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2-Furanmethanol, 5-ethenyltetrahydro-«alpha»,«alpha»,5-trimethyl-, cis-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

Go To: Top, References, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil PONA GBDB-5HP-5SPB-1HP-5MS
Column length (m) 100.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 140.60.50.50.60.
Tend (C) 230.246.250.250.280.
Heat rate (K/min) 5.3.4.5.4.
Initial hold (min) 10. 4.3.5.
Final hold (min) 25. 10.15. 
I 1064.1077.1073.1089.1074.
ReferenceCunicao, Lopes, et al., 2007Hongratanaworakit and Buchbauer, 2007Quijano, Salamanca, et al., 2007Radulovic, Lazarevic, et al., 2007Radulovic, Lazarevic, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5MSDB-5CP Sil 5 CB
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.40.50.
Tend (C) 280.240.280.250.200.
Heat rate (K/min) 4.3.3.5.5.
Initial hold (min) 5.  2. 
Final hold (min)    5. 
I 1080.1074.1088.1068.1087.
ReferenceSaroglou, Arfan, et al., 2007Telascrea, de Araujo, et al., 2007Vagionas, Ngassapa, et al., 2007Wu, Zorn, et al., 2007Andrianoelisoa H.S., Menut C., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SPB-1DB-5BP-1DB-1
Column length (m) 30.30.30.50.30.
Carrier gas  HeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.50.60.50.
Tend (C) 220.250.250.220.220.
Heat rate (K/min) 3.5.5.2.4.
Initial hold (min)  3.3.  
Final hold (min)  15.15.20. 
I 1070.1089.1070.1056.1068.
ReferenceBastos, Ishimoto, et al., 2006Blagojevic, Radulovic, et al., 2006Blagojevic, Radulovic, et al., 2006Bousmaha, Boti, et al., 2006Kuiate, Bessière, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-1SPB-1HP-5MSDB-5
Column length (m) 25.25.30.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.20.20.20.250.25
Phase thickness (mum) 0.330.330.20.250.25
Tstart (C) 60.50.70.60.50.
Tend (C) 300.300.220.280.250.
Heat rate (K/min) 5.4.3.4.5.
Initial hold (min) 3.  5.2.
Final hold (min) 30. 15.  
I 1056.1087.1056.1071.1087.
ReferenceNath, Baruah, et al., 2006Osorio, Alarcon, et al., 2006Salgueiro L.R., Pinto E., et al., 2006Saroglou, Dorizas, et al., 2006Su, Ho, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1DB-5DB-1DB-1
Column length (m) 25.30.30.30.25.
Carrier gas H2N2H2  
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 80.50.35.50.60.
Tend (C) 270.200.270.250.180.
Heat rate (K/min) 10.5.5.2.3.
Initial hold (min)    8.10.
Final hold (min)   20. 10.
I 1072.1078.1074.1059.1075.
ReferenceZiegenbein, Hanssen, et al., 2006Agnaniet, Makani, et al., 2005Alves, Pinto, et al., 2005Dob, Dahmane, et al., 2005bin Jantan, Yalvema, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSSPB-1ZB-5SPB-1
Column length (m) 25.30.30.30.30.
Carrier gas N2HeHeHeliumHe
Substrate      
Column diameter (mm) 0.250.250.250.320.2
Phase thickness (mum) 0.250.250.250.500.2
Tstart (C) 75.60.70.40.70.
Tend (C) 210.250.220.265.220.
Heat rate (K/min) 3.4.3.7.3.
Initial hold (min) 10.2.   
Final hold (min) 1.20.15.5.15.
I 1085.1074.1056.1087.1055.
Referencebin Jantan, Yalvema, et al., 2005, 2Pino, Mesa, et al., 2005Antunes, Sevinate-Pinto, et al., 2004Bell, 2004Cavaleiro, Salgueiro, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1DB-5DB-5SPB-1RSL-200
Column length (m) 25.30.30.30.30.
Carrier gas HeN2N2HeH2
Substrate      
Column diameter (mm) 0.320.250.250.20.32
Phase thickness (mum) 0.170.250.250.20.25
Tstart (C) 50.60.60.70.40.
Tend (C) 200.240.240.220.280.
Heat rate (K/min) 3.3.3.3.6.
Initial hold (min)     5.
Final hold (min)    15.5.
I 1047.1076.1076.1055.1097.
ReferenceFernández-Ocaña, Gómez-Rodríguez, et al., 2004Flamini, Cioni, et al., 2004Flamini, Cioni, et al., 2004Moldão-Martins, Beirão-da-Costa, et al., 2004Ngassoum, Ousmaila, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5HP-5MSBP-1DB-5OV-1
Column length (m) 30.30.50.25.25.
Carrier gas HeHeHeN2H2
Substrate      
Column diameter (mm) 0.250.250.220.250.25
Phase thickness (mum) 0.250.250.250.250.3
Tstart (C) 60.50.60.75.50.
Tend (C) 250.250.220.210.200.
Heat rate (K/min) 4.3.2.3.3.
Initial hold (min) 2.  10.1.
Final hold (min) 20. 20.1.20.
I 1074.1073.1057.1075.1060.
ReferencePino, Marbot, et al., 2004Salido, Valenzuela, et al., 2004Tam, Thuam, et al., 2004bin Ahmad and bin Jantan, 2003Bicchi, Rubiolo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Ultra-2SPB-1DB-5DB-5DB-5
Column length (m) 25.30.30.30.30.
Carrier gas H2HeN2HeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.330.250.250.250.25
Tstart (C) 40.35.70.75.75.
Tend (C) 280.225.230.230.230.
Heat rate (K/min) 3.4.2.3.3.
