | Supelcowax-10 | DB-Wax Etr | DB-Wax | DB-Wax |
| Column length (m) | 30. | 30. | 30. | 60. | 60. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.32 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.5 | 0.25 | 0.25 | 0.25 | |
| Tstart (C) | 40. | 70. | 40. | 40. | 40. |
| Tend (C) | 240. | 220. | 250. | 200. | 200. |
| Heat rate (K/min) | 8. | 4. | 5. | 4. | 4. |
| Initial hold (min) | 2. | 7. | 3. | 1. | 1. |
| Final hold (min) | 5. | 20. | 15. | 10. | 10. |
| I | 1070. | 1099. | 1087. | 1085. | 1097. |
| Reference | Schlutt B., Moran N., et al., 2007 | Arena, Guarrera, et al., 2006 | Aubert C. and Pitrat M., 2006 | Cho, Choi, et al., 2006 | Cho, Kim, et al., 2006 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | CP-Wax 52CB | ZB-Wax | DB-Wax | CP-Wax 52CB |
| Column length (m) | 30. | 60. | 30. | 30. | 50. |
| Carrier gas | He | He | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | 0.32 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.15 | 0.5 | |
| Tstart (C) | 50. | 40. | 35. | 40. | 60. |
| Tend (C) | 230. | 250. | 220. | 240. | 220. |
| Heat rate (K/min) | 10. | 4. | 5. | 5. | 4. |
| Initial hold (min) | 5. | 5. | 5. | ||
| Final hold (min) | 25. | 10. | 10. | 30. | |
| I | 1080. | 1087. | 1064. | 1084. | 1072. |
| Reference | Fernandez-Segovia, Escriche, et al., 2006 | Kourkoutas, Elmore, et al., 2006 | Ledauphin, Basset, et al., 2006 | Lopez-Galilea I., Fournier N., et al., 2006 | Mahadevan and Farmer, 2006 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | CP-Wax 52CB | DB-Wax | DB-Wax | Supelcowax-10 |
| Column length (m) | 30. | 60. | 30. | 30. | 60. |
| Carrier gas | He | He | |||
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.5 | 0.25 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 50. | 35. | 40. | 40. | 35. |
| Tend (C) | 260. | 203. | 250. | 200. | 195. |
| Heat rate (K/min) | 4. | 3. | 3. | 10. | 6. |
| Initial hold (min) | 4. | 3. | 5. | ||
| Final hold (min) | 5. | 20. | 20. | 60. | |
| I | 1091. | 1076. | 1077. | 1051. | 1059. |
| Reference | Selli, Rannou, et al., 2006 | Alasalvar, Taylor, et al., 2005 | Berlinet, Ducruet, et al., 2005 | Carunchia Whetstine, Croissant, et al., 2005 | Chung, Fung, et al., 2005 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Stabilwax | Supelcowax-10 | DB-Wax | Supelcowax-10 | Carbowax 20M |
| Column length (m) | 60. | 60. | 30. | 30. | 60. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 40. | 40. | 40. | 60. | 45. |
| Tend (C) | 240. | 280. | 250. | 240. | 250. |
| Heat rate (K/min) | 3. | 4. | 3. | 3. | 2. |
| Initial hold (min) | 5. | 2. | 5. | 0.17 | |
| Final hold (min) | 10. | 20. | 10. | ||
| I | 1073. | 1097. | 1072. | 1105. | 1077. |
| Reference | Cros, Lignot, et al., 2005 | Elmore, Nisyrios, et al., 2005 | Gancel, Ollitrault, et al., 2005 | Riu-Aumatell, Lopez-Tamames, et al., 2005 | Verzera, Campisi, et al., 2005 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | ZB-Wax | DB-Wax | DB-Wax | DB-Wax |
| Column length (m) | 30. | 30. | 30. | 30. | 0. |
| Carrier gas | He | ||||
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.25 | 0.32 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.5 |
| Tstart (C) | 40. | 40. | 40. | 40. | 40. |
| Tend (C) | 200. | 250. | 200. | 200. | 240. |
