2-Furancarboxaldehyde, 5-methyl-

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5VF-5 MSHP-5 MSDB-5 MS
Column length (m) 30.25.30.30.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.200.250.250.20
Phase thickness (μm) 0.250.330.250.250.33
Tstart (C) 50.50.40.70.40.
Tend (C) 250.240.250.200.250.
Heat rate (K/min) 5.20.5.3.10.
Initial hold (min) 0.51.3.2.1.
Final hold (min) 0.5 3.18. 
I 977.955.966.969.980.
ReferenceFanaro, Duarte, et al., 2012Cais-Sokolinska, Majcher, et al., 2011Liu, Lu, et al., 2011Jerkovic and Marijanovic, 2010Majcher, Lawrowski, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSZB-5HP-5 MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 70.70.40.35.50.
Tend (C) 290.290.280.195.280.
Heat rate (K/min) 5.5.6.2.4.
Initial hold (min)   1.5. 
Final hold (min) 10.10.9.30. 
I 963.958.965.960.966.
ReferenceRadulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Harrison and Priest, 2009Kim and Chung, 2009Zhao, Zeng, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SLB-5MSDB-5DB-5DB-5
Column length (m) 30.10.60.30.60.
Carrier gas HeliumHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.250.180.320.250.32
Phase thickness (μm) 0.250.181.00.25 
Tstart (C) 60.40.35.40.60.
Tend (C) 220.295.240.240.250.
Heat rate (K/min) 3.10.15.3.4.
Initial hold (min)  1.57. 5.
Final hold (min)   10.  
I 957.973.978.951.971.
ReferenceBastos, Ishimoto, et al., 2008Risticevic, Carasek, et al., 2008Gogus, Ozel, et al., 2007Machado, Bastos, et al., 2007Fadel, Mageed, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSSPB-5MDN-5DB-1
Column length (m) 60.30.30.60.60.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.32
Phase thickness (μm)  0.250.250.250.25
Tstart (C) 50.50.60.40.35.
Tend (C) 250.280.250.270.230.
Heat rate (K/min) 4.5.4.4.2.
Initial hold (min) 5.4.2.4.4.
Final hold (min)  10.20.5.25.
I 971.969.963.962.923.
ReferenceFadel, Mageed, et al., 2006, 2Kim, Abd El-Aty, et al., 2006Pino, Marquez, et al., 2006van Loon, Linssen, et al., 2005Park, Lee, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-5SPB-5
Column length (m) 60.60.60.30.30.
Carrier gas HeHeHeH2Helium
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.35.35.60.60.
Tend (C) 230.230.230.280.250.
Heat rate (K/min) 2.2.2.4.4.
Initial hold (min) 4.4.4.10.2.
Final hold (min) 25.25.25.40.20.
I 924.925.926.962.962.
ReferencePark, Lee, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004Pino, Marbot, et al., 2003Pino, Marbot, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-1HP-5DB-1DB-1
Column length (m) 60.60.50.60.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 1.1.0.521.01.0
Tstart (C) 40.40.35.40.40.
Tend (C) 200.260.250.260.260.
Heat rate (K/min) 3.2.2.2.3.
Initial hold (min)   15.  
Final hold (min)   45.  
I 966.937.965.939.937.
ReferencePoligné, Collignan, et al., 2001Chen and Ho, 1999Boylston and Viniyard, 1998Chen and Ho, 1998Chen and Ho, 1998, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-1DB-1DB-1DB-1
Column length (m) 25.60.60.60.60.
Carrier gas  HeHe He
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (μm)  1.01.0 1.
Tstart (C) 35.40.40.30.40.
Tend (C) 250.280.280.200.260.
Heat rate (K/min) 4.2.2.4.2.
Initial hold (min)    25.5.
Final hold (min)    20.60.
I 931.934.934.927.950.
ReferenceOng, Acree, et al., 1998Tai and Ho, 1998Tai and Ho, 1998Buttery, Ling, et al., 1997Yu and Ho, 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-1DB-1
Column length (m) 60.60.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 1.01.00.250.250.25
Tstart (C) 40.40.50.50.50.
Tend (C) 260.260.240.240.240.
Heat rate (K/min) 2.2.3.3.5.
Initial hold (min) 5.5.5.5.3.
Final hold (min) 60.60.   
I 937.938.927.929.927.
ReferenceYu, Wu, et al., 1994Yu, Wu, et al., 1994Shiota, 1993Shiota, 1993Shiota, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5OV-101DB-1DB-1
Column length (m) 30.60.50.60.60.
Carrier gas He Nitrogen  
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 50.40.70.50.50.
Tend (C) 240.250.200.250.250.
Heat rate (K/min) 5.2.2.4.4.
Initial hold (min) 3.5.   
Final hold (min)      
I 929.965.930.926.926.
ReferenceShiota, 1993Lee, Macku, et al., 1991Sugisawa, Nakamura, et al., 1990Flath, Matsumoto, et al., 1989Flath, Matsumoto, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-5DB-1OV-1
Column length (m) 30.50.183.
Carrier gas Hydrogen N2
Substrate    
Column diameter (mm) 0.350.320.762
Phase thickness (μm) 1.0  
Tstart (C) 45.0.0.
Tend (C) 220.250.230.
Heat rate (K/min) 2.3.1.
Initial hold (min)    
Final hold (min)    
I 973.926.932.
ReferenceGeorgilopoulos and Gallois, 1988Habu, Flath, et al., 1985Schreyen, Dirinck, et al., 1979
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Fanaro, Duarte, et al., 2012
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Harrison and Priest, 2009
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Kim and Chung, 2009
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Zhao, Zeng, et al., 2009
Zhao, C.; Zeng, Y.; Wan, M.; Li, R.; Liang, Y.; Li, C.; Zeng, Z.; Chau, F.-T., Comparative analysis of essential oils from eight herbal medicines with pungent flavor and cool nature by GC-MS and chemometric resolution methods, J. Sep. Sci., 2009, 32, 4, 660-670, https://doi.org/10.1002/jssc.200800484 . [all data]

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Park, Lee, et al., 2004
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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References