Initial hold (min) 2.5.2.10.10.
Final hold (min) 10.20.20.20. 
I 1070.1069.1070.1075.1075.
ReferenceCeva-Antunes, Bizzo, et al., 2003Chisholm, Jell, et al., 2003Choi, 2003Jantan, Ling, et al., 2003bin Jantan, Yassin, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5MSHP-5CP Sil 5 CBSPB-5
Column length (m) 30.60.30.60.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.60.
Tend (C) 280.310.240.280.250.
Heat rate (K/min) 4.3.3.3.4.
Initial hold (min) 5.1. 10.2.
Final hold (min)  20. 60.20.
I 1074.1075.1076.1070.1074.
ReferenceKarioti, Skaltsa, et al., 2003Lalel, Singh, et al., 2003Macchioni, Cioni, et al., 2003Pino, Almora, et al., 2003Pino, Marbot, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5Mega 5MSHP-5DB-5BP-1
Column length (m) 30.30.30.30.50.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 240.240.220.260.220.
Heat rate (K/min) 3.3.5.4.2.
Initial hold (min)  2.10.  
Final hold (min)     20.
I 1070.1075.1075.1088.1058.
ReferenceShellie and Marriott, 2003Verzera, Trozzi, et al., 2003Flamini, Cioni, et al., 2002Javidnia, Miri, et al., 2002Lota, de Rocca Serra, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5CP Sil 5 CBCP Sil 5 CBHP-5RTX-5
Column length (m) 30.30.50.30.30.
Carrier gas HeH2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.40.250.25
Tstart (C) 45.60.60.60.45.
Tend (C) 300.280.280.280.250.
Heat rate (K/min) 3.2.3.3.3.
Initial hold (min) 6.10.10. 6.
Final hold (min) 10.40.60.  
I 1072.1068.1068.1047.1074.
ReferenceMondello, Zappia, et al., 2002Pino, Marbot, et al., 2002Pino, Marbot, et al., 2002, 2Pitarokili, Couladis, et al., 2002Shellie, Mondello, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5SPB-1HP-5HP-5MSSE-30
Column length (m) 30.15.30.30.25.
Carrier gas He HeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.20
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 45.35.60.60.60.
Tend (C) 250.225.380.280.180.
Heat rate (K/min) 3.6.3.3.3.
Initial hold (min) 6.3. 5.10.
Final hold (min)  10.  1.
I 1079.1058.1066.1074.1075.
ReferenceShellie, Mondello, et al., 2002Chisholm, Wilson, et al., 2001Couladis, Tsortanidou, et al., 2001Giamakis, Kretsi, et al., 2001bin Jantan, Basni, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1CP Sil 5 CBCP Sil 5 CBHP-5MS
Column length (m) 50.50.50.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.320.320.25
Phase thickness (mum) 0.250.250.40.40.25
Tstart (C) 60.60.60.60.50.
Tend (C) 220.220.280.280.250.
Heat rate (K/min) 2.2.3.3.3.
Initial hold (min)   10.10. 
Final hold (min)   60.60. 
I 1058.1058.1068.1068.1073.
ReferenceLota, Serra, et al., 2001Lota, Serra, et al., 2001Pino and Marbot, 2001Pino, Marbot, et al., 2001Salido, Altarejos, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-1HP-5CP Sil 8 CBCP Sil 8 CB
Column length (m) 30.30.30.25.25.
Carrier gas HeH2He  
Substrate      
Column diameter (mm) 0.200.320.250.20.2
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.70.40.40.
Tend (C) 180.245.230.200.200.
Heat rate (K/min) 4.3.2.2.2.
Initial hold (min) 8.3. 8.8.
Final hold (min) 2.20.   
I 1074.1068.1073.1057.1056.
ReferenceAlonzo, Bosco, et al., 2000Brat, Brillouet, et al., 2000Song, Sawamura, et al., 2000Yassaa, Meklati, et al., 2000Yassaa, Meklati, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1BP-1DB-5Methyl SiliconeHP-101
Column length (m) 60.50.30.25.50.
Carrier gas N2HeH2HeN2
Substrate      
Column diameter (mm) 0.320.220.250.20.25
Phase thickness (mum) 0.250.25 0.3 
Tstart (C) 40.60.60.40.70.
Tend (C) 200.220.220.200.200.
Heat rate (K/min) 4.2.2.2.3.
Initial hold (min)   3.  
Final hold (min) 20.20.   
I 1069.1062.1068.1067.1071.
ReferenceChen, Huang, et al., 1998Tam, An, et al., 1998Sakho, Chassagne, et al., 1997Píry, Príbela, et al., 1995Chung, Eiserich, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillary
Active phase OV-101OV-101
Column length (m) 50.50.
Carrier gas N2N2
Substrate   
Column diameter (mm) 0.250.25
Phase thickness (mum)   
Tstart (C) 80.80.
Tend (C) 200.200.
Heat rate (K/min) 2.2.
Initial hold (min)   
Final hold (min)   
I 1063.1068.
ReferenceYang, Sugisawa, et al., 1992Yang, Sugisawa, et al., 1992
Comment MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Cunicao, Lopes, et al., 2007
Cunicao, M.M.; Lopes, A.R.; Côcco, L.C.; Yamamoto, C.I.; Plocharski, R.C.B.; Miguel, M.D.; Junior, A.G.; Auer, C.G.; Miguel, O.G., Phytochemical and antibacterial evaluation of essential oils from Ottonia Martiana Miq. (Piperaceae), J. Braz. Chem. Soc., 2007, 18, 1, 184-188, https://doi.org/10.1590/S0103-50532007000100021 . [all data]

