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dl-Isopulegol


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-11141.Abella, Cortella, et al., 200030. m/0.25 mm/0.25 «mu»m, 4. K/min; Tstart: 80. C; Tend: 225. C
CapillaryDB-51156.Adams, 200030. m/0.26 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C

Kovats' RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillaryHP-51156.Shellie and Marriott, 200330. m/0.25 mm/0.25 «mu»m, He; Program: not specified

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-11159.Castilho, Liu, et al., 200750. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C
CapillaryDB-51155.Hongratanaworakit and Buchbauer, 200730. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 60. C; Tend: 246. C
CapillaryDB-51160.Su, Ho, et al., 200630. m/0.25 mm/0.25 «mu»m, He, 50. C @ 2. min, 5. K/min; Tend: 250. C
CapillaryHP-5MS1155.Salido, Altarejos, et al., 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 50. C; Tend: 250. C
CapillaryMS51157.Shao, Marriott, et al., 200325. m/0.25 mm/0.25 «mu»m, 3. K/min; Tstart: 40. C; Tend: 180. C
CapillaryHP-51154.Shellie and Marriott, 200330. m/0.25 mm/0.25 «mu»m, He, 3. K/min; Tstart: 40. C; Tend: 240. C

Van Den Dool and Kratz RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryBP-201632.Castilho, Liu, et al., 200750. m/0.22 mm/0.25 «mu»m, He, 2. K/min, 220. C @ 20. min; Tstart: 60. C

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryHP-51150.Bertoli, Lepnardi, et al., 201130. m/0.25 mm/0.25 «mu»m, Helium, 3. K/min; Tstart: 60. C; Tend: 240. C
CapillaryHP-5 MS1156.Adams, Beauchamp, et al., 200730. m/0.25 mm/0.25 «mu»m, Helium, 50. C @ 10. min, 3. K/min, 230. C @ 10. min
CapillaryHP-51145.N/A30. m/0.32 mm/0.25 «mu»m, Helium, 40. C @ 2. min, 5. K/min, 250. C @ 5. min
CapillaryHP-51146.Farsam, Amanlou, et al., 200330. m/0.25 mm/0.25 «mu»m, Helium, 60. C @ 2. min, 4. K/min; Tend: 240. C

Normal alkane RI, non-polar column, custom temperature program

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Column type Active phase I Reference Comment
CapillarySE-301154.Vinogradov, 2004Program: not specified
CapillaryHP-11137.Betts, 200012. m/0.20 mm/0.33 «mu»m, He; Program: 40 0C 6.7 0C/min -> 87 0C (9 min) 10 0C/min -> 187 0C
CapillaryPolydimethyl siloxanes1154.Zenkevich, 1997Program: not specified

Normal alkane RI, polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryZB-Wax1564.N/A30. m/0.32 mm/0.25 «mu»m, Helium, 40. C @ 2. min, 5. K/min, 250. C @ 5. min
CapillaryBP-201585.Bignell, Dunlop, et al., 199725. m/0.33 mm/0.5 «mu»m, 5. K/min; Tstart: 80. C; Tend: 220. C

References

Go To: Top, Gas Chromatography, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Abella, Cortella, et al., 2000
Abella, L.; Cortella, A.R.; Velasco-Negueruela, A.; Pérez-Alonso, M.J., Ethnobotany, volatile oils and secretion tissues of Werneria poposa from Argentina, Pharm. Biol., 2000, 38, 3, 197-203, https://doi.org/10.1076/1388-0209(200007)3831-SFT197 . [all data]

Adams, 2000
Adams, R.P., The serrate leaf margined Juniperus (Section Sabina) of the western hemisphere: systematics and evolution based on leaf essential oils and Random Amplified Polymorphic DNAs (RAPDs), Biochem. Syst. Ecol., 2000, 28, 10, 975-989, https://doi.org/10.1016/S0305-1978(00)00022-3 . [all data]

Shellie and Marriott, 2003
Shellie, R.A.; Marriott, P.J., Comprehensive two-dimensional gas chromatography-mass spectrometry analysis of Pelargonium graveolens essential oil using rapid scanning quadrupole mass spectrometry, Analyst, 2003, 128, 7, 879-883, https://doi.org/10.1039/b304371a . [all data]

