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(1S,4aS,7R,8aS)-1,4a-Dimethyl-7-(prop-1-en-2-yl)decahydronaphthalen-1-ol


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryCP Sil 5 CB1651.Kaul and Vats, 19985. K/min; Column length: 25. m; Column diameter: 0.25 mm; Tstart: 60. C; Tend: 280. C

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillarySPB-11630.Salgueiro L.R., Pinto E., et al., 200630. m/0.2 mm/0.2 «mu»m, He, 3. K/min, 220. C @ 15. min; Tstart: 70. C
CapillaryDB-51667.Su, Ho, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 50. C @ 2. min, 5. K/min; Tend: 250. C
CapillaryDB-11653.Tchoumbougnang, Zollo, et al., 200530. m/0.25 mm/0.25 «mu»m, N2, 5. K/min; Tstart: 50. C; Tend: 200. C
CapillaryRTX-11645.Cavalli, Tomi, et al., 200360. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C

Van Den Dool and Kratz RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-5MS1666.5Andriamaharavo, 201430. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)
CapillaryHP-5MS1674.6Andriamaharavo, 201430. m/0.25 mm/0.25 «mu»m, He; Program: 60C (1 min) => 5 C/min => 210C => 10 C/min => 280C (15 min)

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryRTX-Wax2222.Cavalli, Tomi, et al., 200360. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 230. C @ 45. min; Tstart: 60. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-51667.Scrivanti, Anton, et al., 200930. m/0.25 mm/0.25 «mu»m, Nitrogen, 2. K/min; Tstart: 40. C; Tend: 230. C
CapillaryCP Sil 5 CB1646.Baran, von Reuss, et al., 200730. m/0.32 mm/0.25 «mu»m, N2, 4. K/min; Tstart: 60. C; Tend: 300. C
CapillaryHP-51666.Figuérédo, Cabassu, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 50. C @ 5. min, 5. K/min, 300. C @ 5. min
CapillaryHP-51667.Utsunomia, Kawata, et al., 200530. m/0.32 mm/0.25 «mu»m, Helium, 4. K/min, 300. C @ 5. min; Tstart: 40. C
CapillaryRTX-5Sil1677.Dudai, Larkov, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 4. K/min, 200. C @ 10. min; Tstart: 70. C
CapillaryDB-51654.Abreu and Noronha, 1997He, 3. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 60. C; Tend: 250. C
CapillaryDB-11629.Salgueiro, Vila, et al., 19976. K/min; Tstart: 80. C; Tend: 220. C
CapillaryDB-11647.Kesselmans and Wijnberg, 199260. m/0.25 mm/0.25 «mu»m, Hydrogen, 4. K/min, 238. C @ 8. min; Tstart: 50. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryDB-11626.Nogueira, Marcelo-Curto, et al., 200830. m/0.25 mm/0.25 «mu»m, He; Program: 45C => 3C/min => 175C => 15C/min => 300C (10min)
CapillaryHP-11663.Merle, Verdeguer, et al., 200730. m/0.2 mm/0.33 «mu»m, He; Program: 60C(5min) => 3C/min => 180C => 20C/min => 280C(10min)
CapillaryPolydimethyl siloxane1665.Werka, Boehme, et al., 2007Program: not specified
CapillaryDB-5MS1627.Bagci and Baser, 200530. m/0.25 mm/0.25 «mu»m; Program: 70C(2min) => 10C/min => 150C(15min) => 5C/min => 240C
CapillaryDB-11629.Miguel, Simões, et al., 200430. m/0.25 mm/0.25 «mu»m, He; Program: 45C => 3C/min => 175C => 15C/min => 300C (10min)
CapillaryDB-11626.Faleiro, Miguel, et al., 200330. m/0.25 mm/0.25 «mu»m, He; Program: 45C => 3C/min => 175C => 15C/min => 300C (10min)
CapillaryDB-11626.Figueiredo, Miguel, et al., 200130. m/0.25 mm/0.25 «mu»m; Program: 45 0C 3 K/min -> 175 0C 15 K/min -> 300 0C (10 min)

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryInnowax FSC2262.Lourens, Reddy, et al., 2004Helium, 60. C @ 10. min, 4. K/min; Column length: 60. m; Column diameter: 0.25 mm; Tend: 220. C
CapillaryDB-Wax2247.Abreu and Noronha, 1997He, 3. K/min; Column length: 30. m; Column diameter: 0.32 mm; Tstart: 60. C; Tend: 250. C
CapillaryDB-Wax2247.Kesselmans and Wijnberg, 199260. m/0.25 mm/0.25 «mu»m, Hydrogen, 4. K/min, 238. C @ 8. min; Tstart: 50. C

