Disulfide, dimethyl
- Formula: C2H6S2
- Molecular weight: 94.199
- IUPAC Standard InChIKey: WQOXQRCZOLPYPM-UHFFFAOYSA-N
- CAS Registry Number: 624-92-0
- Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript. - Other names: 2,3-Dithiabutane; Methyl disulfide; (Methyldithio)methane; Dimethyl disulfide; Dimethyl disulphide; (CH3S)2; UN 2381; DMDS; Sulfa-Hitech; NSC 9370; (Methyldisulfanyl)methane
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Normal alkane RI, non-polar column, custom temperature program
Go To: Top, References, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 MS | HP-5 MS | HP-5 | DB-5 MS | DB-5 MS |
Column length (m) | 30. | 30. | 60. | 30. | 60. |
Carrier gas | Helium | Helium | Helium | Helium | Helium |
Substrate | |||||
Column diameter (mm) | 0.25 | 0.32 | 0.25 | 0.25 | 0.32 |
Phase thickness (μm) | 0.25 | 0.25 | 0.25 | 0.25 | 1.0 |
Program | not specified | not specified | 30 0C (2 min) 2 0Cmin -> 60 0C 10 0C/min -> 100 0C 20 0C/min -> 140 0C 10 0C/min -> 200 0C (10 min) | 45 0C (0.75 min) 10 0C/min -> 200 0C 30 0C/min -> 245 0C (1.25 min) | 40 0C (2 min) 6 0C/min -> 100 0C 4 0C/min -> 180 0C 8 0C/min -> 250 0C (12 min) |
I | 733. | 746. | 740. | 748. | 747. |
Reference | Kotowska, Zalikowski, et al., 2012 | Pino, Marquez, et al., 2010 | Rotsatschakul, Visesanguan, et al., 2009 | Cajka, Hajslova, et al., 2007 | Liu, Xu, et al., 2007 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-5 | BPX-5 | HP-1 | Methyl Silicone | HP-5 |
Column length (m) | 60. | 50. | 60. | 60. | |
Carrier gas | He | He | He | Helium | |
Substrate | |||||
Column diameter (mm) | 0.32 | 0.32 | 0.32 | 0.32 | |
Phase thickness (μm) | 1. | 0.52 | 1.0 | 1. | |
Program | 50C => 3C/min => 200C(10min) => 10C/min => 290C(10min) | 40C(4min) => 2C/min => 90C => 4C/min => 130C => 8C/min => 250C | 40C => 2C/min => 130C => 4C/min => 250C (25min) | -50 0C (2 min) 8 0C/min -> 200 0C (7.75 min) 25 0C -> 225 0C (8 min) | not specified |
I | 743. | 756. | 733. | 729. | 741. |
Reference | Splivallo, Bossi, et al., 2007 | van Ruth, Floris, et al., 2006 | Senger-Emonnot, Rochard, et al., 2006 | Blunden, Aneja, et al., 2005 | Thierry, Maillard, et al., 2005 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | HP-1 | CP Sil 5 CB | HP-5 | DB-5 | BPX-5 |
Column length (m) | 25. | 50. | 50. | 50. | 60. |
Carrier gas | He | ||||
Substrate | |||||
Column diameter (mm) | 0.2 | 0.32 | 0.32 | 0.32 | 0.32 |
Phase thickness (μm) | 0.11 | 1.2 | 1.05 | 1.05 | 1. |
Program | 35C(3min) => 4C/min => 190C => 30C/min => 225C(3min) | 36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C(30min) | 40C(10min) => 5C/min => 200C => 20C/min => 250C(5min) | 40C(10min) => 5C/min => 200C => 20C/min => 250C (5min) | 40C (4min) => 2C/min => 90C => 4C/min => 130C => 8C/min => 250 C (10min) |
I | 725. | 732. | 750. | 750. | 750. |
Reference | Carpino, Mallia, et al., 2004 | Counet, Ouwerx, et al., 2004 | Garcia-Estaban, Ansorena, et al., 2004 | Garcia-Estaban, Ansorena, et al., 2004, 2 | Machiels, Istasse, et al., 2004 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SE-30 | SPB-5 | Apieson M | RTX-5 MS | BPX-5 |
Column length (m) | 60. | 60. | 60. | ||
Carrier gas | He | He | |||
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.32 | ||
Phase thickness (μm) | 1. | 0.5 | 1. | ||
Program | not specified | not specified | not specified | 35C (3min) => 10C/min => 50C => 4C/min => 200C => 50C/min => 250C (10min) | 40C (4min) => 2C/min => 90C => 4C/min => 130C => 8C/min => 250 C (10min) |
I | 730. | 742. | 765. | 751. | 744. |
Reference | Vinogradov, 2004 | Begnaud, Pérès, et al., 2003 | Gao, Wang, et al., 2003 | Machiels and Istasse, 2003 | Machiels, van Ruth, et al., 2003 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP Sil 5 CB | DB-5MS | Methyl phenyl siloxane (not specified) | CP Sil 8 CB | CP Sil 5 CB |
Column length (m) | 50. | 60. | 50. | ||
Carrier gas | |||||
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.32 | ||
Phase thickness (μm) | 1.2 | 0.25 | 1.2 | ||
Program | 36C => 20C/min => 85C => 1C/min => 145C=3C/min => 250C(30min) | not specified | not specified | not specified | 36C => 20C/min => 120C(20min) => 2C/min => 250C(30min) |
I | 743. | 724. | 746. | 756. | 734. |