Castilho, Liu, et al., 2007
Castilho, P.; Liu, K.; Rodrigues, A.I.; Feio, S.; Tomi, F.; Casanova, J., Composition and antimicrobial activity of the essential oil of Clinopodium ascendens (Jordan) Sampaio from Madeira, Flavour Fragr. J., 2007, 22, 2, 139-144, https://doi.org/10.1002/ffj.1771 . [all data]

Hongratanaworakit and Buchbauer, 2007
Hongratanaworakit, T.; Buchbauer, G., Chemical composition and stimulating effect of Citrus hystrix oil on humans, Flavour Fragr. J., 2007, 22, 5, 443-449, https://doi.org/10.1002/ffj.1820 . [all data]

Su, Ho, et al., 2006
Su, Y.-C.; Ho, C.-L.; Wang, E.I.-C.; Chang, S.-T., Antifungal activities and chemical compositions of essential oils from leaves of four eucalypts, Taiwan J. For. Sci., 2006, 21, 1, 49-61. [all data]

Salido, Altarejos, et al., 2003
Salido, S.; Altarejos, J.; Nogueras, M.; Sánchez, A.; Luque, P., Chemical composition and seasonal variations of rosemary oil from Southern Spain, J. Essent. Oil Res., 2003, 15, 1, 10-14, https://doi.org/10.1080/10412905.2003.9712248 . [all data]

Shao, Marriott, et al., 2003
Shao, Y.; Marriott, P.; Shellie, R.; Hügel, H., Solid-phase micro-extraction-comprehensive two-dimensional gas chromatography of ginger (Zingiber officinale) volatiles, Flavour Fragr. J., 2003, 18, 1, 5-12, https://doi.org/10.1002/ffj.1133 . [all data]

Bertoli, Lepnardi, et al., 2011
Bertoli, A.; Lepnardi, M.; Krzyzanowska, J.; Oleszek, W.; Pistelli, L., Mentha longifolia in vitro cultures as safe source of flavouring ingradients, Acta Biochem. Polonica, 2011, 58, 4, 581-587. [all data]

Adams, Beauchamp, et al., 2007
Adams, R.P.; Beauchamp, P.S.; Dev, V.; Dutz, S.M., New Natural Products Isolated from One-Seeded Juniperus of the Southwestern United States: Isolation and Occurence of 2-Ethenyl-3-methyl Phanol and Its Derivatives, J. Essent. Oil Res., 2007, 19, 2, 146-152, https://doi.org/10.1080/10412905.2007.9699247 . [all data]

Farsam, Amanlou, et al., 2003
Farsam, H.; Amanlou, M.; Amin, G.; Nezamivand-Chegini, G.; Salehi-Surmaghi, M.-H.; Shafiee, A., Anatomical and phytochemical study of Lilium Ledebourii (Baker) Boiss., a rare endemic species in Iran, DARU, 2003, 11, 4, 164-170. [all data]

Vinogradov, 2004
Vinogradov, B.A., Production, composition, properties and application of essential oils, 2004, retrieved from http://viness.narod.ru. [all data]

Betts, 2000
Betts, T.J., Solid phase microextraction of volatile constituents from individual fresh Eucalyptis leaves of three species, Planta Medica, 2000, 66, 2, 193-195, https://doi.org/10.1055/s-0029-1243133 . [all data]

Zenkevich, 1997
Zenkevich, I.G., Analytical Parameters of Components of Essential Oils for their Chromatographic and Chromato-Spectral Identificaiton. Oxsigenated derivatives of Mono- and Sesquiterpene Hydrocarbons, Rastit, Resursy (Rus.), 1997, 33, 1, 16-28. [all data]

Bignell, Dunlop, et al., 1997
Bignell, C.M.; Dunlop, P.J.; Brophy, J.J., Volatile leaf oils of some Queensland and Norther Australian species of the genus Eucalyptus (Series II) Part II. Subgenera (a) Blakella, (b) Corymbia, (c) Unnamed, (d) Idiogenes, (e) Monocalyptus and (f) Symphyomyrtus, Flavour Fragr. J., 1997, 12, 4, 277-284, https://doi.org/10.1002/(SICI)1099-1026(199707)12:4<277::AID-FFJ642>3.0.CO;2-B . [all data]


Notes

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