2-Furancarboxaldehyde, 5-methyl-

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Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TR-5 MSSLB-5 MSSLB-5 MSPolydimethyl siloxane with 5 % Ph groupsPolydimethyl siloxane with 5 % Ph groups
Column length (m) 15.30.30.  
Carrier gas HeliumHeliumHelium  
Substrate      
Column diameter (mm) 0.250.250.25  
Phase thickness (μm) 0.250.250.25  
Program 35 0C (3 min) 2 0C/min -> 60 0C (3 min) 2 0C/min -> 80 0C (3 min) 4 0C/min -> 120 0C (3 min) 5 0C/min -> 150 0C (3 min) 15 0C/min -> 240 0C (10 min)not specifiednot specifiednot specifiednot specified
I 946.960.963.964.970.
ReferenceKurashov, Mitrukova, et al., 2014Mondello, 2012Mondello, 2012Robinson, Adams, et al., 2012Robinson, Adams, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSVF-5 MSRTX-5 MSRTX-5 MSZB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program 40 0C (1 min) 3 0C/min -> 150 0C (15 min) 5 0C/min -> 250 0C (5 min)not specified50 0C (5 min) 2 0C/min -> 100 0C (5 min) 5 0C/min -> 300 0Cnot specified45 0C 3 0C/min -> 230 0C (10 min) 10 0C/min -> 270 0C (21 min)
I 937.978.960.964.965.
ReferenceRodrigues, Hanson, et al., 2012Liu, Lu, et al., 2011Mebazaa, Mahmoudi, et al., 2009Mebazaa, Mahmoudi, et al., 2009de Simon, Estruelas, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SLB-5MSNonpolarHP-5 MSHP-5
Column length (m) 30.10. 30.30.
Carrier gas HeliumHelium Helium 
Substrate      
Column diameter (mm) 0.250.18 0.250.25
Phase thickness (μm) 0.250.18 0.250.25
Program not specifiednot specifiednot specified50 0C (2 min) 20 0C/min -> 80 0C (1 min) 20 0C -> 100 0C (1 min) 30 0C/min -> 230 0C (2 min)40 0C (2 min) 5 0C/min -> 80 0C 7 oC/min -> 160 0C 9 0C/min -> 200 0C 20 0C/min -> 280 0C (10 min)
I 962.960.978.964.968.
ReferenceBastos, Ishimoto, et al., 2008Risticevic, Carasek, et al., 2008Staples and Zeiger, 2008Wan Aida, Ho, et al., 2008Zhao, Li, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-1DB-5 MSHP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas  HeHeliumHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Program not specified40C(10min) => 2C/min => 200C(1min) => 2C/min => 250C (10min)45 0C (0.75 min) 10 0C/min -> 200 0C 30 0C/min -> 245 0C (1.25 min)50C(2min) => 20C/min => 80C (1min) => 20C/min => 100C(1min) => 30C/min => 230C(3min)not specified
I 972.926.969.964.962.
ReferenceZhao, Li, et al., 2008Bosch-Fuste, Riu-Aumatell, et al., 2007Cajka, Hajslova, et al., 2007Ho, Wan Aida, et al., 2007Machado, Bastos, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSPolydimethyl siloxane with 5 % Ph groupsCP Sil 5 CBSE-30
Column length (m) 30.30. 50. 
Carrier gas HeliumHe   
Substrate      
Column diameter (mm) 0.250.25 0.32 
Phase thickness (μm)  0.25 1.2 
Program 120 0C (2 min( 5 0C/min -> 200 0C 10 0C/min -> 290 0C (5 min)40C(1min) => 8C/min => 160C => 12C/min => 300C(5min)not specified36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250C(30min)not specified
I 927.986.962.928.942.
ReferenceSung, Stone, et al., 2007Li, Deng, et al., 2006Pino, Marbot, et al., 2005Counet, Ouwerx, et al., 2004Vinogradov, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBHP-5HP-5Methyl phenyl siloxane (not specified)
Column length (m) 50.50.30.30. 
Carrier gas  He   
Substrate      
Column diameter (mm) 0.320.320.250.25 
Phase thickness (μm) 1.21.20.250.25 
Program 36C => 20C/min => 85C => 1C/min => 145C=3C/min => 250C(30min)36C => 20C/min => 85C => 1C/min => 145C => 3C/min => 250Cnot specified40C (6min) => 2.5C/min => 150C => 90C/min => 250Cnot specified
I 931.929.976.945.966.
ReferenceCounet, Callemien, et al., 2002Guyot-Declerck, Renson, et al., 2002Jordán, Goodner, et al., 2002Jordán, Margaría, et al., 2002Poligne, Collignan, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1CP Sil 5 CBCP Sil 5 CBCP Sil 5 CBDB-5
Column length (m) 50.50.50.25.50.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.32 0.32
Phase thickness (μm) 0.52 1.20.390.25
Program 40C => 2C/min => 130C => 4C/min => 250C30C => 55C/min => 85C => 1C/min => 145C => 3C/min => 250C30C => 55C/min => 85C => 1C/min => 145C => 3C/min => 250Cnot specified40C(10min) => 3C/min => 95C => 10C/min => 270C(10min)
I 934.935.935.929.973.
ReferenceTeai, Claude-Lafontaine, et al., 2001Guyot, Scheirman, et al., 1999Guyot, Bouseta, et al., 1998Weyerstahl, Marschall, et al., 1998Mateo, Aguirrezábal, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1DB-5
Column length (m) 50.50.60.30.
Carrier gas HeHe He
Substrate     
Column diameter (mm) 0.320.320.320.32
Phase thickness (μm) 0.250.250.25 
Program 40C (10min) => 3C/min => 95C => 10C/min => 270C (10min)40C (10min) => 3C/min => 95C => 10C/min => 270C (10min)not specified35C => 40C/min => 50C(2min) => 4C/min => 240C
I 971.972.927.957.
ReferenceMateo and Zumalacárregui, 1996Mateo and Zumalacárregui, 1996Ciccioli, Cecinato, et al., 1994Schieberle and Grosch, 1994
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Rodrigues, Hanson, et al., 2012
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Staples and Zeiger, 2008
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Wan Aida, Ho, et al., 2008
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Zhao, Li, et al., 2008
Zhao, Y.; Li, J.; Xu, Y.; Duan, H.; Fan, W.; Zhao, G., EXtraction, preparation and identification of volatile compounds in Changyu XO brandy, Chinese J. Chromatogr., 2008, 26, 2, 212-222, https://doi.org/10.1016/S1872-2059(08)60014-0 . [all data]

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Ho, Wan Aida, et al., 2007
Ho, C.W.; Wan Aida, W.M.; Maskat, M.Y.; Osman, H., Changes in volatile compounds of palm sap (Arenga pinnata) during the heating process for production of palm sugar, Food Chem., 2007, 102, 4, 1156-1162, https://doi.org/10.1016/j.foodchem.2006.07.004 . [all data]

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Pino, Marbot, et al., 2005
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Counet, Ouwerx, et al., 2004
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Counet, Callemien, et al., 2002
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Notes

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, References