Cyclohexene, 1-methyl-4-(1-methylethylidene)-

Formula: C₁₀H₁₆
Molecular weight: 136.2340
IUPAC Standard InChI: InChI=1S/C10H16/c1-8(2)10-6-4-9(3)5-7-10/h4H,5-7H2,1-3H3
IUPAC Standard InChIKey: MOYAFQVGZZPNRA-UHFFFAOYSA-N
CAS Registry Number: 586-62-9
Chemical structure:
This structure is also available as a 2d Mol file or as a computed 3d SD file
The 3d structure may be viewed using Java or Javascript.
Species with the same structure:
- α-Terpinolene
- (Z)-β-Terpinolene
Other names: p-Mentha-1,4(8)-diene; Terpinolene; Terpinolen; UN 2541; α- Terpinolen; α-Terpinolene; 4-Isopropylidene-1-methyl-cyclohexene; p-Menth-1,4(8)-diene; 1-Methyl-4-(propan-2-ylidene)cyclohex-1-ene; 1-Methyl-4-(1-methylethylidene)-1-cyclohexene; 69073-38-7; 1-methyl-4-(1-methylethylidene)-cyclohexene (α-terpinolene); 1-Methyl-4-(1-methylethylidene)-cyclohexene; (E)-β-Terpinolene
Information on this page:
Other data available:
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- Gas Phase Kinetics Database
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Normal alkane RI, non-polar column, temperature ramp

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Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	RTX-1	RTX-1	Mega-5
Column length (m)	30.	60.	60.	60.	25.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.22	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	60.	60.	50.
T_end (C)	300.	250.	230.	230.	220.
Heat rate (K/min)	4.	3.	2.	2.	3.
Initial hold (min)	3.	1.			1.
Final hold (min)	15.	20.	5.	5.	5.
I	1090.	1089.	1082.	1082.	1088.
Reference	Bertuzzi, Tirillini, et al., 2013	Sardashti, Valizadeh, et al., 2013	Bendiabdellah, El Amine Dib, et al., 2012	Bendiabdellah, El Amine Dib, et al., 2012	Dell'Agli, Sanna, et al., 2012
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Polydimethyl siloxane with 5 % Ph	HP-5	HP-5	HP-5 MS	HP-1
Column length (m)	30.	25.	25.	30.	30.
Carrier gas	Helium	Hydrogen	Hydrogen	Helium	Helium
Substrate
Column diameter (mm)		0.32	0.32	0.25	0.25
Phase thickness (μm)		0.52	0.52	0.25	0.25
T_start (C)	80.	40.	40.	50.	60.
T_end (C)	200.	280.	280.	250.	240.
Heat rate (K/min)	5.	4.	4.	7.	3.
Initial hold (min)				1.
Final hold (min)	25.	10.	10.	5.
I	1080.	1084.	1084.	1089.	1087.
Reference	Priya, Prathapan, et al., 2012	Velickovic, Ristic, et al., 2012	Velickovic, Ristic, et al., 2012	Zouari, Ayadi, et al., 2012	Alizadeh, Khosh-Khui, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP-Sil 5 CB	VF-5 MS	VF-5 MS	SE-30 MS	CP-Sil 5 CB
Column length (m)	25.	60.	60.	30.	30.
Carrier gas	Hydrogen	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.25
Phase thickness (μm)	0.15	0.25	0.25	0.25	0.26
T_start (C)	50.	30.	30.	50.	45.
T_end (C)	230.	260.	260.	250.	280.
Heat rate (K/min)	3.	2.	2.	5.	3.
Initial hold (min)				5.
Final hold (min)		28.	28.	10.	22.
I	1086.	1086.	1087.	1089.	1080.
Reference	Esseien, Aboaba, et al., 2011	Leffingwell and Alford, 2011	Leffingwell and Alford, 2011	Menichini, Tundis, et al., 2011	Mothana, Hasson, et al., 2011
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5 MS	DB-5 MS	DB-5 MS	RTX-1	DB-5
Column length (m)	30.	25.	25.	60.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.30	0.30	0.22	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	50.	60.	60.
T_end (C)	290.	240.	240.	230.	280.
Heat rate (K/min)	5.	3.	3.	2.	3.
Initial hold (min)
Final hold (min)				30.