Reference | Counet, Callemien, et al., 2002 | Fu, Yoon, et al., 2002 | Poligne, Collignan, et al., 2002 | Duckham, Dodson, et al., 2001 | Lermusieau, Bulens, et al., 2001 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | CP Sil 5 CB | DB-5 MS | Polydimethyl siloxane | CP Sil 5 CB | CP Sil 5 CB |
Column length (m) | 50. | 30. | 50. | 50. | |
Carrier gas | Helium | He | He | ||
Substrate | |||||
Column diameter (mm) | 0.32 | 0.25 | 0.32 | 0.32 | |
Phase thickness (μm) | 1.2 | 1.0 | 1.2 | 1.2 | |
Program | 36C => 20C/min => 120C(20min) => 2C/min => 250C(30min) | not specified | not specified | 33C (16.5min) => 2C/min => 160C => 20C/min => 200C (9min) | 30C => 55C/min => 85C => 1C/min => 145C => 3C/min => 250C |
I | 735. | 761. | 741. | 734. | 723. |
Reference | Lermusieau, Bulens, et al., 2001 | Luo and Agnew, 2001 | Spanier, Shahidi, et al., 2001 | Gijs, Piraprez, et al., 2000 | Guyot, Bouseta, et al., 1998 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SPB-1 | DB-5 | DB-5 | DB-5 | Methyl Silicone |
Column length (m) | 60. | 50. | 50. | 50. | |
Carrier gas | He | He | He | He | |
Substrate | |||||
Column diameter (mm) | 0.53 | 0.32 | 0.32 | 0.32 | |
Phase thickness (μm) | 5. | 0.25 | 0.25 | 0.25 | |
Program | 40C(6min) => 5C/min => 80C => 10C/min => 200C | 40C (10min) => 3C/min => 95C => 10C/min => 270C (10min) | 40C (10min) => 3C/min => 95C => 10C/min => 270C (10min) | 40C (10min) => 3C/min => 95C => 10C/min => 270C (10min) | not specified |
I | 735. | 745. | 746. | 743. | 720. |
Reference | Flanagan, Streete, et al., 1997 | Mateo and Zumalacárregui, 1996 | Mateo and Zumalacárregui, 1996 | Mateo and Zumalacárregui, 1996 | Misharina, 1995 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | SPB-1 | CP Sil 8 CB | methyl silicone oil with 5% Igepal | methyl silicone oil with 5% Igepal | SE-30 |
Column length (m) | 60. | 40. | 150. | 150. | 25. |
Carrier gas | Helium | He | |||
Substrate | |||||
Column diameter (mm) | 0.53 | 0.25 | 0.75 | 0.75 | 0.25 |
Phase thickness (μm) | 5.0 | 0.25 | |||
Program | 40 0C (6 min) 5 0C/min -> 80 0C 10 0C/min -> 200 0C | 30 0C (1 min) 15 0C/min -> 45 0C 3 0C/min -> 120 0C | not specified | not specified | not specified |
I | 735. | 749. | 726. | 732. | 739. |
Reference | Strete, Ruprah, et al., 1992 | Weller and Wolf, 1989 | Schultz, Flath, et al., 1988 | Schultz, Flath, et al., 1988 | P'yanova, Zvereva, et al., 1987 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Capillary | Capillary | Capillary | Capillary | Capillary |
---|---|---|---|---|---|
Active phase | OV-101 | SE-52 | OV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc. | OV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc. | OV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc. |
Column length (m) | 50. | 100. | 50. | 50. | 50. |
Carrier gas | He | Hydrogen | Hydrogen | Hydrogen | |
Substrate | |||||
Column diameter (mm) | 0.24 | 0.50 | 0.32 | 0.32 | 0.32 |
Phase thickness (μm) | |||||
Program | not specified | not specified | not specified | not specified | not specified |
I | 730. | 752. | 720. | 724. | 743. |
Reference | Zenkevich and Malamakhov, 1987 | van Langenhove and Schamp, 1986 | Waggott and Davies, 1984 | Waggott and Davies, 1984 | Waggott and Davies, 1984 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI | MSDC-RI |
Column type | Packed | Packed | Capillary |
---|---|---|---|
Active phase | Apiezon M | Apiezon M | SE-30 |
Column length (m) | 5.6 | 5.6 | 50. |
Carrier gas | N2 | N2 | He |
Substrate | Chromosorb W AW/DMCS | Chromosorb W AW/DMCS | |
Column diameter (mm) | 0.5 | ||
Phase thickness (μm) | |||
Program | 60C(7min), 100C(7min), 150C isothermal | 60C(7min), 100C(7min), 150C isothermal | -10C (8min) => 12C/min => 26C => 3C/min => 170C (30min) |
I | 770. | 770. | 727. |
Reference | Golovnya, Misharina, et al., 1983 | Golovnya, Misharina, et al., 1983 | Heydanek and McGorrin, 1981 |
Comment | MSDC-RI | MSDC-RI | MSDC-RI |
References
Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes
Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.
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Heydanek, M.G.; McGorrin, R.J.,
Gas chromatography-mass spectroscopy investigations on the flavor chemistry of oat groats,
J. Agric. Food Chem., 1981, 29, 5, 950-954, https://doi.org/10.1021/jf00107a016
. [all data]
Notes
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