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Cyclohexene, 1-methyl-4-(1-methylethylidene)-

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Normal alkane RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSRTX-1RTX-1Mega-5
Column length (m) 30.60.60.60.25.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.220.220.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.60.60.50.
Tend (C) 300.250.230.230.220.
Heat rate (K/min) 4.3.2.2.3.
Initial hold (min) 3.1.  1.
Final hold (min) 15.20.5.5.5.
I 1090.1089.1082.1082.1088.
ReferenceBertuzzi, Tirillini, et al., 2013Sardashti, Valizadeh, et al., 2013Bendiabdellah, El Amine Dib, et al., 2012Bendiabdellah, El Amine Dib, et al., 2012Dell'Agli, Sanna, et al., 2012
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Polydimethyl siloxane with 5 % PhHP-5HP-5HP-5 MSHP-1
Column length (m) 30.25.25.30.30.
Carrier gas HeliumHydrogenHydrogenHeliumHelium
Substrate      
Column diameter (mm)  0.320.320.250.25
Phase thickness (mum)  0.520.520.250.25
Tstart (C) 80.40.40.50.60.
Tend (C) 200.280.280.250.240.
Heat rate (K/min) 5.4.4.7.3.
Initial hold (min)    1. 
Final hold (min) 25.10.10.5. 
I 1080.1084.1084.1089.1087.
ReferencePriya, Prathapan, et al., 2012Velickovic, Ristic, et al., 2012Velickovic, Ristic, et al., 2012Zouari, Ayadi, et al., 2012Alizadeh, Khosh-Khui, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP-Sil 5 CBVF-5 MSVF-5 MSSE-30 MSCP-Sil 5 CB
Column length (m) 25.60.60.30.30.
Carrier gas HydrogenHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.320.320.250.25
Phase thickness (mum) 0.150.250.250.250.26
Tstart (C) 50.30.30.50.45.
Tend (C) 230.260.260.250.280.
Heat rate (K/min) 3.2.2.5.3.
Initial hold (min)    5. 
Final hold (min)  28.28.10.22.
I 1086.1086.1087.1089.1080.
ReferenceEsseien, Aboaba, et al., 2011Leffingwell and Alford, 2011Leffingwell and Alford, 2011Menichini, Tundis, et al., 2011Mothana, Hasson, et al., 2011
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-5 MSDB-5 MSDB-5 MSRTX-1DB-5
Column length (m) 30.25.25.60.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.300.300.220.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.50.60.60.
Tend (C) 290.240.240.230.280.
Heat rate (K/min) 5.3.3.2.3.
Initial hold (min)      
Final hold (min)    30. 
I 1087.1085.1085.1082.1084.
ReferenceBoix, Victorio, et al., 2010Chalchat, Figueredo, et al., 2010Chalchat, Figueredo, et al., 2010Dib, Djabou, et al., 2010Georgiou, Koutsaviti, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5HP-5 MSDB-5 MSDB-1
Column length (m) 30.30.30.60.25.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.70.40.60.
Tend (C) 250.240.290.250.250.
Heat rate (K/min) 2.3.5.5.4.
Initial hold (min)  2. 15.1.
Final hold (min)    15.10.
I 1089.1089.1093.1090.1083.
ReferenceHo, Wang, et al., 2010Kahriman, Tosun, et al., 2010Lazarevic, Radulovic, et al., 2010Mesa-Arango, Betancur-Galvis, et al., 2010Mirjalili, Salehi, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5 MSHP-5 MSHP-5 MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHydrogen
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.50.100.70.
Tend (C) 240.220.240.220.290.
Heat rate (K/min) 3.5.4.2.5.
Initial hold (min) 5.10.2.  
Final hold (min)   10.  
I 1086.1090.1088.1084.1094.
ReferenceMonsef-Esfahani, Miri, et al., 2010Ogunwande, Flamini, et al., 2010Pino, Marquez, et al., 2010Pripdeevech, Chumpolsri, et al., 2010Radulovic, Dordevic, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSSLB-5 MSDB-1-MSCP Sil 5 CBDB-5
Column length (m) 10.10.60.25.30.
Carrier gas HeliumHeliumHelium Helium
Substrate      
Column diameter (mm) 0.100.100.250.250.25
Phase thickness (mum) 0.100.100.250.150.25
Tstart (C) 50.50.30.50.80.
Tend (C) 250.250.200.230.240.
Heat rate (K/min) 10.10.2.3.3.
Initial hold (min)   4.  
Final hold (min)   35. 2.
I 1086.1086.1077.1087.1090.
ReferenceScandinaro, Tranchida, et al., 2010Scandinaro, Tranchida, et al., 2010Takeoka, Hobbs, et al., 2010Usman, Zubair, et al., 2010Vahirua-Lechat, Mitermite, et al., 2010
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5MSSE-54DB-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.50.60.35.60.
Tend (C) 250.250.260.220.250.
Heat rate (K/min) 10.7.2.3.2.
Initial hold (min) 1.1.5. 8.
Final hold (min) 3.5.999.40.15.
I 1089.1093.1086.1088.1091.
ReferenceYang, Zhang, et al., 2010Zouari, Zouari, et al., 2010Dayisoylu and Alma, 2009El-Massry, El-Ghorab, et al., 2009Farhat, Ginies, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase ZB-5SPB-5SPB-5DB-5DB-5
Column length (m) 30.60.30.30.30.
Carrier gas HeliumNitrogenNitrogenHeliumHelium
Substrate      
Column diameter (mm) 0.250.350.530.250.25
Phase thickness (mum) 0.250.250.500.250.25
Tstart (C) 50.60.50.50.50.
Tend (C) 240.230.210.250.250.
Heat rate (K/min) 3.4.3.5.5.
Initial hold (min)   5.2. 
Final hold (min) 1.40.45.  
I 1040.1094.1107.1089.1095.
ReferenceGardini, Beletti, et al., 2009Gauvin-Bialecki and Marodon, 2009Gilani, Shah, et al., 2009Ho, Wang, et al., 2009Koba, Catherine, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5HP-5RTX-1RTX-1
Column length (m) 30.30.25.60.60.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.320.250.200.220.22
Phase thickness (mum) 0.250.250.330.250.25
Tstart (C) 50.70.60.60.60.
Tend (C) 280.240.240.230.230.
Heat rate (K/min) 5.5.3.2.2.
Initial hold (min) 2.    
Final hold (min) 5. 7.30.30.
I 1088.1082.1083.1079.1082.
ReferenceLago, Favero, et al., 2009Lawal and Oyedelji, 2009Maridass, 2009Museli, Pau, et al., 2009Museli, Pau, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-55 % Phenyl methyl siloxaneDB-5DB-5
Column length (m) 30.30.60.30.30.
Carrier gas HeliumNitrogenHeliumNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 45.40.90.40.40.
Tend (C) 250.250.225.230.240.
Heat rate (K/min) 3.3.3.2.3.
Initial hold (min) 3.1.  1.
Final hold (min) 5.10.3.  
I 1088.1082.1087.1090.1063.
ReferencePorto, Decorti, et al., 2009Rahmi-Nasrabadi, Gholivand, et al., 2009Retta, Gattuso, et al., 2009Scrivanti, Anton, et al., 2009de Souza, Lopes, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5 MSHP-5MSHP-5 MSHP-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHeliumHeliumHeliumHelium
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.50.60.40.50.
Tend (C) 250.240.325.240.280.
Heat rate (K/min) 4.5.10.4.4.
Initial hold (min) 2. 6.4. 
Final hold (min) 2. 10.  
I 1088.1092.1081.1091.1088.
ReferenceSu, Wang, et al., 2009Wannes, Mhamdi, et al., 2009Zaibunnisa, Norashikin, et al., 2009Zhannan, Shiqiong, et al., 2009Zhao, Zeng, et al., 2009
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5HP-5 MSHP-5HP-5 MS
Column length (m) 30.30.30.30.30.
Carrier gas HeliumHelium N2Helium
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 50.70.60.60.50.
Tend (C) 280.220.280.220.230.
Heat rate (K/min) 9.3.3.5.4.
Initial hold (min) 3.1. 10.4.
Final hold (min) 3.   10.
I 1088.1082.1087.1089.1086.
ReferenceAicha, Ines, et al., 2008Ali, Wurster, et al., 2008Baziou, Couladis, et al., 2008Flamini, Tebano, et al., 2008Forero, Quijano, et al., 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SLB-5 MSZB-1DB-5BPX-5
Column length (m) 30.30.30.60.7.5
Carrier gas HeliumHeliumNitrogenNitrogenHelium
Substrate      
Column diameter (mm) 0.250.250.250.250.10
Phase thickness (mum) 0.250.250.250.2510.
Tstart (C) 50.50.45.60.60.
Tend (C) 300.250.230.250.240.
Heat rate (K/min) 3.3.3.5.3.
Initial hold (min)  2.   
Final hold (min) 30.10. 10. 
I 1085.1086.1072.1093.1092.
ReferenceIsidorov, Lech, et al., 2008Lo Presti, Sciarrone, et al., 2008Mierendorff, Stahl-Biskup, et al., 2008Mosayebi, Amin, et al., 2008Shellie, 2008
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5HP-5HP-5HP-5 MSDB-5
Column length (m) 20.25.30.30.50.
Carrier gas HeliumHeliumHeliumHeliumNitrogen
Substrate      
Column diameter (mm) 0.180.250.250.250.20
