Piperidine, 1-methyl-

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Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryPackedPackedPacked
Active phase OV-101OV-101Apiezon LPMS-100PMS-100
Column length (m) 50.50.2.73.3.
Carrier gas HeHeN2 or HeHeHe
Substrate   Chromosorb G, AWCelite 545 (44-60 mesh)Celite 545 (44-60 mesh)
Column diameter (mm) 0.30.30   
Phase thickness (μm) 0.40.40   
Temperature (C) 110.110.100.130.150.
I 766.769.779.750.760.
ReferenceZhuravleva, 2000Zhuravleva, Golovnya, et al., 1993Zhuravleva, Kapustin, et al., 1976Anderson, Jurel, et al., 1973Anderson, Jurel, et al., 1973
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase PMS-100
Column length (m) 3.
Carrier gas He
Substrate Celite 545 (44-60 mesh)
Column diameter (mm)  
Phase thickness (μm)  
Temperature (C) 180.
I 763.
ReferenceAnderson, Jurel, et al., 1973
Comment MSDC-RI

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Zhuravleva, 2000
Zhuravleva, I.L., Evaluation of the polarity and boiling points of nitrogen-containing heterocyclic compounds by gas chromatography, Russ. Chem. Bull. (Engl. Transl.), 2000, 49, 2, 325-328, https://doi.org/10.1007/BF02494682 . [all data]

Zhuravleva, Golovnya, et al., 1993
Zhuravleva, I.L.; Golovnya, R.V.; Kuzmenko, T.E., The regularities of the gas-chromatographic behavior of methyl-substituted N-alkylpiperidines, Russ. Chem. Bull. (Engl. Transl.), 1993, 42, 10, 1677-1679, https://doi.org/10.1007/BF00697038 . [all data]

Zhuravleva, Kapustin, et al., 1976
Zhuravleva, I.L.; Kapustin, Yu.P.; Golovnya, P.B., Retention indices of some isoaliphatic and heterocyclic nitrogenous bases, Zh. Anal. Khim., 1976, 31, 1378-1380. [all data]

Anderson, Jurel, et al., 1973
Anderson, A.; Jurel, S.; Shymanska, M.; Golender, L., Gas-liquid chromatography of some aliphatic and heterocyclic mono- and pollyfunctional amines. VII. Retention indices of amines in some polar and unpolar stationary phases, Latv. PSR Zinat. Akad. Vestis Kim. Ser., 1973, 1, 51-63. [all data]


Notes

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