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Hongratanaworakit, T.; Buchbauer, G., Chemical composition and stimulating effect of Citrus hystrix oil on humans, Flavour Fragr. J., 2007, 22, 5, 443-449, https://doi.org/10.1002/ffj.1820 . [all data]

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Quijano, C.E.; Salamanca, G.; Pino, J.A., Aroma volatile constituents of Colombian varieties of mango (Mangifera indica L.), Flavour Fragr. J., 2007, 22, 5, 401-406, https://doi.org/10.1002/ffj.1812 . [all data]

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Radulovic, N.; Lazarevic, J.; Ristic, N.; Palic, R., Chemotaxonomic significance of the volatiles in the genus Stachys (Lamiaceae): Essential oil composition of four Balkan Stachys species, Biochem. Syst. Ecol., 2007, 35, 4, 196-208, https://doi.org/10.1016/j.bse.2006.10.010 . [all data]

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Saroglou, V.; Arfan, M.; Shabir, A.; Hadjipavlou-Litina, D.; Skaltsa, H., Composition and antioxidant activity of the essential oil of Teucrium royleanum Wall. ex Benth growing in Pakistan, Flavour Fragr. J., 2007, 22, 2, 154-157, https://doi.org/10.1002/ffj.1774 . [all data]

Telascrea, de Araujo, et al., 2007
Telascrea, M.; de Araujo, C.C.; Marques, M.O.M.; Facanali, R.; de Moraes, P.L.R.; Cavalheiro, A.J., Essential oil from leaves of Cryptocarya mandioccana Meisner (Lauraceae): Composition and intraspecific chemical variability, Biochem. Syst. Ecol., 2007, 35, 4, 222-232, https://doi.org/10.1016/j.bse.2006.09.015 . [all data]

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Vagionas, K.; Ngassapa, O.; Runyoro, D.; Graikou, K.; Gortzi, O.; Chinou, I., Chemical analysis of edible aromatic plants growing in Tanzania, Food Chem., 2007, 105, 4, 1711-1717, https://doi.org/10.1016/j.foodchem.2007.05.029 . [all data]

Wu, Zorn, et al., 2007
Wu, S.; Zorn, H.; Krings, U.; Berger, R.G., Volatiles from submerged and surface-cultured beefsteak fungus, Fistulina hepatica, Flavour Fragr. J., 2007, 22, 1, 53-60, https://doi.org/10.1002/ffj.1758 . [all data]

Andrianoelisoa H.S., Menut C., et al., 2006
Andrianoelisoa H.S.; Menut C.; de Chatelperron P.C.; Saracco J.; Ramanoelina P.; Danthu P., Intraspecific chemical variability and highlighting of chemotypes of leaf essential oils from Ravensara aromatica Sonnerat a tree endemic to Madagascar, Flavour Fragr. J., 2006, 21, 5, 833-838, https://doi.org/10.1002/ffj.1735 . [all data]

Bastos, Ishimoto, et al., 2006
Bastos, D.H.M.; Ishimoto, E.; Marques, M.O.M.; Ferri, A.F.; Torres, E.A.F.S., Essential oil and antioxidant activity of green mate and mate tea (Ilex paraguariensis) infusions, J. Food Comp. Anal., 2006, 19, 6-7, 538-543, https://doi.org/10.1016/j.jfca.2005.03.002 . [all data]

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Kuiate, Bessière, et al., 2006
Kuiate, J.R.; Bessière, J.M.; Vilarem, G.; Amvam Zollo, P.H., Chemical composition and antidermatophytic properties of the essential oils from leaves, flowers and fruits of Cupressus lusitanica Mill. from Cameroon, Flavour Fragr. J., 2006, 21, 4, 693-697, https://doi.org/10.1002/ffj.1686 . [all data]

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Bell, W.A.-M., Examination of Aroma Volatiles Formed from Thermal Processing of Florida Reconstituted Grapefruit Juice. A Thesis presented to the graduate school of the university of Florida in partial fulfillment of the requirements for the degree of master of science, 2004. [all data]

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Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References