Normal alkane RI, polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryCarbowax 20M2218.Merle, Verdeguer, et al., 2007He; Column length: 30. m; Program: 60C(5min) => 3C/min => 180C => 20C/min => 280C(10min)
CapillaryHP-Innowax FSC2264.Suleimenov Y.M., Atazhanova G.A., et al., 200660. m/0.25 mm/0.25 «mu»m, He; Program: 60(10min) => 4C/min => 220C(10min) => 1C/min => 240C
CapillaryInnowax FSC2264.Baser, Özek, et al., 200460. m/0.25 mm/0.25 «mu»m, He; Program: 60C(10min) => 4C/min => 220C(10min) => 1C/min => 240C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kaul and Vats, 1998
Kaul, V.K.; Vats, S.K., Essential oil composition of Bothriochloa pertusa and phyletic relationship in aromatic grasses, Biochem. Syst. Ecol., 1998, 26, 3, 347-356, https://doi.org/10.1016/S0305-1978(97)00103-8 . [all data]

Salgueiro L.R., Pinto E., et al., 2006
Salgueiro L.R.; Pinto E.; Goncalves M.J.; Costa I.; Palmeira A.; Cavaleiro C.; Pina-Vaz C.; Rodrigues A.G.; Martinez-De-Oliveira J., Antifungal activity of the essential oil of Thymus capitellatus against Candida, Aspergillus and dermatophyte strains, Flavour Fragr. J., 2006, 21, 5, 749-753, https://doi.org/10.1002/ffj.1610 . [all data]

Su, Ho, et al., 2006
Su, Y.C.; Ho, C.L.; Wang, E.I.C., Analysis of leaf essential oils from the indigenous five conifers of Taiwan, Flavour Fragr. J., 2006, 21, 3, 447-452, https://doi.org/10.1002/ffj.1685 . [all data]

Tchoumbougnang, Zollo, et al., 2005
Tchoumbougnang, F.; Zollo, P.H.A.; Boyom, F.F.; Nyegue, M.A.; Bessière, J.M.; Menut, C., Aromatic plants of tropical Central Africa. XLVIII. Comparative study of the essential oils of four Hyptis species from Cameroon: H. lanceolata Poit., H. pectinata (L.) Poit., H. spicigera Lam. and H. suaveolens Poit., Flavour Fragr. J., 2005, 20, 3, 340-343, https://doi.org/10.1002/ffj.1441 . [all data]

Cavalli, Tomi, et al., 2003
Cavalli, J.-F.; Tomi, F.; Bernardini, A.-F.; Casanova, J., Composition and chemical variability of the bark oil of Cedrelopsis grevei H. Baillon from Madagascar, Flavour Fragr. J., 2003, 18, 6, 532-538, https://doi.org/10.1002/ffj.1263 . [all data]

Andriamaharavo, 2014
Andriamaharavo, N.R., Retention Data. NIST Mass Spectrometry Data Center., NIST Mass Spectrometry Data Center, 2014. [all data]

Scrivanti, Anton, et al., 2009
Scrivanti, L.R.; Anton, A.M.; Zygadlo, J.A., Essential oil conposition of Bothriochloa Kuntze (Poaceae) from South America and their chemotaxonomy, Biochem. Systematics Ecol., 2009, 37, 3, 206-213, https://doi.org/10.1016/j.bse.2009.03.009 . [all data]

Baran, von Reuss, et al., 2007
Baran, S.; von Reuss, S.H.; König, W.A.; Kalemba, D., Composition of the essential oil of Abies koreana Wils., Flavour Fragr. J., 2007, 22, 1, 78-83, https://doi.org/10.1002/ffj.1762 . [all data]

Figuérédo, Cabassu, et al., 2006
Figuérédo, G.; Cabassu, P.; Chalchat, J.-C.; Pasquier, B., Studies of Mediterranean oregano populations. VIII. Chemical composition of essential oils of oreganos of various origins, Flavour Fragr. J., 2006, 21, 1, 134-139, https://doi.org/10.1002/ffj.1543 . [all data]

Utsunomia, Kawata, et al., 2005
Utsunomia, H.; Kawata, J.; Chanoki, W.; Shirakawa, N.; Miyazawa, M., Components of Essential Oil from Woods of Prunus mume Sieb. at Zucc., J. Oleo Sci., 2005, 54, 11, 609-612, https://doi.org/10.5650/jos.54.609 . [all data]

Dudai, Larkov, et al., 2003
Dudai, N.; Larkov, O.; Chaimovitsh, D.; Lewinsohn, E.; Freiman, L.; Ravid, U., Essential oil compounds of Origanum dayi Post, Flavour Fragr. J., 2003, 18, 4, 334-337, https://doi.org/10.1002/ffj.1237 . [all data]

Abreu and Noronha, 1997
Abreu, P.M.; Noronha, R.G., Volatile constituents of the rhizomes of Aframomum alboviolaceum (Ridley) K. Schum. from Guinea-Bissau, Flavour Fragr. J., 1997, 12, 2, 79-83, https://doi.org/10.1002/(SICI)1099-1026(199703)12:2<79::AID-FFJ617>3.0.CO;2-7 . [all data]