| Heat rate (K/min) | 10. | 5. | 10. | 10. | 7. |
| Initial hold (min) | 3. | 2. | 5. | 5. | |
| Final hold (min) | 20. | 5. | 15. | 15. | 5. |
| I | 1048. | 1075. | 1073. | 1073. | 1087. |
| Reference | Whetstine, Cadwallader, et al., 2005 | Wu, Zorn, et al., 2005 | Avsar, Karagul-Yuceer, et al., 2004 | Avsar, Karagul-Yuceer, et al., 2004 | Gocmen, Gurbuz, et al., 2004 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | ZB-Wax | DB-Wax | DB-Wax Etr | DB-Wax | DB-Wax |
| Column length (m) | 30. | 30. | 30. | 30. | 30. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.15 | 0.5 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 35. | 40. | 40. | 45. | 45. |
| Tend (C) | 220. | 230. | 245. | 240. | 240. |
| Heat rate (K/min) | 1.8 | 5. | 3. | 6. | 6. |
| Initial hold (min) | 10. | 2. | 3. | 10. | 10. |
| Final hold (min) | 10. | 10. | 20. | 30. | 30. |
| I | 1064. | 1097. | 1075. | 1111. | 1111. |
| Reference | Ledauphin, Saint-Clair, et al., 2004 | Mahajan, Goddik, et al., 2004 | Ménager, Jost, et al., 2004 | Nielsen, Larsen, et al., 2004 | Nielsen, Larsen, et al., 2004, 2 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | DB-Wax | DB-Wax | DB-Wax |
| Column length (m) | 30. | 30. | 30. | 30. | 30. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.5 | 0.25 | 0.25 |
| Tstart (C) | 45. | 45. | 40. | 40. | 40. |
| Tend (C) | 240. | 240. | 240. | 200. | 200. |
| Heat rate (K/min) | 6. | 3. | 5. | 4. | 4. |
| Initial hold (min) | 10. | 10. | 5. | 5. | 5. |
| Final hold (min) | 30. | 30. | 20. | 20. | |
| I | 1111. | 1070. | 1083. | 1074. | 1074. |
| Reference | Nielsen, Larsen, et al., 2004, 3 | Nielsen and Poll, 2004 | Rega, Fournier, et al., 2004 | Yu, Kim, et al., 2004 | Yu, Kim, et al., 2004, 2 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | DB-Wax | Supelcowax | Supelcowax |
| Column length (m) | 30. | 30. | 30. | 25. | 25. |
| Carrier gas | He | He | |||
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.5 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 40. | 40. | 40. | 35. | 35. |
| Tend (C) | 200. | 245. | 250. | 225. | 225. |
| Heat rate (K/min) | 4. | 2. | 3. | 4. | 4. |
| Initial hold (min) | 5. | 3. | 5. | 5. | |
| Final hold (min) | 20. | 20. | 20. | 10. | 10. |
| I | 1072. | 1099. | 1063. | 1092. | 1092. |
| Reference | Yu, Kim, et al., 2004, 2 | Aubert, Günata, et al., 2003 | Brat, Rega, et al., 2003 | Chisholm, Wilson, et al., 2003 | Chisholm, Wilson, et al., 2003 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Stabilwax | DB-Wax | DB-Wax | DB-FFAP | DB-Wax |
| Column length (m) | 60. | 60. | 30. | 30. | 60. |
| Carrier gas | He | H2 | He | N2 | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.32 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.5 | 0.25 | 0.25 |
| Tstart (C) | 40. | 40. | 40. | 35. | 40. |
| Tend (C) | 240. | 245. | 240. | 200. | 210. |
| Heat rate (K/min) | 3. | 1.5 | 7. | 10. | 2. |
| Initial hold (min) | 5. | 5. | |||
| Final hold (min) | 10. | 20. | 5. | 30. | 40. |
| I | 1073. | 1072. | 1093. | 1077. | 1068. |
| Reference | Cros, Vandanjon, et al., 2003 | Gancel, Ollitrault, et al., 2003 | Högnadóttir and Rouseff, 2003 | Karagül-Yüceer, Vlahovich, et al., 2003 | Mau, Ko, et al., 2003 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | AT-Wax | DB-Wax | ZB-Wax |
