Home Symbol which looks like a small house Up Solid circle with an upward pointer in it

Methyl valerate

Data at NIST subscription sites:

NIST subscription sites provide data under the NIST Standard Reference Data Program, but require an annual fee to access. The purpose of the fee is to recover costs associated with the development of data collections included in such sites. Your institution may already be a subscriber. Follow the links above to find out more about the data in these sites and their terms of usage.


Van Den Dool and Kratz RI, polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-WaxZB-WaxCP-Wax 52CBAT-WaxDB-Wax
Column length (m) 30.30.60.60.15.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.320.53
Phase thickness (mum) 0.250.250.250.251.
Tstart (C) 40.40.40.65.40.
Tend (C) 250.250.250.250.220.
Heat rate (K/min) 5.5.4.2.5.
Initial hold (min) 2.2. 10.3.
Final hold (min) 5.5. 60.30.
I 1081.1085.1089.1075.1086.
ReferenceWu, Zorn, et al., 2007Wu, Zorn, et al., 2007Kourkoutas, Elmore, et al., 2006Pino and Marbot, 2001Peng, 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-WaxCarbowax 20MDB-WaxCarbowax 20MCarbowax 20M
Column length (m) 15.25.30.25.25.
Carrier gas He He  
Substrate      
Column diameter (mm) 0.530.310.250.310.31
Phase thickness (mum) 1.0.3   
Tstart (C) 40.50.40.50.50.
Tend (C) 220.200.200.200.200.
Heat rate (K/min) 5.2.2.2.2.
Initial hold (min) 3. 10.  
Final hold (min) 30.    
I 1096.1090.1084.1090.1095.
ReferencePeng, 2000Suárez and Duque, 1992Umano, Hagi, et al., 1992Suárez and Duque, 1991Suárez and Duque, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Packed
Active phase Carbowax 20M
Column length (m)  
Carrier gas  
Substrate Celite 545
Column diameter (mm)  
Phase thickness (mum)  
Tstart (C) 75.
Tend (C) 228.
Heat rate (K/min) 4.6
Initial hold (min)  
Final hold (min)  
I 1082.
Referencevan den Dool and Kratz, 1963
Comment MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Wu, Zorn, et al., 2007
Wu, S.; Zorn, H.; Krings, U.; Berger, R.G., Volatiles from submerged and surface-cultured beefsteak fungus, Fistulina hepatica, Flavour Fragr. J., 2007, 22, 1, 53-60, https://doi.org/10.1002/ffj.1758 . [all data]

Kourkoutas, Elmore, et al., 2006
Kourkoutas, D.; Elmore, J.S.; Mottram, D.S., Comparison of the volatile compositions and flavour properties of cantaloupe, Galia and honeydew muskmelons, Food Chem., 2006, 97, 1, 95-102, https://doi.org/10.1016/j.foodchem.2005.03.026 . [all data]

Pino and Marbot, 2001
Pino, J.A.; Marbot, R., Volatile flavor constituents of acerola (Malpighia emarginata DC.) fruit, J. Agric. Food Chem., 2001, 49, 12, 5880-5882, https://doi.org/10.1021/jf010270g . [all data]

Peng, 2000
Peng, C.T., Prediction of retention indices. V. Influence of electronic effects and column polarity on retention index, J. Chromatogr. A, 2000, 903, 1-2, 117-143, https://doi.org/10.1016/S0021-9673(00)00901-8 . [all data]

Suárez and Duque, 1992
Suárez, M.; Duque, C., Change in volatile compounds during lulo (Solanum vestissimum D.) fruit maturation, J. Agric. Food Chem., 1992, 40, 4, 647-649, https://doi.org/10.1021/jf00016a025 . [all data]

Umano, Hagi, et al., 1992
Umano, K.; Hagi, Y.; Nakahara, K.; Shoji, A.; Shibamoto, T., Volatile constituents of green and ripened pineapple (Aanas comosus [L.] Merr.), J. Agric. Food Chem., 1992, 40, 4, 599-603, https://doi.org/10.1021/jf00016a014 . [all data]

Suárez and Duque, 1991
Suárez, M.; Duque, C., Volatile constituents of lulo (Salanum vestissimum D.) fruit, J. Agric. Food Chem., 1991, 39, 8, 1498-1500, https://doi.org/10.1021/jf00008a026 . [all data]

van den Dool and Kratz, 1963
van den Dool, H.; Kratz, P. Dec., A generalization of the retention index system including linear temperature programmed gas-liquid partition chromatography, J. Chromatogr., 1963, 11, 463-471, https://doi.org/10.1016/S0021-9673(01)80947-X . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, References