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2-Furancarboxaldehyde, 5-methyl-

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSDB-5VF-5 MSHP-5 MSDB-5 MS
Column length (m) 30.25.30.30.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.200.250.250.20
Phase thickness (mum) 0.250.330.250.250.33
Tstart (C) 50.50.40.70.40.
Tend (C) 250.240.250.200.250.
Heat rate (K/min) 5.20.5.3.10.
Initial hold (min) 0.51.3.2.1.
Final hold (min) 0.5 3.18. 
I 977.955.966.969.980.
ReferenceFanaro, Duarte, et al., 2012Cais-Sokolinska, Majcher, et al., 2011Liu, Lu, et al., 2011Jerkovic and Marijanovic, 2010Majcher, Lawrowski, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5 MSZB-5HP-5 MSHP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.70.40.35.50.
Tend (C) 290.290.280.195.280.
Heat rate (K/min) 5.5.6.2.4.
Initial hold (min)   1.5. 
Final hold (min) 10.10.9.30. 
I 963.958.965.960.966.
ReferenceRadulovic, Blagojevic, et al., 2010Radulovic, Dordevic, et al., 2010Harrison and Priest, 2009Kim and Chung, 2009Zhao, Zeng, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SLB-5MSDB-5DB-5DB-5
Column length (m) 30.10.60.30.60.
Carrier gas HeliumHeliumHeliumHeHe
Substrate      
Column diameter (mm) 0.250.180.320.250.32
Phase thickness (mum) 0.250.181.00.25 
Tstart (C) 60.40.35.40.60.
Tend (C) 220.295.240.240.250.
Heat rate (K/min) 3.10.15.3.4.
Initial hold (min)  1.57. 5.
Final hold (min)   10.  
I 957.973.978.951.971.
ReferenceBastos, Ishimoto, et al., 2008Risticevic, Carasek, et al., 2008Gogus, Ozel, et al., 2007Machado, Bastos, et al., 2007Fadel, Mageed, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSSPB-5MDN-5DB-1
Column length (m) 60.30.30.60.60.
Carrier gas HeHeHeliumHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.32
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 50.50.60.40.35.
Tend (C) 250.280.250.270.230.
Heat rate (K/min) 4.5.4.4.2.
Initial hold (min) 5.4.2.4.4.
Final hold (min)  10.20.5.25.
I 971.969.963.962.923.
ReferenceFadel, Mageed, et al., 2006, 2Kim, Abd El-Aty, et al., 2006Pino, Marquez, et al., 2006van Loon, Linssen, et al., 2005Park, Lee, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-5SPB-5
Column length (m) 60.60.60.30.30.
Carrier gas HeHeHeH2Helium
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 35.35.35.60.60.
Tend (C) 230.230.230.280.250.
Heat rate (K/min) 2.2.2.4.4.
Initial hold (min) 4.4.4.10.2.
Final hold (min) 25.25.25.40.20.
I 924.925.926.962.962.
ReferencePark, Lee, et al., 2004Park, Lee, et al., 2004Park, Lee, et al., 2004Pino, Marbot, et al., 2003Pino, Marbot, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-1HP-5DB-1DB-1
Column length (m) 60.60.50.60.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (mum) 1.1.0.521.01.0
Tstart (C) 40.40.35.40.40.
Tend (C) 200.260.250.260.260.
Heat rate (K/min) 3.2.2.2.3.
Initial hold (min)   15.  
Final hold (min)   45.  
I 966.937.965.939.937.
ReferencePoligné, Collignan, et al., 2001Chen and Ho, 1999Boylston and Viniyard, 1998Chen and Ho, 1998Chen and Ho, 1998, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-1DB-1DB-1DB-1
Column length (m) 25.60.60.60.60.
Carrier gas  HeHe He
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum)  1.01.0 1.
Tstart (C) 35.40.40.30.40.
Tend (C) 250.280.280.200.260.
Heat rate (K/min) 4.2.2.4.2.
Initial hold (min)    25.5.
Final hold (min)    20.60.
I 931.934.934.927.950.
ReferenceOng, Acree, et al., 1998Tai and Ho, 1998Tai and Ho, 1998Buttery, Ling, et al., 1997Yu and Ho, 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1DB-1DB-1DB-1
Column length (m) 60.60.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 1.01.00.250.250.25
Tstart (C) 40.40.50.50.50.
Tend (C) 260.260.240.240.240.
Heat rate (K/min) 2.2.3.3.5.
Initial hold (min) 5.5.5.5.3.
Final hold (min) 60.60.   
I 937.938.927.929.927.
ReferenceYu, Wu, et al., 1994Yu, Wu, et al., 1994Shiota, 1993Shiota, 1993Shiota, 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5OV-101DB-1DB-1
Column length (m) 30.60.50.60.60.
Carrier gas He Nitrogen  
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 50.40.70.50.50.
Tend (C) 240.250.200.250.250.
Heat rate (K/min) 5.2.2.4.4.
Initial hold (min) 3.5.   
Final hold (min)      
I 929.965.930.926.926.
ReferenceShiota, 1993Lee, Macku, et al., 1991Sugisawa, Nakamura, et al., 1990Flath, Matsumoto, et al., 1989Flath, Matsumoto, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase DB-5DB-1OV-1
Column length (m) 30.50.183.
Carrier gas Hydrogen N2
Substrate    
Column diameter (mm) 0.350.320.762
Phase thickness (mum) 1.0  
Tstart (C) 45.0.0.
Tend (C) 220.250.230.
Heat rate (K/min) 2.3.1.
Initial hold (min)    
Final hold (min)    
I 973.926.932.
ReferenceGeorgilopoulos and Gallois, 1988Habu, Flath, et al., 1985Schreyen, Dirinck, et al., 1979
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Fanaro, Duarte, et al., 2012
Fanaro, G.B.; Duarte, R.C.; Santillo, A.G.; Pinto e Silva, M.E.M.; Purgatto, E.; Villavicento, A.L.C.H., Evaluation of «gamma»-radiation on oolong tea odor volatiles, Radiation Phys. Chem., 2012, 81, 8, 1152-1156, https://doi.org/10.1016/j.radphyschem.2011.11.061 . [all data]

