Cyclohexanemethanol, 4-ethenyl-α,α,4-trimethyl-3-(1-methylethenyl)-, [1R-(1α,3α,4β)]-
- Formula: C15H26O
- Molecular weight: 222.3663
- IUPAC Standard InChIKey: GFJIQNADMLPFOW-UHFFFAOYSA-N
- CAS Registry Number: 639-99-6
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Species with the same structure:
- Stereoisomers:
- Other names: o-Menth-8-ene-4-methanol, α,α-dimethyl-1-vinyl-, (1S,2S,4R)-(-)-; Elemol; 2-((1R,3S,4S)-4-Methyl-3-(prop-1-en-2-yl)-4-vinylcyclohexyl)propan-2-ol; 2-(3-Isopropenyl-4-methyl-4-vinylcyclohexyl)-2-propanol; 1R,1α,3α,4β-4-Ethenyl-α,α,4-trimethyl-3-(1-methylethenyl)cyclohexanemethanol; (1S,2S,4R)-(-)-α,α-dimethyl-1-vinyl-o-menth-8-ene-4-methanol
- Information on this page:
- Other data available:
- Options:
Normal alkane RI, non-polar column, custom temperature program
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | RTX-5 MS | DB-1 | Polydimethyl siloxane with 5 % Ph groups | 5 % Phenyl polydimethyl siloxane | OV-1 |
Column length (m) | 30. | 30. | 30. | 30. | |
Carrier gas | Helium | Hydrogen | Helium | Helium | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Phase thickness (μm) | 0.25 | 0.25 | |||
Program | not specified | 45 0C 3 0C/min -> 175 0C 15 0C/min -> 300 0C (10 min) | 50 0C 4 0C/min -> 200 0C (5 min) 20 0C/min -> 280 0C | not specified | 40 0C 2 0C/min -> 120 0C 10 0C/min -> 230 0C (15 min) |
I | 1549. | 1530. | 1546. | 1551. | 1522. |
Reference | Pinheiro, de Queiros, et al., 2013 | Albano, Lima, et al., 2012 | da Silva, de Souza, et al., 2012 | Chaverri, Diaz, et al., 2011 | Chen and Li, 2011 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CBP-5 | DB-5 MS | HP-5 MS | HP-5 MS | HP-5 MS |
Column length (m) | 30. | 30. | |||
Carrier gas | Helium | Helium | |||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | |||
Phase thickness (μm) | 0.25 | ||||
Program | 60 0C 3 0C/min -> 246 0C 10 0C/min -> 270 0C (5 min) | 50 0C (1.5 min) 4 0C/min -> 200 0C 10 0C/min -> 300 0C (10 min) | not specified | not specified | not specified |
I | 1552. | 1547. | 1547. | 1548. | 1549. |
Reference | Fortes, Naves, et al., 2011 | Lima, Quintans-Junior, et al., 2011 | Payo, Colo, et al., 2011 | Payo, Colo, et al., 2011 | Payo, Colo, et al., 2011 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 MS | HP-5 | Elite-5 MS | Elite-5 MS | HP-5 |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | Helium | Helium | Helium | Helium | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Program | 50 0C (2 min) 3 0C/min -> 130 0C (2 min) 5 0C/min -> 270 0C | not specified | 60 0C (1 min) 1.5 0C/min -> 185 0C (1 min) 9 0C/min -> 275 0C (2 min) | 60 0C (1 min) 1.5 0C/min -> 185 0C (1 min) 9 0C/min -> 275 0C (2 min) | not specified |
I | 1541. | 1549. | 1544. | 1549. | 1549. |
Reference | Bamoniri, Mirjalili, et al., 2010 | Bi Kouame, Bedi, et al., 2010 | Kapoor, Singh, et al., 2009 | Kapoor, Singh, et al., 2009 | Riahi, Pourbasheer, et al., 2009 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP Sil 8 CB | RTX-5 | RTX-5 | HP-5MS | HP-1 |