Phase thickness (mum) 0.200.250.320.250.32
Tstart (C) 50.60.60.50.60.
Tend (C) 280.240.250.230.220.
Heat rate (K/min) 4.4.5.3.5.
Initial hold (min) 1.2.30.10.3.
Final hold (min)    10.5.
I 1094.1089.1090.1088.1087.
ReferenceSkalicka-Wozniak, Los, et al., 2008Verdian-rizi, 2008Yassa and Akhani, 2008Adams, Beauchamp, et al., 2007Amiri, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5CP Sil 5 CBHP-5MSDB-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.260.25
Phase thickness (mum)  0.250.250.250.25
Tstart (C) 70.60.60.60.60.
Tend (C) 240.300.280.240.280.
Heat rate (K/min) 5.4.3.3.3.
Initial hold (min)      
Final hold (min)      
I 1089.1076.1086.1083.1088.
ReferenceAsekun, Olusegun, et al., 2007Baran, von Reuss, et al., 2007Basta, Tzakou, et al., 2007Bos, Woerdenbag, et al., 2007Bozin B., Mlmica-Dukic N., et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5DB-5DB-1Col-Elite 5MSDBP-5
Column length (m) 30.30.60.30.25.
Carrier gas N2HeliumNitrogenHeHelium
Substrate      
Column diameter (mm) 0.250.260.250.250.25
Phase thickness (mum) 0.250.250.250.250.22
Tstart (C) 50.60.60.30.40.
Tend (C) 240.290.250.246.250.
Heat rate (K/min) 5.3.4.3.3.
Initial hold (min) 1. 1. 1.
Final hold (min) 4. 10. 10.
I 1088.1083.1083.1097.1060.
ReferenceCheraif, Ben Jannet, et al., 2007Elfami, Bos, et al., 2007Ghasempour, Shirinpour, et al., 2007Gudaityte and Venskutonis R.P., 2007Heravi and Sereshti, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RTX-5 MSDB-5SE-30HP-5ZB-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 45.60.40.40.60.
Tend (C) 210.300.250.250.220.
Heat rate (K/min) 3.3.5.5.4.
Initial hold (min)   5.5.5.
Final hold (min)   10.10.20.
I 1091.1080.1089.1086.1097.
ReferenceHudaib and Aburjai, 2007Limberger, Scopel, et al., 2007Loizzo, Tundis, et al., 2007Loizzo, Tundis, et al., 2007Mohottalage, Tabacchi, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5Methyl SiliconeDB-1
Column length (m) 30.30.25.50.50.
Carrier gas HeliumHeliumH2HeliumHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.250.33 0.25
Tstart (C) 50.60.60.50.95.
Tend (C) 260.300.240.240.240.
Heat rate (K/min) 2.53.3.3.4.
Initial hold (min) 1.    
Final hold (min) 20.    
I 1073.1061.1090.1088.1085.
ReferenceMonser-Esfahani, Karamkhani, et al., 2007Moreno, Lima, et al., 2007Oliveira, Leitão, et al., 2007Ozcan and Chalchat, 2007Pala-Paul, Brophy, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1BPX-5BPX-5DB-1DB-1
Column length (m) 30.50.50.60.60.
Carrier gas HeHeHeNitrogen 
Substrate      
Column diameter (mm) 0.20.220.220.250.25
Phase thickness (mum) 0.21.1.0.250.25
Tstart (C) 70.50.50.60.60.
Tend (C) 220.300.300.250.250.
Heat rate (K/min) 3.4.4.4.5.
Initial hold (min)  1.1.1. 
Final hold (min) 15.10.10.10. 
I 1077.1111.1105.1083.1082.
ReferencePinto, Salgueiro, et al., 2007Rali, Wossa, et al., 2007Rali, Wossa, et al., 2007Reza, Ebrahim, et al., 2007Salehi, Asghari, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5DBP-5DB-5DB-5
Column length (m) 60.30.25.30.30.
Carrier gas HeHeHelium  
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.220.250.25
Tstart (C) 60.50.40.40.40.
Tend (C) 250.240.250.210.250.
Heat rate (K/min) 5.4.3.2.2.
Initial hold (min)   1.  
Final hold (min)   10.33.33.
I 1081.1086.1060.1098.1097.
ReferenceSalehi, Fakhari, et al., 2007Sefidkon, Abbasi, et al., 2007Sereshti and Samadi, 2007Sylvestre, Longtin, et al., 2007Sylvestre, Pichette, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Elite-5MSHP-5 MSHP-5MSHP-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.50.250.250.250.32
Tstart (C) 40.60.60.40.60.
Tend (C) 280.280.280.250.250.
Heat rate (K/min) 4.3.3.3.5.
Initial hold (min) 5.  5.30.
Final hold (min) 10.  10. 
I 1085.1092.1052.1083.1090.
ReferenceTava, Pecetti, et al., 2007Tsokou, Georgopoulos, et al., 2007Tzakou, Bazos, et al., 2007Vichi, Riu-Aumatell, et al., 2007Yassa and Akhani, 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5CP Sil 5 CBZB-5AT-5
Column length (m) 30.30.25.30.60.
Carrier gas N2N2He He
Substrate      
Column diameter (mm) 0.250.25 0.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 50.50.80.40.60.
Tend (C) 280.280.270.300.200.
Heat rate (K/min) 9.9.10.2.4.
Initial hold (min) 3.3.   
Final hold (min) 3.3.  20.
I 1080.1084.1082.1087.1088.
ReferenceAbdelwahed, Hayder, et al., 2006Abdelwahed, Hayder, et al., 2006Ayoub, Al-Azizi, et al., 2006Biondi, Sari, et al., 2006Borges, Rojas, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1HP-1HP-1SPB-1DB-1
Column length (m) 50.50.50.30.60.
Carrier gas HeHeHeHeliumNitrogen
Substrate      
Column diameter (mm) 0.220.20.20.200.25
Phase thickness (mum) 0.250.50.330.20 
Tstart (C) 60.60.60.70.40.
Tend (C) 220.250.250.220.200.
Heat rate (K/min) 2.2.2.3.2.
Initial hold (min)   4. 1.
Final hold (min) 20.120.30.15.9.
I 1076.1079.1079.1076.1077.
ReferenceBoti, Muselli, et al., 2006Castel, Fernandez, et al., 2006Castel, Fernandez, et al., 2006Cavaleiro, Pinto, et al., 2006Chen, Sheu, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-5HP-5MSDB-5
Column length (m) 30.30.30.30.30.
Carrier gas N2He  Helium
Substrate      
Column diameter (mm) 0.250.320.320.250.26
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 70.60.60.60.60.
Tend (C) 230.246.230.280.290.
Heat rate (K/min) 2.3.3.4.3.
Initial hold (min) 2.    
Final hold (min) 20. 15.  
I 1086.1087.1077.1091.1083.
ReferenceChoi, 2006Coronel, Cerda-Garcia-Rojas, et al., 2006Damjanovic, Skala, et al., 2006Ebrahim Sajjadi and Mehregan, 2006Elfami, Komar, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1HP-5HP-1DB-5
Column length (m) 50.50.30.50.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.250.20.25
Phase thickness (mum) 0.250.250.250.330.25
Tstart (C) 60.60.50.60.50.
Tend (C) 220.220.300.250.250.
Heat rate (K/min) 2.2.5.2.3.
Initial hold (min)   5.  
Final hold (min) 20.20.5.40.10.
I 1078.1078.1085.1079.1084.
ReferenceFanciullino, Tomi, et al., 2006Fanciullino, Tomi, et al., 2006Figuérédo, Cabassu, et al., 2006Filippi, Lanfranchi, et al., 2006Havlik, Kokoska, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5DB-5DB-1CP Sil 8 CB
Column length (m) 30.30.30.60.30.
Carrier gas  HeHelium  
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.60.70.40.
Tend (C) 220.240.260.230.250.
Heat rate (K/min) 3.4.3.2.3.
Initial hold (min)    2.5.
Final hold (min) 3.  20.20.
I 1089.1088.1089.1080.1087.
ReferenceHymete, Rohloff, et al., 2006Ibañez and Usubillaga, 2006Javidnia, Miri, et al., 2006Lan Phi N.T., Nishiyama C., et al., 2006Li, Lee, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBHP-5 MSHP-55 % Phenyl methyl siloxane
Column length (m) 30.30.30.30.30.
Carrier gas N2N2NitrogenN2Helium
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.250.250.250.520.25
Tstart (C) 50.50.50.50.60.
Tend (C) 300.200.280.280.280.
Heat rate (K/min) 4.5.5.5.3.
Initial hold (min)      
Final hold (min)   5.5.30.
I 1082.1077.1088.1088.1054.
ReferenceLis and Milczarek, 2006Martin, Joseph, et al., 2006Marzouk, Mansour, et al., 2006Marzouk, Neffati, et al., 2006Marongiu, Piras, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BP-1DB-5DB-5NB-30
Column length (m) 30.25.30.30.30.
Carrier gas HeliumHeHeHeHe
Substrate      
Column diameter (mm) 0.250.30.250.250.2
Phase thickness (mum) 0.25 0.250.250.25
Tstart (C) 50.70.60.60.50.
Tend (C) 250.220.220.220.250.
Heat rate (K/min) 3.4.4.4.2.
Initial hold (min) 5.2. 5. 
Final hold (min)  10.   
I 1086.1081.1091.1092.1080.
ReferenceMirza, Navaei, et al., 2006Moody, Gundidza, et al., 2006Morteza-Semnani, Akbarzadeh, et al., 2006Morteza-Semnani K., Saeedi M., et al., 2006Orav, Raal, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-1HP-5DB-5
Column length (m) 25.30.50.30.30.
Carrier gas N2HeN2HeHydrogen
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (mum) 0.150.250.250.250.25
Tstart (C) 50.60.95.60.70.