| Column length (m) | 30. | 30. | 60. | 30. | 60. |
| Carrier gas | He | He | He | ||
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.32 | 0.32 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.5 | 0.25 |
| Tstart (C) | 40. | 35. | 65. | 35. | 40. |
| Tend (C) | 240. | 240. | 250. | 240. | 220. |
| Heat rate (K/min) | 6. | 6. | 2. | 5. | 3. |
| Initial hold (min) | 10. | 2. | 10. | 5. | |
| Final hold (min) | 30. | 6. | 60. | 5. | |
| I | 1111. | 1076. | 1062. | 1083. | 1067. |
| Reference | Nielsen, Larsen, et al., 2003 | Peterson and Reineccius, 2003 | Pino, Almora, et al., 2003 | Rega, Fournier, et al., 2003 | Brunton, Cronin, et al., 2002 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Supelcowax-10 | DB-Wax | AT-Wax | DB-Wax | Supelcowax-10 |
| Column length (m) | 60. | 30. | 60. | 30. | 60. |
| Carrier gas | He | He | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.32 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 1. | 0.25 |
| Tstart (C) | 35. | 35. | 65. | 40. | 35. |
| Tend (C) | 195. | 200. | 250. | 200. | 195. |
| Heat rate (K/min) | 2. | 10. | 2. | 10. | 2. |
| Initial hold (min) | 5. | 5. | 10. | 5. | 5. |
| Final hold (min) | 90. | 30. | 60. | 30. | 90. |
| I | 1086. | 1060. | 1062. | 1078. | 1086. |
| Reference | Chung, Yung, et al., 2002 | Karagül-Yüceer, Cadwallader, et al., 2002 | Pino, Marbot, et al., 2002 | Wu and Cadwallader, 2002 | Chung, Yung, et al., 2001 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | EC-WAX | DB-Wax | DB-Wax | DB-Wax | CP-Wax 52CB |
| Column length (m) | 30. | 60. | 60. | 60. | 50. |
| Carrier gas | He | He | He | He | H2 |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.25 | 0.25 | 0.25 | 0.32 |
| Phase thickness (μm) | 0.5 | 0.25 | 0.25 | 0.25 | |
| Tstart (C) | 40. | 40. | 40. | 40. | 50. |
| Tend (C) | 250. | 200. | 200. | 200. | 200. |
| Heat rate (K/min) | 5. | 2. | 2. | 2. | 2. |
| Initial hold (min) | 2. | 5. | |||
| Final hold (min) | 10. | 30. | |||
| I | 1092. | 1078. | 1083. | 1083. | 1071. |
| Reference | le Guen, Prost, et al., 2001 | Kim, 2001 | Lee, Suriyaphan, et al., 2001 | Lee, Suriyaphan, et al., 2001 | Liu, Yang, et al., 2001 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | AT-Wax | AT-Wax | DB-Wax | CP-Wax 52CB | DB-Wax |
| Column length (m) | 60. | 60. | 30. | 60. | 60. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.32 | 0.32 | 0.25 | 0.5 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.5 | 0.25 | 0.32 |
| Tstart (C) | 65. | 65. | 50. | 45. | 40. |
| Tend (C) | 250. | 250. | 250. | 250. | 290. |
| Heat rate (K/min) | 2. | 2. | 8. | 2. | 4. |
| Initial hold (min) | 10. | 10. | 0.17 | 2. | |
| Final hold (min) | 60. | 60. | 5. | ||
| I | 1067. | 1062. | 1088. | 1077. | 1086. |
| Reference | Pino and Marbot, 2001 | Pino, Marbot, et al., 2001 | Serot, Prost, et al., 2001 | Verzera, Campisi, et al., 2001 | Bartley and Jacobs, 2000 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | CP-Wax 52CB | DB-Wax | CP-Wax 52CB | DB-Wax |
| Column length (m) | 60. | 50. | 60. | 50. | 60. |
| Carrier gas | He | He | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.32 | 0.32 | 0.25 | 0.32 |
| Phase thickness (μm) | 0.5 | 0.5 | 0.2 | 0.5 | |
| Tstart (C) | 30. | 60. | 40. | 30. | 40. |
| Tend (C) | 160. | 220. | 250. | 220. | 250. |
