Hexanedioic acid, dimethyl ester

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Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5DB-15 % Phenyl methyl siloxane5 % Phenyl methyl siloxane
Column length (m) 30.30.30.25.30.
Carrier gas HeN2   
Substrate      
Column diameter (mm) 0.250.250.20.310.25
Phase thickness (μm) 0.250.250.250.310.5
Tstart (C) 40.60.50.50.50.
Tend (C) 325.220.300.250.300.
Heat rate (K/min) 3.5.5.5.8.
Initial hold (min)  10.2.1.1.
Final hold (min)   5.10.10.
I 1208.21246.1206.1235.1256.
ReferenceSun and Stremple, 2003Flamini, Cioni, et al., 2002Johnson, Urso, et al., 1997Guisto, Smith, et al., 1993Guisto, Smith, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedPacked
Active phase DB-5SE-30SE-30
Column length (m) 30.  
Carrier gas HeN2 
Substrate  Chromosorb QCelite
Column diameter (mm) 0.26  
Phase thickness (μm) 0.25  
Tstart (C) 50.100.75.
Tend (C) 300.340.228.
Heat rate (K/min) 6.10. 
Initial hold (min) 4.  
Final hold (min) 20.  
I 1243.1205.1213.
ReferenceRostad and Pereira, 1986Messadi and Vergnaud, 1979van den Dool and Kratz, 1963
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Sun and Stremple, 2003
Sun, G.; Stremple, P., Retention index characterization of flavor, fragrance, and many other compounds on DB-1 and DB-XLB, 2003, retrieved from http://www.chem.agilent.com/cag/cabu/pdf/b-0279.pdf. [all data]

Flamini, Cioni, et al., 2002
Flamini, G.; Cioni, P.L.; Morelli, I., Differences in the fragrances of pollen and different floral parts of male and female flowers of Laurus nobilis, J. Agric. Food Chem., 2002, 50, 16, 4647-4652, https://doi.org/10.1021/jf020269x . [all data]

Johnson, Urso, et al., 1997
Johnson, C.I.; Urso, A.; Geleta, L., Broad spectrum analysis of municipal and industrial effluents discharged into the Peace, Athabasca and Slave river basins: characterization of effluent samples, 1994 - Volume 1 of 2, Northern River Basins Study Project Report No. 121, Norther River Basins Study, Edmonton, Alberta, 1997, 27. [all data]

Guisto, Smith, et al., 1993
Guisto, R.; Smith, S.R.; Stuart, J.D., Gas chromatographic retention indices, mass, and infrared spectra of industrially important adipate esters, J. Chromatogr. Sci., 1993, 31, 6, 225-230, https://doi.org/10.1093/chromsci/31.6.225 . [all data]

Rostad and Pereira, 1986
Rostad, C.E.; Pereira, W.E., Kovats and Lee retention indices determined by gas chromatography/mass spectrometry for organic compounds of environmental interest, J. Hi. Res. Chromatogr. Chromatogr. Comm., 1986, 9, 6, 328-334, https://doi.org/10.1002/jhrc.1240090603 . [all data]

Messadi and Vergnaud, 1979
Messadi, D.; Vergnaud, J.-M., Quick identification and analysis of plasticizers in PVC by programmed-temperature gas chromatography using the best stationary phases, J. Appl. Polym. Sci., 1979, 24, 5, 1215-1225, https://doi.org/10.1002/app.1979.070240507 . [all data]

van den Dool and Kratz, 1963
van den Dool, H.; Kratz, P. Dec., A generalization of the retention index system including linear temperature programmed gas-liquid partition chromatography, J. Chromatogr., 1963, 11, 463-471, https://doi.org/10.1016/S0021-9673(01)80947-X . [all data]


Notes

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