I	1087.	1085.	1085.	1082.	1084.
Reference	Boix, Victorio, et al., 2010	Chalchat, Figueredo, et al., 2010	Chalchat, Figueredo, et al., 2010	Dib, Djabou, et al., 2010	Georgiou, Koutsaviti, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	HP-5 MS	DB-5 MS	DB-1
Column length (m)	30.	30.	30.	60.	25.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	70.	40.	60.
T_end (C)	250.	240.	290.	250.	250.
Heat rate (K/min)	2.	3.	5.	5.	4.
Initial hold (min)		2.		15.	1.
Final hold (min)				15.	10.
I	1089.	1089.	1093.	1090.	1083.
Reference	Ho, Wang, et al., 2010	Kahriman, Tosun, et al., 2010	Lazarevic, Radulovic, et al., 2010	Mesa-Arango, Betancur-Galvis, et al., 2010	Mirjalili, Salehi, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5 MS	HP-5 MS	HP-5 MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Hydrogen
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	50.	100.	70.
T_end (C)	240.	220.	240.	220.	290.
Heat rate (K/min)	3.	5.	4.	2.	5.
Initial hold (min)	5.	10.	2.
Final hold (min)			10.
I	1086.	1090.	1088.	1084.	1094.
Reference	Monsef-Esfahani, Miri, et al., 2010	Ogunwande, Flamini, et al., 2010	Pino, Marquez, et al., 2010	Pripdeevech, Chumpolsri, et al., 2010	Radulovic, Dordevic, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SLB-5 MS	SLB-5 MS	DB-1-MS	CP Sil 5 CB	DB-5
Column length (m)	10.	10.	60.	25.	30.
Carrier gas	Helium	Helium	Helium		Helium
Substrate
Column diameter (mm)	0.10	0.10	0.25	0.25	0.25
Phase thickness (μm)	0.10	0.10	0.25	0.15	0.25
T_start (C)	50.	50.	30.	50.	80.
T_end (C)	250.	250.	200.	230.	240.
Heat rate (K/min)	10.	10.	2.	3.	3.
Initial hold (min)			4.
Final hold (min)			35.		2.
I	1086.	1086.	1077.	1087.	1090.
Reference	Scandinaro, Tranchida, et al., 2010	Scandinaro, Tranchida, et al., 2010	Takeoka, Hobbs, et al., 2010	Usman, Zubair, et al., 2010	Vahirua-Lechat, Mitermite, et al., 2010
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5MS	SE-54	DB-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	50.	60.	35.	60.
T_end (C)	250.	250.	260.	220.	250.
Heat rate (K/min)	10.	7.	2.	3.	2.
Initial hold (min)	1.	1.	5.		8.
Final hold (min)	3.	5.	999.	40.	15.
I	1089.	1093.	1086.	1088.	1091.
Reference	Yang, Zhang, et al., 2010	Zouari, Zouari, et al., 2010	Dayisoylu and Alma, 2009	El-Massry, El-Ghorab, et al., 2009	Farhat, Ginies, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	ZB-5	SPB-5	SPB-5	DB-5	DB-5
Column length (m)	30.	60.	30.	30.	30.
Carrier gas	Helium	Nitrogen	Nitrogen	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.35	0.53	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.50	0.25	0.25
T_start (C)	50.	60.	50.	50.	50.
T_end (C)	240.	230.	210.	250.	250.
Heat rate (K/min)	3.	4.	3.	5.	5.
Initial hold (min)			5.	2.
Final hold (min)	1.	40.	45.
I	1040.	1094.	1107.	1089.	1095.
Reference	Gardini, Beletti, et al., 2009	Gauvin-Bialecki and Marodon, 2009	Gilani, Shah, et al., 2009	Ho, Wang, et al., 2009	Koba, Catherine, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	HP-5	RTX-1	RTX-1
Column length (m)	30.	30.	25.	60.	60.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.20	0.22	0.22
Phase thickness (μm)	0.25	0.25	0.33	0.25	0.25
T_start (C)	50.	70.	60.	60.	60.
T_end (C)	280.	240.	240.	230.	230.
Heat rate (K/min)	5.	5.	3.	2.	2.
Initial hold (min)	2.
Final hold (min)	5.		7.	30.	30.