| Heat rate (K/min) | 3. | 4. | 3. | 2. | 4. |
| Initial hold (min) | 5. | 5. | 1.3 | 2. | |
| Final hold (min) | 5. | 30. | 10. | 10. | |
| I | 1120. | 1092. | 1089. | 1069. | 1088. |
| Reference | Beauchene, Grua-Priol, et al., 2000 | Chevance, Farmer, et al., 2000 | le Guen, Prost, et al., 2000 | Jensen, Christensen, et al., 2000 | Le Guen, Prost, et al., 2000 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | HP-Wax | DB-Wax | CP-Wax 52CB |
| Column length (m) | 60. | 15. | 15. | 30. | 50. |
| Carrier gas | He | He | He | ||
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.53 | 0.53 | 0.32 | 0.32 |
| Phase thickness (μm) | 0.5 | 1. | 1. | 0.25 | |
| Tstart (C) | 40. | 40. | 40. | 40. | 60. |
| Tend (C) | 250. | 220. | 220. | 230. | 220. |
| Heat rate (K/min) | 4. | 5. | 5. | 3. | 4. |
| Initial hold (min) | 2. | 3. | 3. | 4. | 5. |
| Final hold (min) | 10. | 30. | 30. | 30. | |
| I | 1092. | 1106. | 1101. | 1067. | 1083. |
| Reference | Le Guen, Prost, et al., 2000 | Peng, 2000 | Peng, 2000 | Ruther, 2000 | Chevance and Farmer, 1999 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | CP-Wax 52CB | CP-Wax 52CB | CP-Wax 52CB | Supelcowax-10 | Supelcowax-10 |
| Column length (m) | 50. | 50. | 50. | 60. | 60. |
| Carrier gas | He | He | |||
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.32 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | |||
| Tstart (C) | 60. | 60. | 40. | 35. | 35. |
| Tend (C) | 220. | 220. | 220. | 195. | 195. |
| Heat rate (K/min) | 4. | 4. | 4. | 2. | 2. |
| Initial hold (min) | 5. | 5. | 5. | 5. | 5. |
| Final hold (min) | 30. | 30. | 30. | 90. | 90. |
| I | 1083. | 1070. | 1085. | 1086. | 1086. |
| Reference | Chevance and Farmer, 1999 | Chevance and Farmer, 1999, 2 | Chevance and Farmer, 1999, 2 | Chung, 1999 | Chung, 1999, 2 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | FFAP | DB-Wax | DB-Wax | PEG-20M | PEG-20M |
| Column length (m) | 60. | 60. | 30. | 25. | 25. |
| Carrier gas | He | H2 | H2 | ||
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.32 | 0.20 | 0.20 |
| Phase thickness (μm) | 0.5 | 0.25 | 0.25 | ||
| Tstart (C) | 50. | 40. | 40. | 50. | 50. |
| Tend (C) | 230. | 200. | 200. | 230. | 230. |
| Heat rate (K/min) | 5. | 3. | 6. | 2. | 2. |
| Initial hold (min) | 3. | 5. | 5. | 3. | 3. |
| Final hold (min) | 15. | 60. | 30. | ||
| I | 1106. | 1075. | 1068. | 1068. | 1069. |
| Reference | Stephan and Steinhart, 1999 | Cha, Kim, et al., 1998 | Cha, Kim, et al., 1998 | Li, Wang, et al., 1998 | Li, Wang, et al., 1998 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | HP-Wax | FFAP | PEG-20M | DB-Wax |
| Column length (m) | 30. | 50. | 30. | 60. | 60. |
| Carrier gas | He | He | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.32 | 0.2 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.5 | 0.4 | 0.25 | 0.25 | 0.25 |
| Tstart (C) | 40. | 30. | 20. | 50. | 50. |
| Tend (C) | 245. | 220. | 200. | 230. | 230. |
| Heat rate (K/min) | 3. | 5. | 4. | 2. | 3. |
| Initial hold (min) | 3. | 1. | 1. | ||
| Final hold (min) | 20. | 30. | 1. | 60. | |
| I | 1090. | 1077. | 1094. | 1086. | 1097. |
| Reference | Ollé, Baumes, et al., 1998 | Christensen, Jakobsen, et al., 1997 | Ott, Fay, et al., 1997 | Shimoda, Nakada, et al., 1997 | Shimoda, Peralta, et al., 1996 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | Supelcowax-10 | Supelcowax-10 | Carbowax 20M |
