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2-Furanmethanol, 5-ethenyltetrahydro-«alpha»,«alpha»,5-trimethyl-, cis-


Kovats' RI, polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxHP-WaxInnowaxSupelcowax-10Carbowax 20M
Column length (m) 30.50.30.30.25.
Carrier gas H2HeHeHeN2
Substrate      
Column diameter (mm) 0.250.20.250.320.5
Phase thickness (mum) 0.250.40.250.25 
Tstart (C) 40.60.50.75.60.
Tend (C) 260.230.250.230.200.
Heat rate (K/min) 4.4.0.53.5.
Initial hold (min) 2. 5.  
Final hold (min) 15.30.10.  
I 1425.1461.1428.1435.1425.
ReferenceAvato, Raffo, et al., 2004Gauvin, Lecomte, et al., 2004Viña and Murillo, 2003Tzakou and Couladis, 2001Mallavarapu, Rao, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-WaxSupelcowax-10DB-WaxDB-WaxCarbowax 20M
Column length (m) 60.60.60.60.50.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.22
Phase thickness (mum)   0.250.25 
Tstart (C) 40.35.40.40.80.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 2.3.3.3.2.
Initial hold (min) 2.5.5.5. 
Final hold (min)  20.   
I 1443.1453.1478.1480.1433.
ReferenceUmano, Hagi, et al., 1994Wong and Tie, 1993Tatsuka, Suekane, et al., 1990Tatsuka, Suekane, et al., 1990Nishimura, Yamaguchi, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-20Carbowax 20MCarbowax 20MCarbowax 20MCarbowax 20M
Column length (m) 25.70.70.50.50.
Carrier gas H2N2N2N2N2
Substrate      
Column diameter (mm) 0.200.280.280.280.28
Phase thickness (mum)      
Tstart (C) 65.80.80.80.80.
Tend (C) 180.200.200.200.200.
Heat rate (K/min) 12.2.2.2.2.
Initial hold (min) 3.    
Final hold (min)      
I 1423.1410.1414.1409.1410.
ReferenceMacLeod and Pieris, 1983Yamaguchi and Shibamoto, 1981Yamaguchi and Shibamoto, 1981Yamaguchi and Shibamoto, 1979Yamaguchi and Shibamoto, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase Carbowax 20M
Column length (m) 50.
Carrier gas He
Substrate  
Column diameter (mm) 0.28
Phase thickness (mum)  
Tstart (C) 70.
Tend (C) 190.
Heat rate (K/min) 2.
Initial hold (min)  
Final hold (min)  
I 1461.
ReferenceTressl, Friese, et al., 1978
Comment MSDC-RI

References

Go To: Top, Kovats' RI, polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Avato, Raffo, et al., 2004
Avato, P.; Raffo, F.; Aldouri, N.A.; Vartanian, S.T., Essential oils of varthemia iphionoides from Jordan, Flavour Fragr. J., 2004, 19, 6, 559-561, https://doi.org/10.1002/ffj.1351 . [all data]

Gauvin, Lecomte, et al., 2004
Gauvin, A.; Lecomte, H.; Smadja, J., Comparative investigations of the essential oils of two scented geranium (Pelargonium spp.) cultivars grown on Reunion Island, Flavour Fragr. J., 2004, 19, 5, 455-460, https://doi.org/10.1002/ffj.1354 . [all data]

Viña and Murillo, 2003
Viña, A.; Murillo, E., Essential oil composition from twelve varieties of basil (Ocimum spp) grown in Columbia, J. Braz. Chem. Soc., 2003, 14, 5, 744-749, https://doi.org/10.1590/S0103-50532003000500008 . [all data]

Tzakou and Couladis, 2001
Tzakou, O.; Couladis, M., The essential oil of Micromeria graeca (L.) Bentham et Reichenb. growing in Greece, Flavour Fragr. J., 2001, 16, 2, 107-109, https://doi.org/10.1002/ffj.955 . [all data]

Mallavarapu, Rao, et al., 1998
Mallavarapu, G.R.; Rao, B.R.R.; Kaul, P.N.; Ramesh, S.; Bhattacharya, A.K., Volatile constituents of the essential oils of the seeds and the herb of palmarosa (Cymbopogon martinii (Roxb.) Wats. var. motia Burk.), Flavour Fragr. J., 1998, 13, 3, 167-169, https://doi.org/10.1002/(SICI)1099-1026(199805/06)13:3<167::AID-FFJ719>3.0.CO;2-B . [all data]

Umano, Hagi, et al., 1994
Umano, K.; Hagi, Y.; Tamura, T.; Shoji, A.; Shibamoto, T., Identification of volatile compounds isolated from round kumquat (Fortunella japonica Swingle), J. Agric. Food Chem., 1994, 42, 9, 1888-1890, https://doi.org/10.1021/jf00045a011 . [all data]

Wong and Tie, 1993
Wong, K.C.; Tie, D.Y., The Essential Oil of the Leaves of Murraya koenigii Spreng., J. Essent. Oil Res., 1993, 5, 4, 371-374, https://doi.org/10.1080/10412905.1993.9698245 . [all data]

Tatsuka, Suekane, et al., 1990
Tatsuka, K.; Suekane, S.; Sakai, Y.; Sumitani, H., Volatile constituents of kiwi fruit flowers: simultaneous distillation and extraction versus headspace sampling, J. Agric. Food Chem., 1990, 38, 12, 2176-2180, https://doi.org/10.1021/jf00102a015 . [all data]

Nishimura, Yamaguchi, et al., 1989
Nishimura, O.; Yamaguchi, K.; Mihara, S.; Shibamoto, T., Volatile Constituents of Guava Fruits (Psidium guajava L.) and Canned Puree, J. Agric. Food Chem., 1989, 37, 1, 139-142, https://doi.org/10.1021/jf00085a033 . [all data]

MacLeod and Pieris, 1983
MacLeod, A.J.; Pieris, N.M., Volatile components of papaya (Carica papaya L.) with particular reference to glucosinolate products, J. Agric. Food Chem., 1983, 31, 5, 1005-1008, https://doi.org/10.1021/jf00119a021 . [all data]

Yamaguchi and Shibamoto, 1981
Yamaguchi, K.; Shibamoto, T., Volatile constituents of green tea, Gyokuro (Camellia sinensis L. var Yabukita), J. Agric. Food Chem., 1981, 29, 2, 366-370, https://doi.org/10.1021/jf00104a035 . [all data]

Yamaguchi and Shibamoto, 1979
Yamaguchi, K.; Shibamoto, T., Volatile constituents of Castanopsis flower, J. Agric. Food Chem., 1979, 27, 4, 847-850, https://doi.org/10.1021/jf60224a025 . [all data]

Tressl, Friese, et al., 1978
Tressl, R.; Friese, L.; Fendesack, F.; Köppler, H., Studies of the volatile composition of hops during storage, J. Agric. Food Chem., 1978, 26, 6, 1426-1430, https://doi.org/10.1021/jf60220a036 . [all data]


Notes

Go To: Top, Kovats' RI, polar column, temperature ramp, References