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Oxazepam


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Polydimethyl siloxanesCP Sil 5 CBCP Sil 5 CBSPB-1BP-1
Column length (m)  10.10.25.12.
Carrier gas    HeHe
Substrate    Chromosorb W(100-120 mesh) 
Column diameter (mm)  0.530.53 0.22
Phase thickness (mum)  5.25.20.40.25
Program not specified100 0C (2 min) 20 0C/min -> 180 0C 7.5 0C/min -> 280 0C (6 min)not specified 120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)
I 2336.2310.2336.2314.2300.
ReferenceSchutz and Wollrab A., 1988Bogusz, Bialka, et al., 1986Bogusz, Bialka, et al., 1986Chiarotti, de Giovanni, et al., 1986Stowell and Wilson, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryOther
Active phase BP-1Methyl Silicone
Column length (m) 12. 
Carrier gas He 
Substrate   
Column diameter (mm) 0.22 
Phase thickness (mum) 0.25 
Program not specifiednot specified
I 2335.2336.
ReferenceStowell and Wilson, 1985Ardrey and Moffat, 1981
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Schutz and Wollrab A., 1988
Schutz, H.; Wollrab A., The significance of the retention index in toxicologic analysis II, Pharmazie in unzerer Zeit, 1988, 17, 4, 97-101. [all data]

Bogusz, Bialka, et al., 1986
Bogusz, M.; Bialka, J.; Gierz, J.; Klys, M., Use of short, wide-bore capillary columns in GC toxicological screening, J. Anal. Toxicol., 1986, 10, 4, 135-138, https://doi.org/10.1093/jat/10.4.135 . [all data]

Chiarotti, de Giovanni, et al., 1986
Chiarotti, M.; de Giovanni, N.; Fiori, A., Analysis of Benzodiazepines. I. Chromatographic Identification, J. Chromatogr., 1986, 358, 169-178, https://doi.org/10.1016/S0021-9673(01)90326-7 . [all data]

Stowell and Wilson, 1985
Stowell, A.; Wilson, L., Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]

Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C., Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase, J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1 . [all data]


Notes

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