| Column length (m) | 60. | 60. | 60. | 60. | 60. |
| Carrier gas | He | He | He | He | He |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.32 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.425 |
| Tstart (C) | 50. | 50. | 40. | 60. | 45. |
| Tend (C) | 230. | 230. | 200. | 230. | 300. |
| Heat rate (K/min) | 2. | 3. | 2. | 5. | 3. |
| Initial hold (min) | 5. | 5. | 3. | ||
| Final hold (min) | 60. | 30. | 20. | 20. | |
| I | 1086. | 1081. | 1075. | 1089. | 1075. |
| Reference | Shimoda, Shiratsuchi, et al., 1996 | Shimoda, Wu, et al., 1996 | Cadwallader, Tan, et al., 1995 | Granicher, Christen, et al., 1995 | Mondello, Dugo, et al., 1995 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | DB-Wax | DB-Wax | DB-Wax | DB-Wax |
| Column length (m) | 60. | 60. | 30. | 60. | 60. |
| Carrier gas | He | He | He | ||
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
| Tstart (C) | 50. | 50. | 40. | 50. | 50. |
| Tend (C) | 230. | 230. | 200. | 230. | 230. |
| Heat rate (K/min) | 2. | 2. | 2. | 2. | 2. |
| Initial hold (min) | 5. | ||||
| Final hold (min) | 60. | 60. | |||
| I | 1073. | 1073. | 1078. | 1085. | 1085. |
| Reference | Shimoda, Shigematsu, et al., 1995 | Shimoda, Shigematsu, et al., 1995, 2 | Iwaoka, Hagi, et al., 1994 | Shiratsuchi, Shimoda, et al., 1994 | Shiratsuchi, Shimoda, et al., 1994, 2 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | Supelcowax-10 | HP-20M | HP-FFAP | DB-Wax |
| Column length (m) | 60. | 60. | 50. | 50. | 60. |
| Carrier gas | He | He | He | He | |
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | |||
| Tstart (C) | 40. | 40. | 60. | 60. | 50. |
| Tend (C) | 200. | 195. | 190. | 210. | 230. |
| Heat rate (K/min) | 3. | 2. | 3. | 3. | 2. |
| Initial hold (min) | 5. | 5. | 4. | ||
| Final hold (min) | 40. | 30. | |||
| I | 1081. | 1080. | 1075. | 1107. | 1079. |
| Reference | Sumitani, Suekane, et al., 1994 | Chung and Cadwallader, 1993 | Chung, Eiserich, et al., 1993 | Chung, Eiserich, et al., 1993 | Shiratsuchi, Shimoda, et al., 1993 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | DB-Wax | CP-Wax 52CB | DB-Wax | Supelcowax-10 | Supelcowax-10 |
| Column length (m) | 30. | 50. | 30. | 60. | 60. |
| Carrier gas | He | H2 | He | ||
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.32 | 0.32 | 0.25 | 0.25 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | ||
| Tstart (C) | 40. | 50. | 40. | 40. | 40. |
| Tend (C) | 200. | 200. | 220. | 175. | 175. |
| Heat rate (K/min) | 2. | 1.5 | 5. | 2. | 2. |
| Initial hold (min) | 10. | 10. | 3. | 5. | 5. |
| Final hold (min) | 80. | 20. | 20. | ||
| I | 1077. | 1044. | 1067. | 1086. | 1087. |
| Reference | Umano, Hagi, et al., 1992 | Wu and Liou, 1992 | Frohlich and Schreier, 1990 | Matiella and Hsieh, 1990 | Tanchotikul and Hsieh, 1989 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
|---|---|---|---|---|---|
| Active phase | Supelcowax-10 | CP-WAX 57CB | Supelcowax-10 | Supelcowax-10 | DB-Wax |
| Column length (m) | 60. | 50. | 60. | 60. | 60. |
| Carrier gas | He | ||||
| Substrate | |||||
| Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.25 | 0.32 |
| Phase thickness (μm) | 0.25 | 0.25 | 0.25 | ||
