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Disulfide, dimethyl

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Optima-5 MSHP-5 MSVF-5 MSDB-5VF-5 MS
Column length (m) 30.30.60.25.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.200.32
Phase thickness (mum) 0.250.250.250.330.25
Tstart (C) 35.35.40.50.30.
Tend (C) 250.300.250.240.260.
Heat rate (K/min) 10.3.4.20.2.
Initial hold (min) 3.5.2.1. 
Final hold (min) 5.15.  28.
I 732.735.740.738.739.
ReferenceGoeminne, Vandendriessche, et al., 2012Kotowska, Zalikowski, et al., 2012Srisajjalerwaja, Apichartsrangkoon, et al., 2012Cais-Sokolinska, Majcher, et al., 2011Leffingwell and Alford, 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase VF-5 MSDB-5 MSHP-5 MSDB-5SPB-1
Column length (m) 60.25.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.200.320.250.25
Phase thickness (mum) 0.250.330.250.251.0
Tstart (C) 30.40.50.50.60.
Tend (C) 260.250.240.220.250.
Heat rate (K/min) 2.10.4.4.5.
Initial hold (min)  1.2. 5.
Final hold (min) 28. 10.  
I 746.751.747.783.729.
ReferenceLeffingwell and Alford, 2011Majcher, Lawrowski, et al., 2010Pino, Marquez, et al., 2010Shedid, 2010Frerot, Velluz, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase VF-5MSSPB-5SPB-5DB-5HP-1
Column length (m) 30.60.60.30.50.
Carrier gas    HeHe
Substrate      
Column diameter (mm) 0.250.320.320.320.2
Phase thickness (mum) 0.251.1.1.0.5
Tstart (C) 40.40.40.40.60.
Tend (C) 250.230.230.250.250.
Heat rate (K/min) 7.3.3.4.2.
Initial hold (min)  5.5.2. 
Final hold (min)  5.5.15.60.
I 735.746.747.756.731.
ReferenceGhiasvand, Setkova, et al., 2007Vasta, Ratel, et al., 2007Vasta, Ratel, et al., 2007Fan and Qian, 2006Bendimerad and Bendiab, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MDN-5HP-55 % Phenyl methyl siloxanePONA
Column length (m) 30.60.30.0.50.
Carrier gas N2HeHeliumHeN2
Substrate      
Column diameter (mm) 0.320.250.320.250.20
Phase thickness (mum) 0.250.250.251.0.50
Tstart (C) 40.40.40.40.35.
Tend (C) 250.270.250.250.170.
Heat rate (K/min) 4.4.5.7.2.
Initial hold (min) 2.4.2.10. 
Final hold (min) 5.5.5.5. 
I 740.743.746.744.736.
ReferenceFan and Qian, 2005van Loon, Linssen, et al., 2005N/ARamírez, Estévez, et al., 2004Yang, Wang, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5SPB-5HP-1PONA
Column length (m) 25.60.60.50.50.
Carrier gas HeHeHeliumHeHelium
Substrate      
Column diameter (mm) 0.20.250.320.20.20
Phase thickness (mum) 0.330.251.00.50.50
Tstart (C) 40.35.30.60.30.
Tend (C) 190.280.230.220.170.
Heat rate (K/min) 4.5.3.2.2.
Initial hold (min)  2.   
Final hold (min) 5.4. 40. 
I 718.760.744.722.723.
ReferenceAzodanlou, Darbellay, et al., 2003Dhanda, Pegg, et al., 2003Sebastian, Viallon-Fernandez, et al., 2003Valette, Fernandez, et al., 2003Yang, Yang, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200SPB-5DB-5AT-1HP-5
Column length (m) 30.60.60. 60.
Carrier gas H2 HeHeHe
Substrate      
Column diameter (mm) 0.320.320.32 0.32
Phase thickness (mum) 0.251.1. 1.
Tstart (C) 50.40.40.50.40.
Tend (C) 280.200.200.300.240.
Heat rate (K/min) 6.3.3.10.3.
Initial hold (min) 5.5.5.2. 
Final hold (min) 5.5.   
I 729.747.746.732.747.
ReferenceJirovetz, Ngassoum, et al., 2002Pérès, Begnaud, et al., 2002Joffraud, Leroi, et al., 2001Kelling, 2001García, Martín, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5SE-54HP-5DB-1
Column length (m) 30.50.25.30.60.
