2-Furanmethanol, 5-ethenyltetrahydro-α,α,5-trimethyl-, cis-


Kovats' RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-1BP-1CP Sil 8 CB
Column length (m) 60.25.25.30.30.
Carrier gas HeHeHeN2H2
Substrate      
Column diameter (mm) 0.250.20.20.320.25
Phase thickness (μm) 0.250.15 0.250.25
Tstart (C) 40.60.60.60.50.
Tend (C) 250.220.220.220.220.
Heat rate (K/min) 3.3.3.5.3.
Initial hold (min) 1.3.3. 2.
Final hold (min) 20.  3. 
I 1078.1081.1080.1059.1076.
ReferenceJalali-Heravi, Zekavat, et al., 2006Mevy, Bessiere, et al., 2006Mevy, Bessiere, et al., 2006, 2Srivastava, Srivastava, et al., 2006Tayoub, Schwob, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-5SPB-5CP Sil 8 CBDB-5
Column length (m) 30.30.60.30.25.
Carrier gas HeH2HeH2He
Substrate      
Column diameter (mm) 0.320.250.320.250.25
Phase thickness (μm) 0.250.251.0.25 
Tstart (C) 60.40.60.50.40.
Tend (C) 240.280.200.220.280.
Heat rate (K/min) 4.4.4.3.3.
Initial hold (min) 4.  2.5.
Final hold (min) 2.30.30. 5.
I 1061.1080.1076.1068.1087.
ReferenceWalde, Jyothirmayi, et al., 2006Avato, Raffo, et al., 2004Gauvin, Lecomte, et al., 2004Schwob, Bessiere, et al., 2004Amparo Blázquez, Pérez, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5HP-5SE-30BP-1
Column length (m) 30.30.30.25.25.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.220.55
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.50.60.70.60.
Tend (C) 280.250.275.220.220.
Heat rate (K/min) 3.0.54.4.5.
Initial hold (min)  5.   
Final hold (min)  10.  15.
I 1065.1074.1075.1062.1062.
ReferenceGkinis, Tzakou, et al., 2003Viña and Murillo, 2003Nickavar, Salehi-Sormagi, et al., 2002Palá-Paúl, Velasco-Negueruela, et al., 2002Raina, Srivastava, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Cross-Linked MethylsiliconeBP-1BP-1BP-1BP-1
Column length (m) 50.25.25.30.25.
Carrier gas HeN2 N2N2
Substrate      
Column diameter (mm) 0.20.50.50.320.55
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 100.60.60.60.60.
Tend (C) 280.220.220.220.220.
Heat rate (K/min) 4.5.5.5.5.
Initial hold (min)      
Final hold (min)  10.10.13.15.
I 1064.1063.1063.1057.1063.
ReferenceRajeswara Rao, Kaul, et al., 2002Rajeswara Rao, 2002Rao B.R.R., 2002Shawl, Srivastava, et al., 2002Jain, Aggarwal, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1HP-5DB-1BP-1
Column length (m) 25.25.30.30.25.
Carrier gas N2N2He N2
Substrate      
Column diameter (mm) 0.550.550.250.250.5
Phase thickness (μm) 0.250.250.250.25 
Tstart (C) 60.60.60.80.60.
Tend (C) 220.220.280.225.220.
Heat rate (K/min) 5.5.3.4.5.
Initial hold (min)      
Final hold (min) 15.15.  10.
I 1056.1059.1072.1054.1063.
ReferenceJain, Srivastava, et al., 2001Raina, Srivastava, et al., 2001Tzakou and Couladis, 2001Abella, Cortella, et al., 2000Rao, Kaul, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1CP Sil 5 CBMethyl SiliconeDB-1SE-30
Column length (m) 25.25.25.25.25.
Carrier gas N2HeN2HeN2
Substrate      
Column diameter (mm) 0.500.250.50.230.2
Phase thickness (μm) 0.25  0.13 
Tstart (C) 60.60.60.60.60.
Tend (C) 220.280.220.200.180.
Heat rate (K/min) 5.5.5.4.3.
Initial hold (min)    2.10.
Final hold (min) 10.   1.
I 1063.1065.1063.1057.1066.
ReferenceRao, Sastry, et al., 2000Kaul, Gujral, et al., 1999Mallavarapu, Rao, et al., 1998Breheret, Talou, et al., 1997Jantan, Ahmad, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101OV-101OV-101
Column length (m) 25.25.70.70.70.
Carrier gas N2N2N2N2N2
Substrate      
Column diameter (mm) 0.250.250.280.280.28
Phase thickness (μm) 0.25    
Tstart (C) 50.50.80.80.80.
Tend (C) 200.200.200.200.200.
Heat rate (K/min) 5.5.2.2.2.
Initial hold (min)      
Final hold (min)      
I 1063.1063.1066.1066.1081.
Referencevon Poser, Menut, et al., 1996Menut, Molangui, et al., 1995Yamaguchi and Shibamoto, 1981Yamaguchi and Shibamoto, 1981Yamaguchi and Shibamoto, 1979
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase OV-101
Column length (m) 70.
Carrier gas N2
Substrate  
Column diameter (mm) 0.28
Phase thickness (μm)  
Tstart (C) 80.
Tend (C) 200.
Heat rate (K/min) 2.
Initial hold (min)  
Final hold (min)  
I 1082.
ReferenceYamaguchi and Shibamoto, 1979
Comment MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Jalali-Heravi, Zekavat, et al., 2006
Jalali-Heravi, M.; Zekavat, B.; Sereshti, H., Characterization of essential oil components of Iranian geranium oil using gas chromatography-mass spectrometry combined with chemometric resolution techniques, J. Chromatogr. A, 2006, 1114, 1, 154-163, https://doi.org/10.1016/j.chroma.2006.02.034 . [all data]