Column length (m) | 30. | 30. | 30. | 30. | 30. |
Carrier gas | Helium | Helium | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.2 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 0.33 |
Program | 60C => 2.5C/min => 170C => 10C/min => 250C (5min) | 60 0C (5 min) 5 0C/min -> 110 0C 3 0C/min -> 220 0C (5 min) | not specified | 40C(10min) => 3C/min => 200C => 2C/min => 220C | 60C(5min) => 3C/min => 180C => 20C/min => 280C(10min) |
I | 1549. | 1553. | 1547. | 1550. | 1547. |
Reference | Kristiawan, Sobolik, et al., 2008 | Zachariah, Leela, et al., 2008 | Zachariah, Leela, et al., 2008 | Cole, Haber, et al., 2007 | Merle, Verdeguer, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | CP Sil 8 CB | HP-5 MS | HP-5 MS | HP-5MS |
Column length (m) | 50. | 50. | 30. | 30. | |
Carrier gas | Helium | Helium | Helium | He | |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.32 | 0.25 | 0.25 | |
Phase thickness (μm) | 0.25 | 0.25 | |||
Program | 60 0C (1 min) 5 0C/min -> 160 0C 10 0C/min -> 250 0C | 60 0C (2 min) 5 0C/min -> 160 0C (1 min) 10 0C/min -> 280 0C (3 min) | 40 0C (10 min) 3 oC/min -> 200 0C 2 0C/min -> 220 0C | not specified | 40C(10min) => 3C/min => 200C => 2C/min => 220C |
I | 1550. | 1550. | 1549. | 1550. | 1549. |
Reference | Nivinsliene, Butkiene, et al., 2007 | Radusiene, Judzentiene, et al., 2007 | Setzer, Stokes, et al., 2007 | Stokes, Cole, et al., 2007 | Takaku, Haber, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | Polydimethyl siloxane | HP-5 MS | DB-5 | HP-5 MS | HP-5MS |
Column length (m) | 30. | 30. | 30. | 30. | |
Carrier gas | HGelium | He | Helium | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.32 | |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Program | not specified | 40 0C (3 min) 10 0C/min -> 108 0C 3 0C/min -> 188 0C 4 0C/min -> 280 0C (5 min) | 40C (5min) => 2C/min => 250C(15min) => 5C/min => 270C (10min) | 40 0C (10 min) 3 0C/min -> 200 0C 2 0C/min -> 220 0C | 60C(1min) => 1.5C => 185C => 9C/min => 275C (2min) |
I | 1548. | 1552. | 1542. | 1551. | 1550. |
Reference | Werka, Boehme, et al., 2007 | Kawaree, Phutdhawong, et al., 2006 | Massardo, Senatore, et al., 2006 | Schmidt, Noletto, et al., 2006 | Singh G., Maurya S., et al., 2006 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SE-52 | CP Sil 8 CB | DB-5 | DB-1 | CP Sil 8 CB |
Column length (m) | 30. | 50. | 30. | 30. | 50. |
Carrier gas | He | He | He | He | He |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.32 | 0.25 | 0.25 | 0.32 |
Phase thickness (μm) | 0.15 | 0.25 | 0.25 | 0.25 | 0.25 |
Program | 45C => 1C/min => 100C => 5C/min => 250C (10min) | 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min) | 35C => 4C/min => 180C => 10C/min => 250C | 45C => 3C/min => 175C => 15C/min => 300C (10min) | 60C(1min) => 5C/min => 160C => 5C/min => 250C(3min) |
I | 1550. | 1550. | 1551.5 | 1530. | 1549. |
Reference | Tognolini, Barocelli, et al., 2006 | Butkienë, Nivinskienë, et al., 2005 | Cysne, Canuto, et al., 2005 | Faleio, Miguel, et al., 2005 | Nivinskienë, Butkienë, et al., 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | DB-5 | CP Sil 8 CB | HP-5 | DB-5 | CP Sil 8 CB |