Tend (C) 200.280.240.220.280.
Heat rate (K/min) 4.5.4.5.4.
Initial hold (min) 3.0.5 10.4.
Final hold (min)  2.   
I 1085.1088.1086.1089.1089.
ReferenceOuamba, Ouabonzi, et al., 2006Ozel, Gogus, et al., 2006Pala-Paul J., Perez-Alonso M.J., et al., 2006Pintore G., Chessa M., et al., 2006Pino, Marbot, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5MSDB-5DB-5ZB-5
Column length (m) 30.30.30.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.50.60.60.40.
Tend (C) 280.250.200.260.300.
Heat rate (K/min) 3.10.2.5.2.
Initial hold (min)  5.   
Final hold (min)   60.  
I 1054.1088.1088.1088.1087.
ReferencePitarokili, Tzakou, et al., 2006Robinson, 2006Rout, Naik, et al., 2006Sabulal, Dan, et al., 2006Sari M., Biondi D.M., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1FSOT-RSL-200DB-5DB-1HP-5
Column length (m) 60.30.30.60.25.
Carrier gas  HydrogenHeHeN2
Substrate      
Column diameter (mm) 0.250.320.250.250.2
Phase thickness (mum) 0.250.250.25 0.33
Tstart (C) 70.40.40.40.30.
Tend (C) 230.280.240.250.280.
Heat rate (K/min) 2.6.4.4.3.
Initial hold (min) 2.5.   
Final hold (min) 20.5.   
I 1079.1087.1087.1078.1091.
ReferenceSawamura, Onishi, et al., 2006Schmidt, Jirovetz, et al., 2006Sefidkon and Jamzad, 2006Sefidkon, Jamzad, et al., 2006Shafi, Jose, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBSPB-5DB-5DB-1HP-5
Column length (m) 25.60.30.50.25.
Carrier gas  HeN2N2H2
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (mum)  1.0.250.250.52
Tstart (C) 50.40.60.90.50.
Tend (C) 230.230.240.240.280.
Heat rate (K/min) 3.3.4.4.2.5
Initial hold (min)  5.  5.
Final hold (min)  2.   
I 1089.1102.1089.1068.1087.
ReferenceTesso, Kubeczka, et al., 2006Tornambe, Cornu, et al., 2006Trilles, Bombarda, et al., 2006Velasco-Negueruela, Pérez-Alonso, et al., 2006Wang, Kong, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5SPB-1SPB-1DB-5DB-5
Column length (m) 30.50.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.250.330.250.250.25
Tstart (C) 60.50.50.40.40.
Tend (C) 250.220.250.250.250.
Heat rate (K/min) 10.4.4.4.4.
Initial hold (min) 2.1.1.  
Final hold (min) 10.10.10.  
I 1094.1077.1072.1062.1082.
ReferenceWang, Yang, et al., 2006Wong, Lim, et al., 2006Wong, Sivasothy, et al., 2006Yadegarinia, Gachkar, et al., 2006Yadegarinia, Gachkar, et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-5Methyl SiliconeSPB-5
Column length (m) 30.30.50.60.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.2490.30.30.32
Phase thickness (mum) 0.250.250.25 1.
Tstart (C) 60.60.60.50.40.
Tend (C) 280.290.240.240.230.
Heat rate (K/min) 3.3.2.3.3.
Initial hold (min)     5.
Final hold (min)      
I 1083.1085.1095.1088.1098.
ReferenceBasta, Tzakou, et al., 2005Bos, Stojanova, et al., 2005Chagonda and Chalchat, 2005Chalchat and Özcan, 2005Cornu, Kondjoyan, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-1HP-5HP-5MSCP Sil 5 CB
Column length (m) 60.50.30.25.30.
Carrier gas He HeHeN2
Substrate      
Column diameter (mm) 0.250.20.250.250.25
Phase thickness (mum) 0.250.250.25 0.25
Tstart (C) 60.60.50.50.60.
Tend (C) 250.250.300.250.250.
Heat rate (K/min) 5.2.5.3.5.
Initial hold (min)  60.5.3. 
Final hold (min)   5.10.10.
I 1079.1077.1085.1089.1086.
ReferenceFakhari, Salehi, et al., 2005Fernandez, Lizzani-Cuvelier, et al., 2005Figuérédo, Cabassu, et al., 2005Ghasemi Y., Faridi P., et al., 2005Jassbi, Mehrdad, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200DB-1HP-5CP Sil 5 CBCP Sil 5 CB
Column length (m) 30.30.60.25.25.
Carrier gas  HeHe  
Substrate      
Column diameter (mm) 0.250.250.320.250.25
Phase thickness (mum) 0.250.250.250.150.15
Tstart (C) 40.50.30.50.50.
Tend (C) 280.265.260.230.230.
Heat rate (K/min) 6.2.52.3.3.
Initial hold (min) 2.1.2.  
Final hold (min) 10.30.28.  
I 1089.1072.1086.51083.1083.
ReferenceJirovetz, Buchbauer, et al., 2005Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005Leffingwell and Alford, 2005Ogunwande, Olawore, et al., 2005Olawore, Ogunwande, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5RTX-5 MSHP-5MSSPB-5HP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.250.25 0.250.32
Tstart (C) 70.50.60.60.60.
Tend (C) 240.280.280.250.250.
Heat rate (K/min) 5.8.3.4.5.
Initial hold (min)  2. 2.3.
Final hold (min)  2. 20. 
I 1089.1091.1089.1088.1091.
ReferenceOyedeji, Yani, et al., 2005Pellati, Benvenuti, et al., 2005Petrakis, Roussis, et al., 2005Pino, Marbot, et al., 2005Pourmortazavi, Ghadiri, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBCP Sil 5 CBHP-5HP-5MSHP-5MS
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.25 0.250.25
Tstart (C) 40.40.60.60.60.
Tend (C) 220.220.240.280.275.
Heat rate (K/min) 4.4.5.4.4.
Initial hold (min) 1.1.   
Final hold (min)      
I 1089.1089.1088.1087.1087.
ReferenceRohloff and Bones, 2005Rohloff and Bones, 2005Saeidnia, Gohari, et al., 2005Sajjadi S.E. and Eskandari B., 2005Sajjadi and Ghannadi, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5DB-1DB-5HP-5MS
Column length (m) 30.30.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.25 0.25
Tstart (C) 60.60.60.40.60.
Tend (C) 280.220.250.240.280.
Heat rate (K/min) 4.3.5.4.3.
Initial hold (min)  4.  5.
Final hold (min)   10.  
I 1085.1086.1064.1087.1092.
ReferenceSajjadi, 2005Salehi, Sefidkon, et al., 2005Salehi, Sonboli, et al., 2005Sefidkon and Jamzad, 2005Setzer, Noletto, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase PE-5DB-5HP-5MSRTX-1RTX-1
Column length (m) 30.30.30.60.60.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.60.60.
Tend (C) 230.230.280.250.25.
Heat rate (K/min) 5.3.3.5.5.
Initial hold (min) 2.    
Final hold (min) 4.20. 10.10.
I 1078.1089.1089.1083.1082.
ReferenceSingh, Raina, et al., 2005Skoula and Grayer, 2005Slavkovska, Couladis, et al., 2005Sonboli A., Fakhari A.R., et al., 2005Sonboli, Salehi, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5HP-5MSHP-5MSDB-5
Column length (m) 60.30.30.30.30.
Carrier gas He HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.50.60.60.
Tend (C) 250.210.240.280.280.
Heat rate (K/min) 5.2.3.3.3.
Initial hold (min)  2.3.  
Final hold (min) 10.33.   
I 1081.1099.1095.1052.1058.
ReferenceSonboli, Salehi, et al., 2005, 2Stevanovic, Garneau, et al., 2005Tepe B., Sokmen M., et al., 2005Tzakou, Bazos, et al., 2005Tzakou and Constantinidis, 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5MSSPB-1BP-1
Column length (m) 50.50.30.50.50.
Carrier gas N2  He 
Substrate      
Column diameter (mm) 0.250.250.250.20.22
Phase thickness (mum) 0.250.250.250.330.25
Tstart (C) 90.60.40.50.60.
Tend (C) 240.240.220.220.220.
Heat rate (K/min) 4.3.3.4.2.
Initial hold (min)   5.3. 
Final hold (min)   10.30.20.
I 1068.1066.1083.1076.1078.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2005Velasco-Negueruela, Pérez-Alonso, et al., 2005, 2Vichi, Riu-Aumatell, et al., 2005Wong, Lee, et al., 2005Blanc, Muselli, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-52SPB-5DB-1DB-5ZB-5
Column length (m) 25.60.25.25.60.
Carrier gas N2He NitrogenHe
Substrate      
Column diameter (mm) 0.320.320.250.250.25
Phase thickness (mum) 0.151.0.250.250.25
Tstart (C) 45.60.60.60.40.
Tend (C) 200.200.180.240.260.
Heat rate (K/min) 3.4.3.3.6.
Initial hold (min) 5. 10. 4.6
Final hold (min) 30.30.10. 1.
I 1079.1092.1089.1088.1099.
ReferenceCakir, Kordali, et al., 2004Gauvin, Ravaomanarivo, et al., 2004bin Jantan, Ayop, et al., 2004JAvidnia, Mojab, et al., 2004Jürgens and Dötterl, 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5SE-54HP-5MSRTX-1DB-5
Column length (m) 60.30.30.30.30.
Carrier gas HeHeHeN2 
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.50.60.40.
Tend (C) 280.260.230.300.210.
Heat rate (K/min) 4.2.5.4.2.
Initial hold (min) 4.5.2. 2.
Final hold (min)   10. 33.
I 1086.1086.1088.1080.1098.