Cais-Sokolinska, Majcher, et al., 2011
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Liu, Lu, et al., 2011
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Jerkovic, I.; Marijanovic, Z., Oak (Quercus frainetto Ten.) honeydaw honey - approach to screening of volatile organic composition and antioxidant capacity (DPPH and FRAP assay), Molecules, 2010, 15, 5, 3744-3756, https://doi.org/10.3390/molecules15053744 . [all data]

Majcher, Lawrowski, et al., 2010
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Radulovic, Blagojevic, et al., 2010
Radulovic, N.; Blagojevic, P.; Palic, R., Comparative study of the leaf volatiles of Arctostaphylos uva-ursi (L.) Spreng. and Vaccinium vitis-idaea L. (Ericaceae), Molecules, 2010, 15, 9, 6168-6185, https://doi.org/10.3390/molecules15096168 . [all data]

Radulovic, Dordevic, et al., 2010
Radulovic, N.; Dordevic, N.; Markovic, M.; Palic, R., Volatile constituents of Glechoma Hirsuta Waldst. Kit. and G. Hederacea L. (Lamiaceae), Bull. Chem. Soc. Ethiop., 2010, 24, 1, 67-76, https://doi.org/10.4314/bcse.v24i1.52962 . [all data]

Harrison and Priest, 2009
Harrison, B.M.; Priest, F.G., Composition of peaks used in the preparation of malt for Scotch Whisky production - influence of geographical source and extraction depth, J. Agric. Food Chem., 2009, 57, 6, 2385-2391, https://doi.org/10.1021/jf803556y . [all data]

Kim and Chung, 2009
Kim, J.-S.; Chung, H.Y., GC-MS analysis of the volatile components in dried boxthorn (Lycium chimensis) Fruit, J. Korean Soc. Appl. Biol. Chem., 2009, 52, 5, 516-524, https://doi.org/10.3839/jksabc.2009.088 . [all data]

