2-Furanmethanol, 5-ethenyltetrahydro-α,α,5-trimethyl-, cis-


Van Den Dool and Kratz RI, polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxZB-WaxBP-20DB-WaxLM-120
Column length (m) 30.30.50.30.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (μm) 0.50.250.250.250.5
Tstart (C) 40.40.60.50.50.
Tend (C) 240.250.220.220.240.
Heat rate (K/min) 7.5.2.4.3.
Initial hold (min)  2. 4. 
Final hold (min) 5.5.20.20.30.
I 1451.1431.1439.1427.1487.
ReferenceMahattanatawee K., Perez-Cacho P.R., et al., 2007Wu, Zorn, et al., 2007Bousmaha, Boti, et al., 2006Osorio, Alarcon, et al., 2006Pinto, Guedes, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Supelcowax-10DB-WaxOV-351DB-WaxSupelcowax-10
Column length (m) 30.30.50.30.30.
Carrier gas HeHeHeHeliumHe
Substrate      
Column diameter (mm) 0.20.250.320.320.2
Phase thickness (μm) 0.20.250.20.500.2
Tstart (C) 70.40.60.40.70.
Tend (C) 220.240.220.240.220.
Heat rate (K/min) 3.6.5.7.3.
Initial hold (min)  10.   
Final hold (min) 15.25. 5.15.
I 1442.1451.1420.1480.1439.
ReferenceSalgueiro L.R., Pinto E., et al., 2006Varming, Andersen, et al., 2006Bonvehí, 2005Bell, 2004Cavaleiro, Salgueiro, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-WaxDB-Wax EtrBP-20DB-WaxDB-Wax
Column length (m) 30.30.50.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.220.250.32
Phase thickness (μm) 0.150.250.250.250.5
Tstart (C) 35.40.60.40.40.
Tend (C) 220.245.220.240.245.
Heat rate (K/min) 1.83.2.6.3.
Initial hold (min) 10.3. 10.3.
Final hold (min) 10.20.20.25.20.
I 1463.1457.1443.1425.1465.
ReferenceLedauphin, Saint-Clair, et al., 2004Ménager, Jost, et al., 2004Tam, Thuam, et al., 2004Varming, Andersen, et al., 2004Aubert, Ambid, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MInnowaxDB-WaxAT-WaxBP-20
Column length (m) 25.15.60.60.50.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.22
Phase thickness (μm) 0.30.250.250.250.25
Tstart (C) 50.35.70.65.60.
Tend (C) 200.225.230.250.220.
Heat rate (K/min) 3.4.2.2.2.
Initial hold (min) 1.5.2.10. 
Final hold (min) 20.20.20.60.20.
I 1395.1445.1453.1454.1436.
ReferenceBicchi, Rubiolo, et al., 2003Chisholm, Jell, et al., 2003Choi, 2003Pino, Almora, et al., 2003Lota, de Rocca Serra, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-WaxSupelcowax-10AT-WaxDB-WaxAT-Wax
Column length (m) 30.30.60.30.60.
Carrier gas HeHeHeH2He
Substrate      
Column diameter (mm) 0.250.250.320.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 45.50.65.35.65.
Tend (C) 250.230.250.220.250.
Heat rate (K/min) 3.3.2.4.2.
Initial hold (min) 6. 10.0.510.
Final hold (min) 10.30.60. 60.
I 1423.1474.1449.1471.81424.
ReferenceMondello, Zappia, et al., 2002Moreira, Trugo, et al., 2002Pino, Marbot, et al., 2002Pet'ka, Mocák, et al., 2001Pino and Marbot, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase AT-WaxDB-WaxDB-WaxDB-WaxDB-Wax
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.320.320.320.320.32
Phase thickness (μm) 0.250.50.50.50.5
Tstart (C) 65.60.60.60.60.
Tend (C) 250.245.245.245.245.
Heat rate (K/min) 2.3.3.3.3.
Initial hold (min) 10.3.3.3.3.
Final hold (min) 60.20.20.20.20.
I 1449.1465.1468.1472.1471.
ReferencePino, Marbot, et al., 2001Wirth, Guo, et al., 2001Wirth, Guo, et al., 2001Bureau, Baumes, et al., 2000Bureau, Razungles, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Wax 52CBDB-WaxDB-WaxDB-WaxCarbowax 20M
Column length (m) 25.60.25.60.60.
Carrier gas  N2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (μm) 0.150.250.250.250.425
Tstart (C) 40.70.50.50.45.
Tend (C) 220.230.240.230.300.
Heat rate (K/min) 3.2.4.3.3.
Initial hold (min) 5.2.3. 3.
Final hold (min)  20.  20.
I 1415.1454.1429.1477.1430.
ReferenceChagonda, Makanda, et al., 2000Choi and Sawamura, 2000Möllenbeck, König, et al., 1997Shimoda, Wu, et al., 1996Mondello, Dugo, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Carbowax 20MDB-WaxDB-WaxHP-20MHP-FFAP
Column length (m) 50.60.60.50.50.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (μm) 0.20.250.25  
Tstart (C) 30.50.50.60.60.
Tend (C) 170.230.230.190.210.
Heat rate (K/min) 4.2.2.3.3.
Initial hold (min) 2.    
Final hold (min) 20.    
I 1425.1458.1458.1420.1471.
ReferencePíry, Príbela, et al., 1995Shimoda, Shigematsu, et al., 1995Shimoda, Shigematsu, et al., 1995, 2Chung, Eiserich, et al., 1993Chung, Eiserich, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxDB-WaxCarbowax 20MCarbowax 20M
Column length (m) 30.30.30.25.25.
Carrier gas HeHeHe  
Substrate      
Column diameter (mm) 0.250.250.250.310.31
Phase thickness (μm)  0.250.25  
Tstart (C) 40.50.50.50.50.
Tend (C) 200.220.240.200.200.
Heat rate (K/min) 2.4.4.2.2.
Initial hold (min) 10.3.3.  
Final hold (min)  20.   
I 1438.1431.1431.1423.1430.
ReferenceUmano, Hagi, et al., 1992Humpf and Schreier, 1991Krammer, Winterhalter, et al., 1991Suárez and Duque, 1991Suárez and Duque, 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxDB-WaxCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 30.30.30.60.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.32
Phase thickness (μm) 0.250.250.25  
Tstart (C) 50.50.40.50.50.
Tend (C) 250.250.240.225.200.
Heat rate (K/min) 4.4.4.1.52.
Initial hold (min) 3.3.3. 5.
Final hold (min)    80.40.
I 1431.1432.1421.1435.1428.
ReferenceFröhlich, Duque, et al., 1989Fröhlich, Duque, et al., 1989Schwab, Mahr, et al., 1989Chen and Ho, 1988Chen, Kuo, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Suárez and Duque, 1991
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Fröhlich, Duque, et al., 1989
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Schwab, Mahr, et al., 1989
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Chen and Ho, 1988
Chen, C.-C.; Ho, C.-T., Gas chromatographic analysis of volatile components of ginger oil (Zingiber officinale Roscoe) extracted with liquid carbon dioxide, J. Agric. Food Chem., 1988, 36, 2, 322-328, https://doi.org/10.1021/jf00080a020 . [all data]

Chen, Kuo, et al., 1986
Chen, C.-C.; Kuo, M.-C.; Liu, S.-E.; Wu, C.-M., Volatile components of salted and pickled prunes (Prunus mume Sieb. et Zucc.), J. Agric. Food Chem., 1986, 34, 1, 140-144, https://doi.org/10.1021/jf00067a038 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, polar column, temperature ramp, References