Salgueiro, Vila, et al., 1997
Salgueiro, L.R.; Vila, R.; Tomi, F.; Figueiredo, A.C.; Barroso, J.G.; Cañigueral, S.; Casanova, J.; da Cunha, A.P.; Adzet, T., Variability of essential oils of Thymus caespititius from Portugal, Phytochemistry, 1997, 45, 2, 307-311, https://doi.org/10.1016/S0031-9422(96)00872-2 . [all data]

Kesselmans and Wijnberg, 1992
Kesselmans, R.P.W.; Wijnberg, J.B.P.A., Chromatographic and spectroscopic data of all stereoisomers of eudesm-11-en-4-ol, J. Essent. Oil Res., 1992, 4, 3, 201-217, https://doi.org/10.1080/10412905.1992.9698050 . [all data]

Nogueira, Marcelo-Curto, et al., 2008
Nogueira, T.; Marcelo-Curto, M.J.; Cristina Figueiredo, A.; Barroso, J.G.; Pedro, L.G.; Rubiolo, P.; Bicchi, C., Chemotaxonomy of Hypericum genus from Portugal: Geographical distribution and essential oils composition of Hypericum perfoliatum, Hypericum humifusum, Hypericum linarifolium and Hypericum pulchrum, Biochem. Syst. Ecol., 2008, 36, 1, 40-50, https://doi.org/10.1016/j.bse.2007.07.004 . [all data]

Merle, Verdeguer, et al., 2007
Merle, H.; Verdeguer, M.; Blázquez, M.A.; Boira, H., Chemical composition of the essential oils from Eriocephalus africanus L. var. africanus populations growing in Spain, Flavour Fragr. J., 2007, 22, 6, 461-464, https://doi.org/10.1002/ffj.1821 . [all data]

Werka, Boehme, et al., 2007
Werka, J.S.; Boehme, A.K.; Setzer, W.N., Biological activities of essential oils from Monteverde, Costa Rica, Natural Product Communications, 2007, 2, 12, 1215-1219. [all data]

Bagci and Baser, 2005
Bagci, E.; Baser, K.H.C., Study of the essential oils of Thymus haussknechtii Velen and Thymus kotschyanus Boiss. et Hohen var. kotschyanus (Lamiaceae) taxa from the eastern Anatolian region in Turkey, Flavour Fragr. J., 2005, 20, 2, 199-202, https://doi.org/10.1002/ffj.1397 . [all data]

Miguel, Simões, et al., 2004
Miguel, G.; Simões, M.; Figueiredo, A.C.; Barroso, J.G.; Pedro, L.G.; Carvalho, L., Composition and antioxidant activities of the essential oils of Thymus caespititius, Thymus camphoratus and Thymus mastichina, Food Chem., 2004, 86, 2, 183-188, https://doi.org/10.1016/j.foodchem.2003.08.031 . [all data]

Faleiro, Miguel, et al., 2003
Faleiro, M.L.; Miguel, M.G.; Ladeiro, F.; Venancio, F.; Tavares, R.; Brito, J.C.; Figueiredo, A.C.; Barroso, J.G.; Pedro, L.G., Antimicrobial activity of essential oils isolated from Portuguese endemic species of Thymus, Lett. Appl. Microbiol., 2003, 36, 1, 35-40, https://doi.org/10.1046/j.1472-765X.2003.01259.x . [all data]

Figueiredo, Miguel, et al., 2001
Figueiredo, A.C.; Miguel, M.G.; Duarte, A.M.F.; Barroso, J.G.; Pedro, L.G., Essential oil composition of Thymus lotocephallus G. López R. Morales, collected during flowering and vegetative phases, Flavour Fragr. J., 2001, 16, 6, 417-421, https://doi.org/10.1002/ffj.1028 . [all data]

Lourens, Reddy, et al., 2004
Lourens, A.C.U.; Reddy, D.; Baser, K.H.C.; Viljoen, A.M.; Van Vuuren, S.F., In vitro Biological Activity and Essential Oil Composition of Four Indigenous South Africal Helichrysum Species, J. Ethnopharmacol., 2004, 95, 2-3, 253-258, https://doi.org/10.1016/j.jep.2004.07.027 . [all data]

Suleimenov Y.M., Atazhanova G.A., et al., 2006
Suleimenov Y.M.; Atazhanova G.A.; Ozek T.; Demirci B.; Kulyyasov A.T.; Adekenov S.M.; Baser K.H.C., Essential oil composition of three species of Achillea from Kazakhstan, Chem. Nat. Compd. (Engl. Transl.), 2006, 37, 5, 447-450, https://doi.org/10.1023/A:1014471326724 . [all data]

Baser, Özek, et al., 2004
Baser, K.H.C.; Özek, T.; Kirimer, N.; Deliorman, D.; Ergun, F., Composition of the essential oils of Galium aparine L. and Galium odoratum (L.) Scop. from Turkey, J. Essent. Oil Res., 2004, 16, 4, 305-307, https://doi.org/10.1080/10412905.2004.9698728 . [all data]


Notes

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