Column length (m) | 30. | 50. | 30. | 30. | 50. |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.32 | 0.25 | 0.32 |
Phase thickness (μm) | 0.25 | 0.1 | 0.25 | ||
Program | not specified | 60C(2min) => 5C/min => 160C(1min) => 10C/min => 250C (3min) | 65C(1min) => 1C/min => 75C (2min) => 0.5C/min => 81C(2min) => 3C/min => 180C(7min) | 35C => 4C/min => 180C => 20C/min => 280C | 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min) |
I | 1538. | 1550. | 1550. | 1549. | 1550. |
Reference | de Oliveira, Dias, et al., 2005 | Radudienë, Judpintienë, et al., 2005 | Singh, Maurya, et al., 2005 | Barros-Filho, Nunes, et al., 2004 | Butkienë, Nivinskienë, et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | Methyl Silicone | OV-1 | BPX-5 | DB-1 | HP-5 |
Column length (m) | 30. | 30. | 30. | 30. | |
Carrier gas | He | H2 | He | He | |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Program | not specified | 45 0C (4 min) 3 0C/min -> 75 0C 4 0C/min -> 115 0C 6 0C/min -> 312 0C | 50 0C (1 min) 3 0C/min -> 150 0C 5 0C/min -> 250 0C (5 min) | 45C => 3C/min => 175C => 15C/min => 300C (10min) | 50C (3min) => 3C/min => 150C (10min) => 10C/min => 250C |
I | 1546. | 1532. | 1550. | 1530. | 1550. |
Reference | Couladis, Özcan, et al., 2004 | Hafez and Abdel-Salam, 2004 | Koba, Sanda, et al., 2004 | Miguel, Simões, et al., 2004 | Tepe, Donmez, et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SE-30 | SE-30 | DB-1 | Methyl Silicone | SE-30 |
Column length (m) | 30. | 60. | |||
Carrier gas | He | He | |||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | |||
Phase thickness (μm) | 0.25 | ||||
Program | not specified | not specified | 45C => 3C/min => 175C => 15C/min => 300C (10min) | not specified | 50 0C (5 min) 5 0C/min -> 165 0C 4 0C/min -> 230 0C |
I | 1533. | 1535. | 1530. | 1537. | 1543. |
Reference | Vinogradov, 2004 | Vinogradov, 2004 | Faleiro, Miguel, et al., 2003 | Bakshu and Raju, 2002 | Li, Wu, et al., 2002 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SE-30 | DB-1 | DB-5 | OV-101 | DB-1 |
Column length (m) | 60. | 30. | 50. | 30. | |
Carrier gas | He | N2 | H2 | ||
Substrate | |||||
Column diameter (mm) | 0.25 | 0.25 | 0.25 | 0.25 | |
Phase thickness (μm) | 0.25 | 0.25 | |||
Program | not specified | 45 0C 3 K/min -> 175 0C 15 K/min -> 300 0C (10 min) | not specified | not specified | 45C => 3C/min => 175C => 15C => 240C(10min) |
I | 1540. | 1530. | 1544. | 1540. | 1530. |
Reference | Li, Wu, et al., 2002 | Figueiredo, Miguel, et al., 2001 | Petrakis, Tsitsimpikou, et al., 2001 | Yang, 2001 | da Silva, Figueiredo, et al., 1998 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary |
---|---|
Active phase | Polydimethyl siloxanes |
Column length (m) | |
Carrier gas | |
Substrate | |
Column diameter (mm) | |
Phase thickness (μm) | |
Program | not specified |
I | 1535. |
Reference | Zenkevich, 1997 |