I	1088.	1082.	1083.	1079.	1082.
Reference	Lago, Favero, et al., 2009	Lawal and Oyedelji, 2009	Maridass, 2009	Museli, Pau, et al., 2009	Museli, Pau, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	5 % Phenyl methyl siloxane	DB-5	DB-5
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	Helium	Nitrogen	Helium	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	45.	40.	90.	40.	40.
T_end (C)	250.	250.	225.	230.	240.
Heat rate (K/min)	3.	3.	3.	2.	3.
Initial hold (min)	3.	1.			1.
Final hold (min)	5.	10.	3.
I	1088.	1082.	1087.	1090.	1063.
Reference	Porto, Decorti, et al., 2009	Rahmi-Nasrabadi, Gholivand, et al., 2009	Retta, Gattuso, et al., 2009	Scrivanti, Anton, et al., 2009	de Souza, Lopes, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5 MS	HP-5MS	HP-5 MS	HP-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium	Helium	Helium	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	50.	60.	40.	50.
T_end (C)	250.	240.	325.	240.	280.
Heat rate (K/min)	4.	5.	10.	4.	4.
Initial hold (min)	2.		6.	4.
Final hold (min)	2.		10.
I	1088.	1092.	1081.	1091.	1088.
Reference	Su, Wang, et al., 2009	Wannes, Mhamdi, et al., 2009	Zaibunnisa, Norashikin, et al., 2009	Zhannan, Shiqiong, et al., 2009	Zhao, Zeng, et al., 2009
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	HP-5 MS	HP-5	HP-5 MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	Helium	Helium		N2	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	50.	70.	60.	60.	50.
T_end (C)	280.	220.	280.	220.	230.
Heat rate (K/min)	9.	3.	3.	5.	4.
Initial hold (min)	3.	1.		10.	4.
Final hold (min)	3.				10.
I	1088.	1082.	1087.	1089.	1086.
Reference	Aicha, Ines, et al., 2008	Ali, Wurster, et al., 2008	Baziou, Couladis, et al., 2008	Flamini, Tebano, et al., 2008	Forero, Quijano, et al., 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	SLB-5 MS	ZB-1	DB-5	BPX-5
Column length (m)	30.	30.	30.	60.	7.5
Carrier gas	Helium	Helium	Nitrogen	Nitrogen	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.10
Phase thickness (μm)	0.25	0.25	0.25	0.25	10.
T_start (C)	50.	50.	45.	60.	60.
T_end (C)	300.	250.	230.	250.	240.
Heat rate (K/min)	3.	3.	3.	5.	3.
Initial hold (min)		2.
Final hold (min)	30.	10.		10.
I	1085.	1086.	1072.	1093.	1092.
Reference	Isidorov, Lech, et al., 2008	Lo Presti, Sciarrone, et al., 2008	Mierendorff, Stahl-Biskup, et al., 2008	Mosayebi, Amin, et al., 2008	Shellie, 2008
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-5	HP-5	HP-5	HP-5 MS	DB-5
Column length (m)	20.	25.	30.	30.	50.
Carrier gas	Helium	Helium	Helium	Helium	Nitrogen
Substrate
Column diameter (mm)	0.18	0.25	0.25	0.25	0.20
Phase thickness (μm)	0.20	0.25	0.32	0.25	0.32
T_start (C)	50.	60.	60.	50.	60.
T_end (C)	280.	240.	250.	230.	220.
Heat rate (K/min)	4.	4.	5.	3.	5.
Initial hold (min)	1.	2.	30.	10.	3.
Final hold (min)				10.	5.
I	1094.	1089.	1090.	1088.	1087.
Reference	Skalicka-Wozniak, Los, et al., 2008	Verdian-rizi, 2008	Yassa and Akhani, 2008	Adams, Beauchamp, et al., 2007	Amiri, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	CP Sil 5 CB	HP-5MS	DB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.26	0.25
Phase thickness (μm)		0.25	0.25	0.25	0.25
T_start (C)	70.	60.	60.	60.	60.
T_end (C)	240.	300.	280.	240.	280.
Heat rate (K/min)	5.	4.	3.	3.	3.
Initial hold (min)
Final hold (min)
I	1089.	1076.	1086.	1083.	1088.