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Walde, S.G.; Jyothirmayi, T.; Prabhakara Rao, P.G.; Srinivas, P., Flavour volatiles of flowers and stalks of Murraya koenigii L., Flavour Fragr. J., 2006, 21, 4, 581-584, https://doi.org/10.1002/ffj.1737 . [all data]

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Gauvin, Lecomte, et al., 2004
Gauvin, A.; Lecomte, H.; Smadja, J., Comparative investigations of the essential oils of two scented geranium (Pelargonium spp.) cultivars grown on Reunion Island, Flavour Fragr. J., 2004, 19, 5, 455-460, https://doi.org/10.1002/ffj.1354 . [all data]

Schwob, Bessiere, et al., 2004
Schwob, I.; Bessiere, J.-M.; Masotti, V.; Viano, J., Changes in essential oil composition in Saint John's wort (Hypericum perforatum L.) aerial parts during its phenological cycle, Biochem. Syst. Ecol., 2004, 32, 8, 735-745, https://doi.org/10.1016/j.bse.2003.12.005 . [all data]

Amparo Blázquez, Pérez, et al., 2003
Amparo Blázquez, M.; Pérez, I.; Boira, H., Essential oil analysis of Teucrium libanitis and T. turredanum by GC and GC-MS, Flavour Fragr. J., 2003, 18, 6, 497-501, https://doi.org/10.1002/ffj.1256 . [all data]

Gkinis, Tzakou, et al., 2003
Gkinis, G.; Tzakou, O.; Iliopoulou, D.; Roussis, V., Chemical Composition and Biological Activity of Nepeta parnassica Oils and Isolated Nepetalactones, Z. Naturforsch. C:, 2003, 58, 681-686. [all data]

Viña and Murillo, 2003
Viña, A.; Murillo, E., Essential oil composition from twelve varieties of basil (Ocimum spp) grown in Columbia, J. Braz. Chem. Soc., 2003, 14, 5, 744-749, https://doi.org/10.1590/S0103-50532003000500008 . [all data]

Nickavar, Salehi-Sormagi, et al., 2002
Nickavar, B.; Salehi-Sormagi, M.H.; Amin, Gh.; Daneshtalab, M., Steam volatiles of Vaccinium arctostaphylos, Pharm. Biol., 2002, 40, 6, 448-449, https://doi.org/10.1076/phbi.40.6.448.8449 . [all data]

Palá-Paúl, Velasco-Negueruela, et al., 2002
Palá-Paúl, J.; Velasco-Negueruela, A.; Pérez-Alonso, M.J.; Sanz, J., Essential oil composition of the aerial parts of Cachrys sicula L., Flavour Fragr. J., 2002, 17, 1, 64-68, https://doi.org/10.1002/ffj.1042 . [all data]