ReferenceKalvandi, Sefidkon, et al., 2004Kilic, Hafizoglu, et al., 2004Li and Jiang, 2004Lis, Boczek, et al., 2004Lopez Arze, Collin, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-5MSNB-30NB-30DB-1
Column length (m) 30.30.50.50.50.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.20.20.22
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.50.50.70.
Tend (C) 280.280.250.250.220.
Heat rate (K/min) 3.3.2.2.4.
Initial hold (min)      
Final hold (min) 30.30.   
I 1051.1050.1080.1080.1082.
ReferenceMarongiu, Piras, et al., 2004Marongiu, Porcedda, et al., 2004Orav, Stulova, et al., 2004Orav, Stulova, et al., 2004Palá-Paúl, García-Jiménez, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1NB-30NB-30DB-5Methyl Silicone
Column length (m) 50.50.50.30.60.
Carrier gas N2HeHeHeHe
Substrate      
Column diameter (mm) 0.250.20.200.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 95.50.50.35.60.
Tend (C) 240.250.250.220.200.
Heat rate (K/min) 4.2.2.2.54.
Initial hold (min)     1.
Final hold (min)    6.20.
I 1074.1080.1080.1089.1080.
ReferencePalá-Paúl, Velasco-Negueruela, et al., 2004Raal, Arak, et al., 2004Raal, Paaver, et al., 2004Rohloff, Mordal, et al., 2004Rojas, Usubillaga, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5 MSHP-5MSHP-5MSDB-1DB-1
Column length (m) 30.30.30.60.60.
Carrier gas HeliumHeHe Nitrogen
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.60.70.70.
Tend (C) 200.280.280.230.230.
Heat rate (K/min) 4.4.4.2.2.
Initial hold (min) 1.  2.2.
Final hold (min) 20.  20. 
I 1080.1084.1090.1086.1086.
ReferenceRoyas, Usubillaga, et al., 2004Sadeghpour, Asghari, et al., 2004Sajjadi and Shahpiri, 2004Sawamura, Son, et al., 2004Sawamura, Sou, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-1DB-5DB-5CP Sil 5 CB
Column length (m) 30.30.30.30.20.
Carrier gas  He HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.330.250.250.25
Tstart (C) 50.40.60.60.100.
Tend (C) 250.260.300.240.270.
Heat rate (K/min) 3.2.3.3.8.
Initial hold (min) 5.5.  2.
Final hold (min)  20.   
I 1088.1061.1079.1087.1074.
ReferenceSefidkon, Jamzad, et al., 2004Senatore, Napolitano, et al., 2004Suyenaga, Apel, et al., 2004Tellez, Khan, et al., 2004Thappa, Bakshi, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5BPX-5CP Sil 8 CBCP Sil 8 CBDB-5
Column length (m) 30.25.30.30.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.220.250.320.249
Phase thickness (mum) 0.251.0.250.250.25
Tstart (C) 60.60.50.50.60.
Tend (C) 300.250.200.200.300.
Heat rate (K/min) 3.3.10.5.3.
Initial hold (min)  5.3.5. 
Final hold (min)  10.2.  
I 1089.1096.1086.1088.1086.
ReferenceTirillini, Pellegrino, et al., 2004Vilaseca, Guy, et al., 2004Wang and Guo-Y. -L., 2004Wang, Guo, et al., 2004Woerdenbag, Windono, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSHP-5DB-1HP-5MSRTX-5Sil
Column length (m) 30.30.60.30.30.
Carrier gas HeN2HeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.60.70.60.70.
Tend (C) 275.220.230.280.200.
Heat rate (K/min) 4.5.2.3.4.
Initial hold (min)  10.2.  
Final hold (min)   20. 10.
I 1088.1082.1086.1086.1086.
ReferenceAfsharypuor and Jahromy, 2003Bertoli, Menichini, et al., 2003Choi, 2003Couladis, Özcan, et al., 2003Dudai, Larkov, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5HP-5MSHP-1
Column length (m) 60.60.60.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.320.320.320.250.25
Phase thickness (mum)    0.250.25
Tstart (C) 50.50.50.60.70.
Tend (C) 220.220.200.220.200.
Heat rate (K/min) 3.3.3.5.10.
Initial hold (min)    20. 
Final hold (min)    20. 
I 1090.1090.1090.1094.1079.
ReferenceEdris and Farrag, 2003Edris and Farrag, 2003Edris, Shalaby, et al., 2003Feizbaksh, Saber Tehrani, et al., 2003Fekam Boyom, Amvam Zollo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-5MSHP-5HP-5MSRSL-200
Column length (m) 30.30.30.30.30.
Carrier gas N2HeHeHeH2
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 50.60.60.60.40.
Tend (C) 200.280.275.275.280.
Heat rate (K/min) 5.4.4.4.6.
Initial hold (min)     5.
Final hold (min)     5.
I 1068.1088.1086.1087.1079.
ReferenceFekam Boyom, Ngouana, et al., 2003Ghasemi, Asghari, et al., 2003Ghannadi and Zolfaghari, 2003Hajhashemi, Ghannadi, et al., 2003Jirovetz, Buchbauer, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200SE-30CP Sil 5 CBDB-5MSDB-5
Column length (m) 30.12.25.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.220.250.250.25
Phase thickness (mum) 0.250.30.250.250.25
Tstart (C) 40.70.35.60.60.
Tend (C) 280.220.280.240.280.
Heat rate (K/min) 6.3.5.3.3.
Initial hold (min) 5. 2.5  
Final hold (min) 5.   30.
I 1084.1076.1077.1087.1070.
ReferenceJirovetz, Buchbauer, et al., 2003, 2Kambouche and El-Abed, 2003Kanjilal, Kotoky, et al., 2003Maia, Taveira, et al., 2003Marongiu, Porcedda, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5ZB-1DB-1HP-5OV-101
Column length (m) 50.30.60.30.50.
Carrier gas HeN2HeHeliumHe
Substrate      
Column diameter (mm) 0.20.250.250.320.2
Phase thickness (mum) 0.250.250.25 0.5
Tstart (C) 50.45.50.70.50.
Tend (C) 220.230.270.210.250.
Heat rate (K/min) 3.3.4.2.2.
Initial hold (min) 2.    
Final hold (min)    60. 
I 1088.1072.1087.1086.1077.
ReferenceMasotti, Juteau, et al., 2003Mierendorff, Stahl-Biskup, et al., 2003Mirza, Nik, et al., 2003Mookdasanit, Tamura, et al., 2003Orav, Kailas, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBDB-1DB-5HP-5DB-1
Column length (m) 25.50.30.30.60.
Carrier gas H2N2H2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.150.250.250.250.25
Tstart (C) 50.95.60.60.50.
Tend (C) 230.240.280.280.250.
Heat rate (K/min) 3.4.4.3.4.
Initial hold (min)   10.  
Final hold (min)   40.  
I 1081.1081.1088.1072.1076.
ReferenceOyedeji, Ekundayo, et al., 2003Perez-Alonso, Velasco-Negueruela, et al., 2003Pino, Marbot, et al., 2003Pitarokili, Tzakou, et al., 2003Pourmortazavi, Sefidkon, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-5DB-1DB-5HP-5
Column length (m) 30.30.60.30.60.
Carrier gas N2HeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.50.60.40.
Tend (C) 230.280.280.240.250.
Heat rate (K/min) 2.4.4.3.5.
Initial hold (min)     15.
Final hold (min)      
I 1082.1089.1084.1087.1088.
ReferenceRotman, Ahumada, et al., 2003Sajjadi and Mehregan, 2003Shahmir, Ahmadi, et al., 2003da Silva, Luz, et al., 2003Stashenko, Jaramillo, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1Cross-Linked MethylsiliconeHP-5HP-5HP-5
Column length (m) 50.25.25.25.25.
Carrier gas N2HeH2H2Helium
Substrate      
Column diameter (mm) 0.250.20.320.320.32
Phase thickness (mum) 0.250.330.530.530.53
Tstart (C) 90.70.40.40.40.
Tend (C) 240.250.280.280.280.
Heat rate (K/min) 4.4.4.4.4.
Initial hold (min)      
Final hold (min)      
I 1069.1068.1088.1089.1084.
ReferenceVelasco-Negueruela, Pérez-Alonso, et al., 2003Velasco-Negueruela, Pérez-Alonso, et al., 2003, 2Velickovic, Randjelovic, et al., 2003Velickovic, Randjelovic, et al., 2003Velickovic, Ristic, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5DB-5DB-5DB-5
Column length (m) 25.30.30.25.30.
Carrier gas HeliumHeHeN2He
Substrate      
Column diameter (mm) 0.320.250.250.250.249
Phase thickness (mum) 0.530.320.250.250.25
Tstart (C) 40.60.60.50.60.
Tend (C) 280.250.240.250.300.
Heat rate (K/min) 4.5.3.4.3.
Initial hold (min)  30.   
Final hold (min)    10.5.
I 1089.1097.1085.1089.1087.
ReferenceVelickovic, Ristic, et al., 2003Yassa, Akhani, et al., 2003Zoghbi, Andrade, et al., 2003Zrira, Elamrani, et al., 2003Bos, Koulman, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-15 % Phenyl methyl siloxaneDB-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeN2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.70.75.60.50.
Tend (C) 280.220.200.280.250.
Heat rate (K/min) 3.3.3.3.4.
Initial hold (min)   4. 5.
Final hold (min) 30.15.8.  
I 1070.1077.1089.1079.1089.
ReferenceCaredda, Marongiu, et al., 2002Cavaleiro, Salgueiro, et al., 2002Cicció and Gómez-Laurito, 2002Congiu, Falconieri, et al., 2002Farah, Fechtal. M., et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1PTE-5SE-30RSL-200