Carrier gas    N2 
Substrate      
Column diameter (mm) 0.320.320.310.250.25
Phase thickness (mum) 1.0.52 0.25 
Tstart (C) 40.35.35.40.30.
Tend (C) 200.250.250.240.200.
Heat rate (K/min) 3.2.4.4.4.
Initial hold (min) 5.15.3.3.25.
Final hold (min)  45. 10.20.
I 749.761.730.746.722.
ReferenceMeynier, Novelli, et al., 1999Boylston and Viniyard, 1998Ding, Deng, et al., 1998Kubec, Drhová, et al., 1998Buttery, Ling, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1DB-1DB-1
Column length (m) 60.60.30.30.30.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm) 0.320.320.20.20.32
Phase thickness (mum) 1.1.0.250.250.5
Tstart (C) 40.40.50.50.35.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 3.3.4.4.10.
Initial hold (min) 5.5.2.2.1.
Final hold (min) 2.2.   
I 744.746.740.732.736.
ReferenceKondjoyan, Viallon, et al., 1997Kondjoyan, Viallon, et al., 1997Rapior, Breheret, et al., 1997Rapior, Breheret, et al., 1997Robacker and Bartelt, 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-54DB-1HP-5OV-101OV-101
Column length (m) 25.30. 50.50.
Carrier gas HeHe N2N2
Substrate      
Column diameter (mm) 0.20.25 0.250.25
Phase thickness (mum) 0.50.25   
Tstart (C) 35.35.35.80.80.
Tend (C) 250.150.200.200.200.
Heat rate (K/min) 5.5.6.2.2.
Initial hold (min) 2. 2.  
Final hold (min)      
I 751.768.740.722.725.
ReferenceBellesia, Pinetti, et al., 1996Hanum, Sinha, et al., 1995Larsen and Frisvad, 1995Tamura, Nakamoto, et al., 1995Tamura, Nakamoto, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-1DB-5
Column length (m) 60.60.60.60.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.320.320.2
Phase thickness (mum) 1.1.0.25  
Tstart (C) 40.40.60.30.30.
Tend (C) 260.260.220.200.200.
Heat rate (K/min) 2.2.3.4.2.
Initial hold (min) 5.5. 25. 
Final hold (min) 60.60. 20. 
I 731.748.733.722.770.
ReferenceYu and Ho, 1995Yu, Wu, et al., 1994Güntert, Bertram, et al., 1992Hansen, Buttery, et al., 1992Sinha, Guyer, et al., 1992
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101DB-1DB-1
Column length (m) 50.50.50.60.60.
Carrier gas HeNitrogenNitrogen  
Substrate      
Column diameter (mm) 0.320.250.250.320.32
Phase thickness (mum) 0.5  0.250.25
Tstart (C) 50.70.80.50.50.
Tend (C) 250.200.200.250.250.
Heat rate (K/min) 4.2.2.4.4.
Initial hold (min)      
Final hold (min)      
I 726.738.730.722.722.
ReferenceMisharina, Golovnya, et al., 1991Sugisawa, Nakamura, et al., 1990Sugisawa, Nakamura, et al., 1990Flath, Matsumoto, et al., 1989Flath, Matsumoto, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1OV-101SF96+Igepal
Column length (m) 60.60.50.50.213.
Carrier gas    He 
Substrate      
Column diameter (mm) 0.320.320.320.310.7
Phase thickness (mum) 0.250.25   
Tstart (C) 50.50.0.0.45.
Tend (C) 250.250.250.225.200.
Heat rate (K/min) 4.4.3.3.2.
Initial hold (min)    1.30.
Final hold (min)      
I 723.724.719.719.732.
ReferenceFlath, Matsumoto, et al., 1989Flath, Matsumoto, et al., 1989Habu, Flath, et al., 1985del Rosario, de Lumen, et al., 1984Lorenz, Stern, et al., 1983
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase SP 2100
Column length (m) 40.
Carrier gas Helium
Substrate  
Column diameter (mm) 0.20
Phase thickness (mum)  
Tstart (C) 40.
Tend (C) 200.
Heat rate (K/min) 10.
Initial hold (min)  
Final hold (min)  
I 726.
ReferenceLabropoulos, Palmer, et al., 1982
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Labropoulos, Palmer, et al., 1982
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Notes

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