Raina, Srivastava, et al., 2002
Raina, V.K.; Srivastava, S.K.; Jain, N.; Ahmad, A.; Syamasundar, K.V.; Aggarwal, K.K., Essential oil composition of Curcuma longa L. cv. Roma from the plains of northern India, Flavour Fragr. J., 2002, 17, 2, 99-102, https://doi.org/10.1002/ffj.1053 . [all data]

Rajeswara Rao, Kaul, et al., 2002
Rajeswara Rao, B.R.; Kaul, P.N.; Syamasundar, K.V.; Ramesh, S., Water soluble fractions of rose scented geranium (Pelargonium species) essential oil, Bioresour. Technol., 2002, 84, 3, 243-246, https://doi.org/10.1016/S0960-8524(02)00057-3 . [all data]

Rajeswara Rao, 2002
Rajeswara Rao, B.R., Biomass yield, essential oil yield and essential oil composition of rose-scented geranium (Pelargonium species) as influenced by row spacings and intercropping with cornmint (Mentha arvensis L.f. piperascens Malinv. ex Holmes), Ind. Crops Prod., 2002, 16, 2, 133-144, https://doi.org/10.1016/S0926-6690(02)00038-9 . [all data]

Rao B.R.R., 2002
Rao B.R.R., Biomass yield, essential oil yield and essential oil composition of rose-scented geranium (Pelargonium species) as influenced by row spacings and intercropping with cornmint (Mentha arvensis L.f. piperascens Malinv. ex Holmes), Industrial Crops and Products, 2002, 16, 2, 133-144, https://doi.org/10.1016/S0926-6690(02)00038-9 . [all data]

Shawl, Srivastava, et al., 2002
Shawl, A.S.; Srivastava, S.K.; Syamasundar, K.V.; Tripathi, S.; Raina, V.K., Essential oil composition of Achillea millefolium L. growing wild in Kashmir, India, Flavour Fragr. J., 2002, 17, 3, 165-168, https://doi.org/10.1002/ffj.1074 . [all data]

Jain, Aggarwal, et al., 2001
Jain, N.; Aggarwal, K.K.; Syamasundar, K.V.; Srivastava, S.K.; Kumar, S., Essential oil composition of geranium (Pelargonium sp.) from the plains of Northern India, Flavour Fragr. J., 2001, 16, 1, 44-46, https://doi.org/10.1002/1099-1026(200101/02)16:1<44::AID-FFJ943>3.0.CO;2-X . [all data]

Jain, Srivastava, et al., 2001
Jain, N.; Srivastava, S.K.; Aggarwal, K.K.; Ramesh, S.; Kumar, S., Essential oil composition of Zanthoxylum alatum seeds from northern India, Flavour Fragr. J., 2001, 16, 6, 408-410, https://doi.org/10.1002/ffj.1024 . [all data]

Raina, Srivastava, et al., 2001
Raina, V.K.; Srivastava, S.K.; Aggarwal, K.K.; Ramesh, S.; Kumar, S., Essential oil composition of Cinnamomum zeylanicum Blume leaves from Little Andaman, India, Flavour Fragr. J., 2001, 16, 5, 374-376, https://doi.org/10.1002/ffj.1016 . [all data]

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von Poser, Menut, et al., 1996
von Poser, G.L.; Menut, C.; Toffoli, M.E.; Vérin, P.; Sobral, M.; Bessière, J.-M.; Lamaty, G.; Henriques, A.T., Essential oil composition and allelopathic effect of the Brazilian Lamiaceae Hesperozygis ringens (Benth.) Epling and Hesperozygis rhododon Epling, J. Agric. Food Chem., 1996, 44, 7, 1829-1832, https://doi.org/10.1021/jf950653c . [all data]

Menut, Molangui, et al., 1995
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Yamaguchi and Shibamoto, 1981
Yamaguchi, K.; Shibamoto, T., Volatile constituents of green tea, Gyokuro (Camellia sinensis L. var Yabukita), J. Agric. Food Chem., 1981, 29, 2, 366-370, https://doi.org/10.1021/jf00104a035 . [all data]

Yamaguchi and Shibamoto, 1979
Yamaguchi, K.; Shibamoto, T., Volatile constituents of Castanopsis flower, J. Agric. Food Chem., 1979, 27, 4, 847-850, https://doi.org/10.1021/jf60224a025 . [all data]


Notes

Go To: Top, Kovats' RI, non-polar column, temperature ramp, References