Comment | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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Faleio, L.; Miguel, G.; Gomes, S.; Costa, L.; Venancio, F.; Teixeira, A.; Figueiredo, A.C.; Barroso, J.G.; Pedro, L.G.,
Antibacterial and Antioxidant Activities of Essential Oils Isolated from Thymbra capitata L. (Cav.) and Origanum vulgare L.,
J. Agric. Food Chem., 2005, 53, 21, 8162-8168, https://doi.org/10.1021/jf0510079
. [all data]
Nivinskienë, Butkienë, et al., 2005
Nivinskienë, O.; Butkienë, R.; Mockutë, D.,
Chemical composition of seed (fruit) essential oils of Angelica archangelica L. growing wild in Lithuania,
Chemija, 2005, 16, 3-4, 51-54. [all data]
de Oliveira, Dias, et al., 2005
de Oliveira, R.N.; Dias, I.J.M.; Câmara, C.A.G.,
Estudo comparativo do óleo essencial de Eugenia punicifolia (HBK) DC. de diferentes localidades de Pernambuco,
Rev. Bras. Farmacogn., 2005, 15, 1, 39-43, https://doi.org/10.1590/S0102-695X2005000100009
. [all data]
Radudienë, Judpintienë, et al., 2005
Radudienë, J.; Judpintienë, A.; Peèiulytë, D.; Janulis, V.,
Chemical composition of essential oil and antimicrobial activity of Origanum vulgare,
Biologija, 2005, 4, 53-58. [all data]
Singh, Maurya, et al., 2005
Singh, G.; Maurya, S.; Catalan, C.; de Lampasona, M.P.,
Studies on essential oils, Part 42: chemical, antifungal, antioxidant and sprout suppressant studies on ginger essential oil and its oleoresin,
Flavour Fragr. J., 2005, 20, 1, 1-6, https://doi.org/10.1002/ffj.1373
. [all data]
Barros-Filho, Nunes, et al., 2004
Barros-Filho, B.A.; Nunes, F.M.; de Oliveira, M.C.F.; Mafezoli, J.; Andrade-Neto, M.; Silveira, E.R.; Pirani, J.R.,
Volatile constituents from Esenbeckia almawillia (Rutaceae),
Biochem. Syst. Ecol., 2004, 32, 9, 817-821, https://doi.org/10.1016/j.bse.2004.02.003
. [all data]
Butkienë, Nivinskienë, et al., 2004
Butkienë, R.; Nivinskienë, O.; Mockutë, D.,
Chemical composition of unripe and ripe berry essential oils of Juniperus communis L. growing wild in Vilnius district,
Chemija, 2004, 15, 4, 57-63. [all data]
Couladis, Özcan, et al., 2004
Couladis, M.; Özcan, M.; Tzakou, O.; Akgül, A.,
Menengic (Pistacia terebinthus L.) agacinin degisik organlarinda ucucu yag bilesimi, Bitkisel Ilac Hammaddeleri Toplantisi, Bildiriler, 29-31 Mayis 2002, 2004, 6. [all data]
Hafez and Abdel-Salam, 2004
Hafez, S.S.; Abdel-Salam, H.A.,
chemical composition and antimicrobial activity of the volatile constituents of thuja occidentalis L. growing in Egipt,
Alexandria J. Pharm. Sci., 2004, 18, 1, 41-47. [all data]
Koba, Sanda, et al., 2004
Koba, K.; Sanda, K.; Raynaud, C.; Nenonene, Y.A.; Millet, J.; Chaumont, J.P.,
Activités antimicrobiennes d'huiles essentielles de trois Cymbopogon sp. africains vis-àvis de germes pathogènes d'animaux de compagnie,
Ann. Med. Vet., 2004, 148, 202-206. [all data]
Miguel, Simões, et al., 2004
Miguel, G.; Simões, M.; Figueiredo, A.C.; Barroso, J.G.; Pedro, L.G.; Carvalho, L.,
Composition and antioxidant activities of the essential oils of Thymus caespititius, Thymus camphoratus and Thymus mastichina,
