Benadryl


Kovats' RI, non-polar column, isothermal

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryPackedPackedPacked
Active phase BP-1BP-1SE-30SE-30SE-30
Column length (m) 25.25.2.1.1.
Carrier gas N2N2N2N2N2
Substrate   1% se-30 on Anachrom ABS(80-100mesh)Inerton N AW (1), NaCl (2), and steel powder (3)Inerton N AW (1), NaCl (2), and steel powder (3)
Column diameter (mm) 0.220.53   
Phase thickness (μm) 0.251.   
Temperature (C) 200.200.200.210.210.
I 1865.1872.1868.1874.1890.
ReferenceJapp, Gill, et al., 1987Japp, Gill, et al., 1987Musumarra, Scarlata, et al., 1987Lenchik, Rudenko, et al., 1986Lenchik, Rudenko, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryPackedPackedPackedPacked
Active phase SPB-1OV-1OV-101OV-101OV-101
Column length (m) 25. 2.2.2.
Carrier gas He N2N2N2
Substrate   Chromosorb WChromosorb WChromosorb W
Column diameter (mm) 0.20    
Phase thickness (μm)      
Temperature (C) 250.200.150.190.230.
I 1888.1870.1850.1870.1885.
ReferenceLora-Tamayo, Rams, et al., 1986Berninger and Möller, 1977Möller, 1976Möller, 1976Möller, 1976
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Kovats' RI, non-polar column, isothermal, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Japp, Gill, et al., 1987
Japp, M.; Gill, R.; Osselton, M.D., Comparison of drug retention indices determined on packed, wide bore capillary and narrow bore capillary columns, J. Forensic Sci., 1987, 32, 6, 1574-1586. [all data]

Musumarra, Scarlata, et al., 1987
Musumarra, G.; Scarlata, G.; Romano, G.; Cappello, G.; Clementi, S.; Giulietti, G., Qualitative organic analysis. Part 2. Identification of drugs by principal components analysis of standardized TLC data in four eluent systems and of retention indices on SE 30, J. Anal. Toxicol., 1987, 11, 4, 154-163, https://doi.org/10.1093/jat/11.4.154 . [all data]

Lenchik, Rudenko, et al., 1986
Lenchik, N.V.; Rudenko, B.A.; Dzhabarov, D.N., Gas chromatographic analysis of nitrogen-containing pharmaceticals using a thermoaerosol detector and non-porous sorbents, Zh. Anal. Khim., 1986, 1438-1443. [all data]

Lora-Tamayo, Rams, et al., 1986
Lora-Tamayo, C.; Rams, M.A.; Chacon, J.M.R., Gas Chromatographic Data for 187 Nitrogen- or Phosphorus-Containing Drugs and Metabolites of Toxicological Interest Analysed on Methyl Silicone Capillary Columns, J. Chromatogr., 1986, 374, 73-85, https://doi.org/10.1016/S0378-4347(00)83254-5 . [all data]

Berninger and Möller, 1977
Berninger, H.; Möller, M.R., Retentionsindices zur gaschromatographischen Identifizierung von Arzneimitteln, Arch. Toxicol., 1977, 37, 4, 295-305, https://doi.org/10.1007/BF00330821 . [all data]

Möller, 1976
Möller, M.R., Comparability of retention indices of polar substances at elevated temperatures, Chromatographia, 1976, 9, 7, 311-314, https://doi.org/10.1007/BF02268832 . [all data]


Notes

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