Column length (m) 30.30.60.50.30.
Carrier gas HeH2H2HeH2
Substrate      
Column diameter (mm) 0.250.320.320.250.32
Phase thickness (mum) 0.250.250.300.250.25
Tstart (C) 60.40.60.70.40.
Tend (C) 240.245.285.240.280.
Heat rate (K/min) 3.3.4.34.6.
Initial hold (min)  20.  5.
Final hold (min)     5.
I 1089.1067.1088.1086.1078.
ReferenceFlamini, Ertugrul, et al., 2002Gancel, Ollé, et al., 2002Gudzic, Djokovic, et al., 2002Iñigo, Palá-Paúl, et al., 2002Jirovetz, Buchbauer, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200CP Sil 8 CBDB-1DB-5DB-5
Column length (m) 30.30.25.30.30.
Carrier gas H2HeHeHeHe
Substrate      
Column diameter (mm) 0.320.250.230.250.25
Phase thickness (mum) 0.250.250.200.250.25
Tstart (C) 50.50.50.60.35.
Tend (C) 280.220.200.240.280.
Heat rate (K/min) 6.3.3.3.3.
Initial hold (min) 5.2.3. 2.
Final hold (min) 5. 30. 15.
I 1074.1087.1089.1090.1089.
ReferenceJirovetz, Ngassoum, et al., 2002Juteau, Masotti, et al., 2002Khallouki, Younos, et al., 2002Kobaisy, Tellez, et al., 2002Krauze-Baranowska, Mardarowicz, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-101DB-5DB-5MSOV-101
Column length (m) 30.25.30.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.320.250.250.32
Phase thickness (mum) 0.25 0.250.25 
Tstart (C) 35.50.60.60.50.
Tend (C) 280.200.240.240.200.
Heat rate (K/min) 4.5.3.3.5.
Initial hold (min) 2.    
Final hold (min) 15.    
I 1090.1082.1086.1089.1080.
ReferenceKrauze-Baranowska, Mardarowicz, et al., 2002, 2Kuiate, Bessière, et al., 2002Maia, da Silva, et al., 2002Maia, Zoghbi, et al., 2002Menut, Bessière, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBHP-5OV-101ZEBRON-5DB-1
Column length (m) 25.30.50.6.50.
Carrier gas He HeHeN2
Substrate      
Column diameter (mm) 0.250.250.20.250.25
Phase thickness (mum) 0.390.250.50.250.25
Tstart (C) 60.60.50.40.80.
Tend (C) 220.240.250.200.225.
Heat rate (K/min) 5.3.2.3.4.
Initial hold (min)    5. 
Final hold (min)    15. 
I 1080.1091.1078.1053.1068.
ReferenceMojab, Rustaiyan, et al., 2002Novak, Langbehn, et al., 2002Orav, Kailas, et al., 2002Öztürk, Akay, et al., 2002Palá-Paúl, Pérez-Alonso, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-1DB-1DB-1HP-5
Column length (m) 30.60.50.50.30.
Carrier gas HeliumHeN2N2H2
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 60.40.95.60.40.
Tend (C) 250.280.240.240.280.
Heat rate (K/min) 4.4.4.3.4.
Initial hold (min) 2.5.   
Final hold (min) 20.    
I 1088.1077.1068.1066.1088.
ReferencePino, Marbot, et al., 2002Sefidkon, 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002Velasco-Negueruela, Pérez-Alonso, et al., 2002, 2Velickovic, Randjelovic, et al., 2002
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-5MSDB-5DB-5MSSPB-5
Column length (m) 60.30.30.30.60.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.32
Phase thickness (mum) 0.250.250.250.25 
Tstart (C) 50.60.60.60.40.
Tend (C) 250.270.240.240.220.
Heat rate (K/min) 4.3.3.3.3.
Initial hold (min) 5.   5.
Final hold (min)     15.
I 1077.1088.1089.1075.1089.
ReferenceYamini, Sefidkon, et al., 2002Zoghbi, Andrade, et al., 2002Zoghbi, Andrade, et al., 2002, 2Cherchi, Deidda, et al., 2001Cornu, Carnat, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1DB-1HP-5OV-1HP-5
Column length (m) 60.60.30.30.30.
Carrier gas HeHeN2H2N2
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (mum) 0.250.250.250.30.25
Tstart (C) 40.40.60.50.60.
Tend (C) 280.280.220.250.220.
Heat rate (K/min) 4.4.5.3.5.
Initial hold (min) 5.5.10.1.10.
Final hold (min)    20. 
I 1070.1078.1089.1076.1089.
ReferenceDabiri and Sefidkon, 2001Dabiri and Sefidkon, 2001Flamini, Cioni, et al., 2001Gallori, Bilia, et al., 2001Gallori, Flamini, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200RTX-1SPB-5BP-1CBP-1
Column length (m) 30.30.60.50.25.
Carrier gas H2N2HeliumHeNitrogen
Substrate      
Column diameter (mm) 0.320.250.250.220.25
Phase thickness (mum) 0.250.250.250.250.25
Tstart (C) 40.60.50.60.50.
Tend (C) 280.300.240.230.210.
Heat rate (K/min) 6.4.3.2.3.
Initial hold (min) 5. 3. 2.
Final hold (min) 5. 10.35. 
I 1079.1083.1097.1078.1076.
ReferenceJirovetz L., Buchbauer G., et al., 2001Kalemba, Marschall, et al., 2001Kim and Lee, 2001Lota, de Rocca Serra, et al., 2001Ly, Yamauchi, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSDB-1RSL-200OV-101OV-101
Column length (m) 30.60.30.50.50.
Carrier gas HeHeH2HeHe
Substrate      
Column diameter (mm) 0.250.250.320.20.2
Phase thickness (mum) 0.250.250.250.5 
Tstart (C) 60.50.40.50.50.
Tend (C) 240.270.280.250.250.
Heat rate (K/min) 3.4.6.2.2.
Initial hold (min)   5.  
Final hold (min) 30. 5.  
I 1088.1076.1077.1073.1076.
ReferenceMarongiu, Porcedda, et al., 2001Mirza, Ahmadi, et al., 2001Ngassoum, Jirovetz, et al., 2001Orav, Kailas, et al., 2001Orav and Kann, 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-1DB-5DB-5DB-5
Column length (m) 50.30.60.30.30.
Carrier gas HeN2HeH2He
Substrate      
Column diameter (mm) 0.20.250.250.250.25
Phase thickness (mum)  0.25 0.250.25
Tstart (C) 50.80.50.60.60.
Tend (C) 250.225.250.285.240.
Heat rate (K/min) 2.4.3.3.3.
Initial hold (min)   5.  
Final hold (min)      
I 1076.1045.1090.1086.1089.
ReferenceOrav and Kann, 2001Palá-Paúl, Pérez-Alonso, et al., 2001Rousis, Papadogianni, et al., 2001Santos-Gomes and Fernandes-Ferreira, 2001Tellez M., Estell R., et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1OV-101OV-101CP Sil 5 CBCP Sil 5 CB
Column length (m) 30.50.50.25.25.
Carrier gas HeN2N2 He
Substrate      
Column diameter (mm) 0.320.250.250.250.25
Phase thickness (mum) 0.25  0.150.4
Tstart (C) 50.80.80.50.60.
Tend (C) 250.200.200.230.260.
Heat rate (K/min) 2.2.2.3.5.
Initial hold (min)     40.
Final hold (min)      
I 1083.1082.1082.1078.1074.
ReferenceVijayanand, Rao, et al., 2001Yang, 2001Yang, 2001, 2Asekun and Ekundayo, 2000Baser, Özek, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase RSL-200DB-1DB-5BP-1HP-5
Column length (m) 60.25.30.25.30.
Carrier gas H2NitrogenN2N2He
Substrate      
Column diameter (mm) 0.320.500.220.330.25
Phase thickness (mum) 0.250.250.251.00.25
Tstart (C) 40.60.70.60.60.
Tend (C) 250.220.230.275.275.
Heat rate (K/min) 6.5.4.4.4.
Initial hold (min)   2.  
Final hold (min)   20.  
I 1077.1081.1092.1087.1087.
ReferenceJirovetz, Puschmann, et al., 2000Mallavarapu, Rao, et al., 2000Mitiku, Sawamura, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-101DB-5Methyl SiliconeSPB-1
Column length (m) 30.50.30.60.50.
Carrier gas HeNitrogenHe  
Substrate      
Column diameter (mm) 0.250.250.250.250.2
Phase thickness (mum) 0.25 0.250.250.33
Tstart (C) 40.40.60.40.60.
Tend (C) 260.200.240.220.260.
Heat rate (K/min) 2.2.3.5.4.
Initial hold (min) 5.10. 10. 
Final hold (min) 2.    
I 1077.1082.1090.1080.401080.
ReferenceSenatore, Napolitano, et al., 2000Tamura, Boonbumrung, et al., 2000Tellez, Dayan, et al., 2000Baraldi, Rapparini, et al., 1999Choo, Wong, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SE-30RTX-1DB-1OV-101CBP-1
Column length (m) 30.30.25.25.25.
Carrier gas N2N2He He
Substrate      
Column diameter (mm) 0.250.250.250.320.3
Phase thickness (mum) 0.250.250.25  
Tstart (C) 60.60.50.50.60.
Tend (C) 220.300.290.200.240.
Heat rate (K/min) 4.4.4.5.4.
Initial hold (min) 10.    
Final hold (min)      
I 1075.1082.1087.1082.1082.
ReferenceJassbi, Ahmad, et al., 1999Kalemba, 1999Koulman, 1999Kuiate, Zollo, et al., 1999Labuckas, Zygadlo, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5OV-1OV-1OV-101CP Sil 5 CB
Column length (m) 30.25. 50.25.
Carrier gas  H2 HeliumHe
Substrate      
Column diameter (mm) 0.320.25 0.200.25
Phase thickness (mum) 1.0.25 0.50 
Tstart (C) 40.40.50.30.50.
Tend (C) 200.220.160.100.230.
Heat rate (K/min) 3.3.2.1.3.
Initial hold (min) 5.5. 6. 
Final hold (min)  5.   