Food Chem., 2004, 86, 2, 183-188, https://doi.org/10.1016/j.foodchem.2003.08.031
. [all data]
Tepe, Donmez, et al., 2004
Tepe, B.; Donmez, E.; Unlu, M.; Candan, F.; Daferera, D.; Vardar-Unlu, G.; Polissiou, M.; Sokmen, A.,
Antimicrobial and antioxidative activities of the essential oils and methanol extracts of Salvia cryptantha (Montbret et Aucher ex Benth.) and Salvia multicaulis (Vahl),
Food Chem., 2004, 84, 4, 519-525, https://doi.org/10.1016/S0308-8146(03)00267-X
. [all data]
Vinogradov, 2004
Vinogradov, B.A.,
Production, composition, properties and application of essential oils, 2004, retrieved from http://viness.narod.ru. [all data]
Faleiro, Miguel, et al., 2003
Faleiro, M.L.; Miguel, M.G.; Ladeiro, F.; Venancio, F.; Tavares, R.; Brito, J.C.; Figueiredo, A.C.; Barroso, J.G.; Pedro, L.G.,
Antimicrobial activity of essential oils isolated from Portuguese endemic species of Thymus,
Lett. Appl. Microbiol., 2003, 36, 1, 35-40, https://doi.org/10.1046/j.1472-765X.2003.01259.x
. [all data]
Bakshu and Raju, 2002
Bakshu, L.Md.; Raju, R.R.V.,
Essential oil composition and antimicrobial activity of tuberous roots of Pimpinella tirupatiensis Bal. Subr., an endemic taxon from eastern ghats, India,
Flavour Fragr. J., 2002, 17, 6, 413-415, https://doi.org/10.1002/ffj.1118
. [all data]
Li, Wu, et al., 2002
Li, C.; Wu, H.; Yang, L.; ren, Y.,
Study of the composition of ginger oil from Laifeng,
Flavour Fragr. Cosmetics, 2002, 5, 15-17. [all data]
Figueiredo, Miguel, et al., 2001
Figueiredo, A.C.; Miguel, M.G.; Duarte, A.M.F.; Barroso, J.G.; Pedro, L.G.,
Essential oil composition of Thymus lotocephallus G. López R. Morales, collected during flowering and vegetative phases,
Flavour Fragr. J., 2001, 16, 6, 417-421, https://doi.org/10.1002/ffj.1028
. [all data]
Petrakis, Tsitsimpikou, et al., 2001
Petrakis, P.V.; Tsitsimpikou, C.; Tzakou, O.; Couladis, M.; Vagias, C.; Roussis, V.,
Needle volatiles from five Pinus species growing in Greece,
Flavour Fragr. J., 2001, 16, 4, 249-252, https://doi.org/10.1002/ffj.990
. [all data]
Yang, 2001
Yang, R.,
Analysis of the volatile components in peel oil of Yuzu by gas chromatography/mass spectrometry,
Chin. J. Anal. Chem., 2001, 29, 3, 313-316. [all data]
da Silva, Figueiredo, et al., 1998
da Silva, J.A.; Figueiredo, A.C.; Barroso, J.G.; Pedro, L.G.; Gomes, M.A.; Fontinha, S.S.; Scheffer, J.J.C.,
Composition of the essential oil of Melanoselinum decipiens (Schrad. Wendl.) Hoffm., an endemic species of the Madeira and Azores archipelagos,
Flavour Fragr. J., 1998, 13, 2, 90-92, https://doi.org/10.1002/(SICI)1099-1026(199803/04)13:2<90::AID-FFJ700>3.0.CO;2-D
. [all data]
Zenkevich, 1997
Zenkevich, I.G.,
Analytical Parameters of Components of Essential Oils for their Chromatographic and Chromato-Spectral Identificaiton. Oxsigenated derivatives of Mono- and Sesquiterpene Hydrocarbons,
Rastit, Resursy (Rus.), 1997, 33, 1, 16-28. [all data]
Notes
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