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1H-Naphtho[2,1-b]pyran, 3-ethenyldodecahydro-3,4a,7,7,10a-pentamethyl-, [3R-(3«alpha»,4a«beta»,6a«alpha»,10a«beta»,10b«alpha»)]-


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase TR-5 MSHP-5CP Sil 8 CBSLB-5 MSHP-5
Column length (m) 15.25.50.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (mum) 0.250.170.250.250.25
Program 35 0C (3 min) 2 0C/min -> 60 0C (3 min) 2 0C/min -> 80 0C (3 min) 4 0C/min -> 120 0C (3 min) 5 0C/min -> 150 0C (3 mion) 15 0C/min -> 240 0C (10 min)60 0C (5 min) 4 0C/min -> 220 0C 11 0C/min -> 280 0Cnot specifiednot specified130 0C 5 0C/min -> 240 0C 15 0C/min -> 320 0C (10 min)
I 2003.1997.1988.1998.1996.
ReferenceKurashov, Krylova, et al., 2013Maggi, Bilek, et al., 2009Kupcinskiene, Stikliene, et al., 2008Lo Presti, Sciarrone, et al., 2008Vichi, Aumatell, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 8 CBCP Sil 8 CBHP-5DB-1DB-5
Column length (m) 50.50.30.30.30.
Carrier gas HeHeHeH2 
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (mum) 0.250.250.250.25 
Program 50C(5min) => 2C/min => 90C => 15C/min => 240C(4min)60C(1min) => 5C/min => 160C => 10C/min => 250C(5min)50 0C 3 K/min -> 200 0C 8 K/min -> 280 0C40 0C 3 K/min -> 175 0C 15 K/min -> 240 0C (10 min)60 0C (2 min) 2 0C/min -> 140 0C 1 0C/min -> 190 0C 2 0C/min -> 210 0C (28 min)
I 1998.1989.1977.1977.1982.
ReferenceButkienë, Nivinskienë, et al., 2005Mockute, Nivinskiene, et al., 2003Usubillaga, Aparicio, et al., 2001da Silva, Pedro, et al., 2000Pichette, Garneau, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Capillary
Active phase CP Sil 5 CB
Column length (m) 25.
Carrier gas He
Substrate  
Column diameter (mm)  
Phase thickness (mum) 0.39
Program not specified
I 1983.
ReferenceWeyerstahl, Marschall, et al., 1998
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Kurashov, Krylova, et al., 2013
Kurashov, E.A.; Krylova, Yu.V.; Mitrukova, G.G., Variations in component composition of essential oil of Potamogeton pusillus (Potamogetonaceae) dirong vegetation, Plant Resources (Rastitel'nye Resursy), 2013, 000-000. [all data]

Maggi, Bilek, et al., 2009
Maggi, F.; Bilek, T.; Lucarini, D.; Papa, F.; Sagratini, G.; Vittori, S., Melittis melissophyllum L. subsp. melissophylum (Lamiaceae) from central Italy: A new source of a mushrrom-like flavour, Food Chem., 2009, 113, 1, 216-221, https://doi.org/10.1016/j.foodchem.2008.07.066 . [all data]

Kupcinskiene, Stikliene, et al., 2008
Kupcinskiene, E.; Stikliene, A.; Judzentiene, A., The essential oil guatitative composition in the needles of Pinus sylvestris L. growing along industrial transects, Environ. Pollution, 2008, 155, 3, 481-491, https://doi.org/10.1016/j.envpol.2008.02.001 . [all data]

Lo Presti, Sciarrone, et al., 2008
Lo Presti, M.; Sciarrone, D.; Crupi, M.C.; Costa, R.; Ragusa, S.; Dugo, G.; Mondello, L., Evaliation of the volatile and chiral composition in Pistacia lentiscus L. essential oil, Flavour Fragr. J., 2008, 23, 4, 249-257, https://doi.org/10.1002/ffj.1878 . [all data]

Vichi, Aumatell, et al., 2008
Vichi, S.; Aumatell, M.R.; Buxaderas, S.; Lopez-Tamames, E., Assessment of some diterpenoids in commercial distilled gin, Anal. Chim. Acta, 2008, 628, 2, 222-229, https://doi.org/10.1016/j.aca.2008.09.005 . [all data]

Butkienë, Nivinskienë, et al., 2005
Butkienë, R.; Nivinskienë, O.; Mockutë, D., «alpha»-Pinene chemotype of leaf (needle) essential oils of Juniperus communis L. growing wild in Vilnius district, Chemija, 2005, 16, 1, 53-60. [all data]

Mockute, Nivinskiene, et al., 2003
Mockute, D.; Nivinskiene, O.; Bernotiene, G.; Butkiene, R., The cis-thujone chemotype of Salvia officinalis L. essential oils, Chemija, 2003, 14, 4, 216-220. [all data]

Usubillaga, Aparicio, et al., 2001
Usubillaga, A.; Aparicio, R.; Romero, M.; Rojas, L.B.; Khouri, N., Volatile constituents from the leaves of four Libanothamus species from the Venezuelan Andes, Flavour Fragr. J., 2001, 16, 3, 209-211, https://doi.org/10.1002/ffj.981 . [all data]

da Silva, Pedro, et al., 2000
da Silva, J.A.; Pedro, L.G.; Santos, P.A.G.; Figueiredo, A.C.; Barroso, J.G.; Tenreiro, R.P.; Ribeiro, C.A.; Deans, S.G.; Looman, A.; Scheffer, J.J.C., Essential oils from seven populations of Juniperus brevifolia (Seub.) Antoine, an endemic species of the Azores, Flavour Fragr. J., 2000, 15, 1, 31-39, https://doi.org/10.1002/(SICI)1099-1026(200001/02)15:1<31::AID-FFJ862>3.0.CO;2-C . [all data]

Pichette, Garneau, et al., 1998
Pichette, A.; Garneau, F.-X.; Jean, F.-I.; Riedl, B.; Girarg, M., Chemical differences between the wood extracts pf Jack pine (pinus banksiana(. blacj spruce (Picea mariana) and balsam for (Abies balsamea) from eastern Canada, J. Wood Chem. Technol., 1998, 18, 4, 427-438, https://doi.org/10.1080/02773819809349590 . [all data]

Weyerstahl, Marschall, et al., 1998
Weyerstahl, P.; Marschall, H.; Weirauch, M.; Thefeld, K.; Surburg, H., Constituents of commercial Labdanum oil, Flavour Fragr. J., 1998, 13, 5, 295-318, https://doi.org/10.1002/(SICI)1099-1026(1998090)13:5<295::AID-FFJ751>3.0.CO;2-I . [all data]


Notes

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