I 1090.1075.1080.1075.1077.
ReferenceMeynier, Novelli, et al., 1999Oberhofer, Nikiforov, et al., 1999Orav, Kailas, et al., 1999Orav, Kailas, et al., 1999, 2Oyedeji, Olawore, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101SE-30BP-1CP Sil 5 CBDB-1
Column length (m) 50.30.25.25.60.
Carrier gas HeHeliumN2HeHe
Substrate      
Column diameter (mm) 0.250.250.50.250.25
Phase thickness (mum) 0.250.20 0.390.25
Tstart (C) 70.60.60.60.40.
Tend (C) 220.200.220.220.280.
Heat rate (K/min) 2.3.5.5.4.
Initial hold (min) 5.4. 5.5.
Final hold (min)   10.20. 
I 1079.1080.1081.1083.1080.
ReferencePateira, Nogueira, et al., 1999Prikhod'ko, Klyuev, et al., 1999Rao, Bhattacharya, et al., 1999Rustaiyan, Masoudi, et al., 1999Sefidkon, Dabiri, et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5OV-101SPB-5
Column length (m) 30.60.30.25.60.
Carrier gas HeHeHeNitrogenHe
Substrate      
Column diameter (mm) 0.250.250.250.200.32
Phase thickness (mum) 0.250.250.25 1.
Tstart (C) 40.50.60.60.40.
Tend (C) 220.220.240.220.200.
Heat rate (K/min) 4.4.3.4.3.
Initial hold (min) 5.  0.5.
Final hold (min)    0.2.
I 1087.1087.1090.1083.1097.
ReferenceSefidkon and Khajavi, 1999Sefidkon and Mirza, 1999Tellez, Canel, et al., 1999Tropnikova, Zenkevich, et al., 1999Viallon C., Verdier-Metz I., et al., 1999
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101DB-5MSSPB-5DB-5SE-30
Column length (m) 25.30.50.30.25.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.200.250.320.250.2
Phase thickness (mum)  0.250.250.25 
Tstart (C) 80.60.60.60.60.
Tend (C) 240.240.240.240.180.
Heat rate (K/min) 6.3.3.3.3.
Initial hold (min)     10.
Final hold (min)   20.  
I 1079.1085.1090.1082.1081.
ReferenceZenkevich, Kosman, et al., 1999Zoghbi, Andrade, et al., 1999Doneanu and Anitescu, 1998El-Sakhawy, El-Tantawy, et al., 1998Jantan, Ahmad, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5HP-101HP-1HP-5HP-1
Column length (m) 30.25.25.25.60.
Carrier gas HeHe HeHe
Substrate      
Column diameter (mm) 0.250.20.320.20.25
Phase thickness (mum) 0.250.2 0.330.25
Tstart (C) 60.70.35.70.50.
Tend (C) 240.200.250.290.280.
Heat rate (K/min) 3.3.4.3.4.
Initial hold (min)  2. 8.5.
Final hold (min)  10. 20. 
I 1087.1081.1077.1088.1077.
ReferenceMaia, Zohhbi, et al., 1998Milso, Mastelic, et al., 1998Ong and Acree, 1998Poiana, Sicari, et al., 1998Stashenko, Cervantes, et al., 1998
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101CP Sil 5 CBCP Sil 5 CBSPB-SulfurSPB-Sulfur
Column length (m) 25.25.25.30.30.
Carrier gas  N2HeHeHe
Substrate      
Column diameter (mm) 0.320.320.250.320.32
Phase thickness (mum)  0.250.254.4.
Tstart (C) 50.50.60.45.45.
Tend (C) 200.290.300.240.240.
Heat rate (K/min) 5.4.6.5.5.
Initial hold (min)    13.13.
Final hold (min)    5.5.
I 1082.1075.1075.1095.1096.
ReferenceZollo, Biyiti, et al., 1998Bos, Woerdenbag, et al., 1997Bos, Woerdenbag, et al., 1997, 2Mariaca, Berger, et al., 1997Mariaca, Berger, et al., 1997
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-1DB-5CBP-1HP-1
Column length (m) 30. 30.25.23.
Carrier gas He HeliumHeHe
Substrate      
Column diameter (mm) 0.25 0.250.220.32
Phase thickness (mum) 0.25 0.25 0.17
Tstart (C) 50.80.60.60.60.
Tend (C) 250.220.240.240.250.
Heat rate (K/min) 2.6.3.5.5.
Initial hold (min) 5.   3.
Final hold (min)     30.
I 1059.1064.1089.1072.1077.
ReferenceReverchon, Porta, et al., 1997Salgueiro, Vila, et al., 1997Tellez, Estell, et al., 1997Zygadlo, Ariza-Espinar, et al., 1997Ayedoun, Adeoti, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101BP-1BP-1BP-1
Column length (m) 50.50.25.25.25.
Carrier gas N2HeN2N2N2
Substrate      
Column diameter (mm) 0.250.250.500.500.50
Phase thickness (mum) 0.17    
Tstart (C) 50.50.60.60.60.
Tend (C) 220.250.220.220.220.
Heat rate (K/min) 5.2.5.5.5.
Initial hold (min)      
Final hold (min)      
I 1069.1077.1081.1082.1083.
ReferenceChacko, Jayalekshmy, et al., 1996Orav, Kailas, et al., 1996Rajeswara, Kaul, et al., 1996Rajeswara, Kaul, et al., 1996Rajeswara, Kaul, et al., 1996
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1HP-1SPB-1OV-101DB-1
Column length (m) 60.25.50.50.60.
Carrier gas HeHeliumHeHeHe
Substrate      
Column diameter (mm) 0.320.320.20.20.25
Phase thickness (mum) 0.500.250.330.50.25
Tstart (C) 50.60.40.70.70.
Tend (C) 250.220.200.180.270.
Heat rate (K/min) 8.4.3.1.2.5
Initial hold (min) 1.2.3. 5.
Final hold (min) 6.20.30.  
I 1072.1077.1084.1076.1080.
ReferenceSagrero-Nieves and Bartley, 1996Thanh, Dung, et al., 1996Wong and Lai, 1996Orav, Kuningas, et al., 1995Tirado, Stashenko, et al., 1995
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-1OV-1HP-5HP-101Methyl Silicone
Column length (m) 60.50. 50.50.
Carrier gas HeN2 H2N2
Substrate      
Column diameter (mm) 0.250.27 0.320.25
Phase thickness (mum) 0.250.2 0.30.17
Tstart (C) 70.80.40.65.80.
Tend (C) 270.240.210.300.200.
Heat rate (K/min) 2.53.2.2.2.
Initial hold (min) 5.  5. 
Final hold (min)      
I 1080.1081.1098.1076.1074.
ReferenceTirado, Stashenko, et al., 1995Ramanoelina, Viano, et al., 1994Collin, Deslauriers, et al., 1993Demarne and van der Walt, 1993Gopalakrishnan, Menon, et al., 1993
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase Methyl SiliconeCP Sil 5 CBMethyl SiliconeSE-54DB-1
Column length (m) 50.25.25.30.30.
Carrier gas N2  HydrogenN2
Substrate      
Column diameter (mm) 0.250.250.500.25 
Phase thickness (mum) 0.17  0.25 
Tstart (C) 80.60.60.60.80.
Tend (C) 200.280.220.250.220.
Heat rate (K/min) 3.5.5.2.4.
Initial hold (min)    5. 
Final hold (min)    2. 
I 1066.1082.1080.1087.1053.
ReferenceGopalakrishnan, Menon, et al., 1993Kaul, Singh, et al., 1993Mallavarapu, Ramesh, et al., 1993Kollmannsberger, Nitz, et al., 1992Velasco-Negueruela, Pérez Alonso, et al., 1991
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1OV-101OV-101BP-1SE-30
Column length (m) 25.50.50.50.40.
Carrier gas  N2N2H2He
Substrate      
Column diameter (mm) 0.330.250.250.300.50
Phase thickness (mum)     0.75
Tstart (C) 45.80.80.40.30.
Tend (C) 180.200.200.250.220.
Heat rate (K/min) 3.2.2.10.3.
Initial hold (min) 3.  1. 
Final hold (min)      
I 1080.1081.1084.1081.1077.
ReferenceWyllie, Brophy, et al., 1990Yang and Sugisawa, 1990Yang and Sugisawa, 1990Brophy, Davies, et al., 1989de Pooter, de Buyck, et al., 1989
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-101DB-1OV-1
Column length (m) 50.50.50.60.60.
Carrier gas N2N2N2HeHelium
Substrate      
Column diameter (mm) 0.250.250.250.3150.50
Phase thickness (mum)    0.251.2
Tstart (C) 80.80.80.50.40.
Tend (C) 200.200.200.250.220.
Heat rate (K/min) 2.2.2.4.2.
Initial hold (min)      
Final hold (min)      
I 1081.1081.1084.1077.1077.
ReferenceSugisawa, Yamamoto, et al., 1989Sugisawa, Yang, et al., 1989Sugisawa, Yang, et al., 1989Engel, Flath, et al., 1988Wahab, Aboutabl, et al., 1987
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase OV-101OV-101OV-1OV-1OV-101
Column length (m) 50.50.40. 30.
Carrier gas   HeHeHe
Substrate      
Column diameter (mm) 0.300.300.5 0.5
Phase thickness (mum)   0.75 0.8
Tstart (C) 40.40.30.40.40.
Tend (C) 230.230.220.220.220.
Heat rate (K/min) 3.53.53.2.2.
Initial hold (min) 5.5.   
Final hold (min)      
I 1078.1091.1077.1077.1077.
ReferenceNykanen, 1986Nykanen, 1986de Pooter, de Buyck, et al., 1986De Pooter, De Buyck, et al., 1986De Pooter and Schamp, 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillary
Active phase OV-101SE-30+IgepalSE-30+Igepal
Column length (m) 50.100.100.
Carrier gas He  
Substrate    
Column diameter (mm) 0.310.250.25
Phase thickness (mum)    
Tstart (C) 0.70.70.
Tend (C) 225.170.170.
Heat rate (K/min) 3.1.1.
Initial hold (min) 1.  
Final hold (min)    
I 1072.1082.1085.
Referencedel Rosario, de Lumen, et al., 1984Shibamoto and Jennings, 1977Shibamoto and Jennings, 1977
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