| Tstart (C) | 40. | 60. | 40. | 40. | 50. |
| Tend (C) | 175. | 200. | 175. | 175. | 225. |
| Heat rate (K/min) | 2. | 4. | 2. | 2. | 1.5 |
| Initial hold (min) | 5. | 5. | 5. | 5. | |
| Final hold (min) | 20. | 20. | 20. | 50. | |
| I | 1091. | 1088. | 1089. | 1091. | 1072. |
| Reference | Tanchotikul and Hsieh, 1989 | Salter L.J., Mottram D.S., et al., 1988 | Vejaphan, Hsieh, et al., 1988 | Vejaphan, Hsieh, et al., 1988 | Chen and Ho, 1987 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
| Column type | Capillary | Capillary | Packed |
|---|---|---|---|
| Active phase | Carbowax 20M | Carbowax 20M | Carbowax 20M |
| Column length (m) | 50. | ||
| Carrier gas | He | He | |
| Substrate | Celite 545 | ||
| Column diameter (mm) | 0.32 | ||
| Phase thickness (μm) | |||
| Tstart (C) | 50. | 50. | 75. |
| Tend (C) | 200. | 160. | 228. |
| Heat rate (K/min) | 2. | 1. | 4.6 |
| Initial hold (min) | 5. | 10. | |
| Final hold (min) | 40. | ||
| I | 1069. | 1063. | 1080. |
| Reference | Chen, Kuo, et al., 1986 | Chen, Kuo, et al., 1982 | van den Dool and Kratz, 1963 |
| Comment | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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Nielsen, Larsen, et al., 2004, 2
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Nielsen, Larsen, et al., 2004, 3
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Impact of blanching and packaging atmosphere on the formation of aroma compounds during long-term frozen storage of leek (Allium ampeloprasum Var. Bulga) slices,
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Nielsen and Poll, 2004
Nielsen, G.S.; Poll, L.,
Determination of odor active aroma compounds in freshly cut leek (Allium ampeloprasum Var. Bulga) and in long-term stored frozen unblanched and blanched leek slices by gas chromatography olfactometry analysis,
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Yu, Kim, et al., 2004
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Volatile flavor constituents of acerola (Malpighia emarginata DC.) fruit,
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Bartley, J.P.; Jacobs, A.L.,
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Chevance, F.F.V.; Farmer, L.J.,
Identification of major volatile odor compounds in frankfurters,
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Chevance and Farmer, 1999, 2
Chevance, F.F.V.; Farmer, L.J.,
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Chung, H.Y.,
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Chung, 1999, 2
Chung, H.Y.,
Volatile components in fermented soybean (Glycine max) curds,
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Stephan and Steinhart, 1999
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Volatiles emitted from flowers of γ-radiated and nonradiated Jasminum polyanthum Franch. in Situ,
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Volatile Flavor Components in Crayfish Waste,
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A generalization of the retention index system including linear temperature programmed gas-liquid partition chromatography,
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Notes
Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, References
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