Zhao, Zeng, et al., 2009
Zhao, C.; Zeng, Y.; Wan, M.; Li, R.; Liang, Y.; Li, C.; Zeng, Z.; Chau, F.-T., Comparative analysis of essential oils from eight herbal medicines with pungent flavor and cool nature by GC-MS and chemometric resolution methods, J. Sep. Sci., 2009, 32, 4, 660-670, https://doi.org/10.1002/jssc.200800484 . [all data]

Bastos, Ishimoto, et al., 2008
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Gogus, Ozel, et al., 2007
Gogus, F.; Ozel, M.Z.; Lewis, A.C., The Effect of Various Drying Techniques on Apricot Volatiles Analysed Using Direct Desorption-GC-TOF/MS, Talanta, 2007, 73, 2, 321-325, https://doi.org/10.1016/j.talanta.2007.03.048 . [all data]

Machado, Bastos, et al., 2007
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Fadel, Mageed, et al., 2006
Fadel, H.H.M.; Mageed, M.A.A.; Lotfy, S.N., Quality and flavour stability of coffee substitute prepared by extrusion of wheat germ and chicory roots, Amino Acids, 2006, https://doi.org/10.1007/s007260200008 . [all data]

Fadel, Mageed, et al., 2006, 2
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Kim, Abd El-Aty, et al., 2006
Kim, M.R.; Abd El-Aty, A.M.; Kim, I.S.; Shim, J.H., Determination of volatile flavor components in danggui cultivars by solvent free injection and hydrodistillation followed by gas chromatographic-mass spectrometric analysis, J. Chromatogr. A, 2006, 1116, 1-2, 259-264, https://doi.org/10.1016/j.chroma.2006.03.060 . [all data]

Pino, Marquez, et al., 2006
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van Loon, Linssen, et al., 2005
van Loon, W.A.M.; Linssen, J.P.H.; Legger, A.; Posthumus, M.A.; Voragen, A.G.J., Identification and olfactometry of French fries flavour extracted at mouth conditions, Food Chem., 2005, 90, 3, 417-425, https://doi.org/10.1016/j.foodchem.2004.05.005 . [all data]

Park, Lee, et al., 2004
Park, B.-S.; Lee, K.-G.; Takeoka, G.R., Comparison of three sample preparation methods on the recovery of volatiles from taheebo (Tabebuia impetiginosa Martius ex DC), Flavour Fragr. J., 2004, 19, 4, 287-292, https://doi.org/10.1002/ffj.1345 . [all data]

Pino, Marbot, et al., 2003
Pino, J.A.; Marbot, R.; Fuentes, V., Characterization of volatiles in Bullock's heart (Annona reticulata L.) fruit cultivars from Cuba, J. Agric. Food Chem., 2003, 51, 13, 3836-3839, https://doi.org/10.1021/jf020733y . [all data]

Pino, Marbot, et al., 2002
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Poligné, Collignan, et al., 2001
Poligné, I.; Collignan, A.; Trystram, G., Characterization of traditional processing of pork meat into boucané, Meat Sci., 2001, 59, 4, 377-389, https://doi.org/10.1016/S0309-1740(01)00090-0 . [all data]

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Chen and Ho, 1998
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Tai, C.-Y.; Ho, C.-T., Influence of glutathione oxidation and pH on thermal formation of Maillard-type volatile compounds, J. Agric. Food Chem., 1998, 46, 6, 2260-2265, https://doi.org/10.1021/jf971111t . [all data]

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Yu and Ho, 1995
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Sugisawa, Nakamura, et al., 1990
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Habu, Flath, et al., 1985
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Schreyen, Dirinck, et al., 1979
Schreyen, L.; Dirinck, P.; Sandra, P.; Schamp, N., Flavor analysis of quince, J. Agric. Food Chem., 1979, 27, 4, 872-876, https://doi.org/10.1021/jf60224a058 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References