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Rahmi-Nasrabadi, Gholivand, et al., 2009
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Retta, Gattuso, et al., 2009
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Scrivanti, Anton, et al., 2009
Scrivanti, L.R.; Anton, A.M.; Zygadlo, J.A., Essential oil conposition of Bothriochloa Kuntze (Poaceae) from South America and their chemotaxonomy, Biochem. Systematics Ecol., 2009, 37, 3, 206-213, https://doi.org/10.1016/j.bse.2009.03.009 . [all data]

de Souza, Lopes, et al., 2009
de Souza, A.; Lopes, E.M.C.; da Silva, M.C.; Cordeiro, I.; Young, M.C.M.; Sobral, M.E.G.; Moreno, P.R.H., Chemical composition and acetylcholinesterase inhibitory activity of essential oils of Myrceugenia myrcioides (Chambess.) O. Berg and Eugenia riedeliana O. Berg, Myrtaceae, Braz. J. Pharmacognosy, 2009, 20, 2, 175-179. [all data]

Su, Wang, et al., 2009
Su, Y.; Wang, C.; Yinlong, G., Analysis of volatile compounds from Mentha hapioealyx Briq. by GC-MS based on accurate mass measurements and retention indices, Acta Chem. Sinica, 2009, 67, 6, 546-554. [all data]

Wannes, Mhamdi, et al., 2009
Wannes, W.A.; Mhamdi, B.; Marzouk, B., GC comparative analysis of least essential oils from two Myrtle varieties at different phenological stages, Chromatographia, 2009, 69, 1/2, 145-150, https://doi.org/10.1365/s10337-008-0818-9 . [all data]

Zaibunnisa, Norashikin, et al., 2009
Zaibunnisa, A.H.; Norashikin, S.; Mamot, S.; Osman, H., An experimental design approach for the extraction of volatile compounds from turmeric leaves (Curcuma domestica) using pressurised liquid extraction (PLE), LWT-Food Sci. Technol., 2009, 42, 1, 233-238, https://doi.org/10.1016/j.lwt.2008.03.015 . [all data]

Zhannan, Shiqiong, et al., 2009
Zhannan, Y.; Shiqiong, L.; Quancai, P.; Chao, Z.; Zhengwen, Y., GC-MS analysis of the essential oil of Coral Ginger (Zingiber corallinum Hance) rhizome obtained by supercritical fluid extraction and steam distillation extraction, Chromatographia, 2009, 69, 7/8, 785-790, https://doi.org/10.1365/s10337-009-0971-9 . [all data]

Zhao, Zeng, et al., 2009
Zhao, C.; Zeng, Y.; Wan, M.; Li, R.; Liang, Y.; Li, C.; Zeng, Z.; Chau, F.-T., Comparative analysis of essential oils from eight herbal medicines with pungent flavor and cool nature by GC-MS and chemometric resolution methods, J. Sep. Sci., 2009, 32, 4, 660-670, https://doi.org/10.1002/jssc.200800484 . [all data]

Aicha, Ines, et al., 2008
Aicha, N.; Ines, S.; Mohamed, B.S.; Ines, B.; Soumaya, K.; Kamel, G.; Mohamed, N.; Imed, C.; Mohamed, H.; Leila, C.-G., Chemical composition, mutagenic and antimutagenic activities of essential oils from (Tunisian) Artemisia campestris and Artemisia herba-alba, J. Ess. Oil Res., 2008, 20, 5, 471-477. [all data]

Ali, Wurster, et al., 2008
Ali, N.A.A.; Wurster, M.; Arnold, N.; Teichert, A.; Schmidt, J.; Lindequist, U.; Wessjohann, L., Chemical composition and biological activities of essential oils from the oleogum resins of three endemic soqotraen Boswellia species, Rec. Nat. Prod., 2008, 2, 1, 6-12. [all data]

Baziou, Couladis, et al., 2008
Baziou, P.; Couladis, M.; Petrakis, P.V.; Verykokidou, E.; Harvala, C., Composition and antioxidant activity of the essential oil of Hypericum perfoliatum from Greece, 2008, retrieved from http://www.amapseec.org/cmapseec.1/Papers/papp065.htm. [all data]

Flamini, Tebano, et al., 2008
Flamini, G.; Tebano, M.; Cioni, P.L., Composition of the essential oils from leafy parts of the shoots, flowers and fruits of Eryngium amethystinum from Amiata Mount (Tuscany, Italy), Food Chem., 2008, 107, 2, 671-674, https://doi.org/10.1016/j.foodchem.2007.08.064 . [all data]

Forero, Quijano, et al., 2008
Forero, M.D.; Quijano, C.E.; Pino, J.A., Volatile compounds of Chile pepper (Capsicum annuum L. var. glabriusculum) at two ripening stages, Flavour Fragr. J., 2008, 24, 1, 25-30, https://doi.org/10.1002/ffj.1913 . [all data]

Isidorov, Lech, et al., 2008
Isidorov, V.A.; Lech, P.; Zolciak, A.; Rusak, N.; Szczepaniak, L., Gas Chromatographic - nass spectrometric investigation of metabolites from the needles and roots of pine seedlings at early stages of pathogenic fungi Armillaria ostoyae attack, Trees, 2008, 22, 4, 531-542, https://doi.org/10.1007/s00468-008-0213-z . [all data]

Lo Presti, Sciarrone, et al., 2008
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Cicció, J.F.; Gómez-Laurito, J., Volatile constituents of the leaves of Siparuna thecaphora (Siparunaceae) from Turrialba, Costa Rica, Rev. Biol. Trop., 2002, 50, 3/4, 963-967. [all data]

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Koulman, A., Podophyllotoxin: a study of biosynthesis, evolution, function, and use of podophyllotoxin and related lignans, University Library Groningen, Nederlands, 1999, 188, retrieved from http://www.ub.rug.nl/eldoc/dis/science/a.koulman/. [all data]

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Notes

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