Reference	Asekun, Olusegun, et al., 2007	Baran, von Reuss, et al., 2007	Basta, Tzakou, et al., 2007	Bos, Woerdenbag, et al., 2007	Bozin B., Mlmica-Dukic N., et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	DB-5	DB-1	Col-Elite 5MS	DBP-5
Column length (m)	30.	30.	60.	30.	25.
Carrier gas	N2	Helium	Nitrogen	He	Helium
Substrate
Column diameter (mm)	0.25	0.26	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.22
T_start (C)	50.	60.	60.	30.	40.
T_end (C)	240.	290.	250.	246.	250.
Heat rate (K/min)	5.	3.	4.	3.	3.
Initial hold (min)	1.		1.		1.
Final hold (min)	4.		10.		10.
I	1088.	1083.	1083.	1097.	1060.
Reference	Cheraif, Ben Jannet, et al., 2007	Elfami, Bos, et al., 2007	Ghasempour, Shirinpour, et al., 2007	Gudaityte and Venskutonis R.P., 2007	Heravi and Sereshti, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RTX-5 MS	DB-5	SE-30	HP-5	ZB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	45.	60.	40.	40.	60.
T_end (C)	210.	300.	250.	250.	220.
Heat rate (K/min)	3.	3.	5.	5.	4.
Initial hold (min)			5.	5.	5.
Final hold (min)			10.	10.	20.
I	1091.	1080.	1089.	1086.	1097.
Reference	Hudaib and Aburjai, 2007	Limberger, Scopel, et al., 2007	Loizzo, Tundis, et al., 2007	Loizzo, Tundis, et al., 2007	Mohottalage, Tabacchi, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5	Methyl Silicone	DB-1
Column length (m)	30.	30.	25.	50.	50.
Carrier gas	Helium	Helium	H2	Helium	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.33		0.25
T_start (C)	50.	60.	60.	50.	95.
T_end (C)	260.	300.	240.	240.	240.
Heat rate (K/min)	2.5	3.	3.	3.	4.
Initial hold (min)	1.
Final hold (min)	20.
I	1073.	1061.	1090.	1088.	1085.
Reference	Monser-Esfahani, Karamkhani, et al., 2007	Moreno, Lima, et al., 2007	Oliveira, Leitão, et al., 2007	Ozcan and Chalchat, 2007	Pala-Paul, Brophy, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	BPX-5	BPX-5	DB-1	DB-1
Column length (m)	30.	50.	50.	60.	60.
Carrier gas	He	He	He	Nitrogen
Substrate
Column diameter (mm)	0.2	0.22	0.22	0.25	0.25
Phase thickness (μm)	0.2	1.	1.	0.25	0.25
T_start (C)	70.	50.	50.	60.	60.
T_end (C)	220.	300.	300.	250.	250.
Heat rate (K/min)	3.	4.	4.	4.	5.
Initial hold (min)		1.	1.	1.
Final hold (min)	15.	10.	10.	10.
I	1077.	1111.	1105.	1083.	1082.
Reference	Pinto, Salgueiro, et al., 2007	Rali, Wossa, et al., 2007	Rali, Wossa, et al., 2007	Reza, Ebrahim, et al., 2007	Salehi, Asghari, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	DBP-5	DB-5	DB-5
Column length (m)	60.	30.	25.	30.	30.
Carrier gas	He	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.22	0.25	0.25
T_start (C)	60.	50.	40.	40.	40.
T_end (C)	250.	240.	250.	210.	250.
Heat rate (K/min)	5.	4.	3.	2.	2.
Initial hold (min)			1.
Final hold (min)			10.	33.	33.
I	1081.	1086.	1060.	1098.	1097.
Reference	Salehi, Fakhari, et al., 2007	Sefidkon, Abbasi, et al., 2007	Sereshti and Samadi, 2007	Sylvestre, Longtin, et al., 2007	Sylvestre, Pichette, et al., 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Elite-5MS	HP-5 MS	HP-5MS	HP-5MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	Helium	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.5	0.25	0.25	0.25	0.32
T_start (C)	40.	60.	60.	40.	60.
T_end (C)	280.	280.	280.	250.	250.
Heat rate (K/min)	4.	3.	3.	3.	5.
Initial hold (min)	5.			5.	30.
Final hold (min)	10.			10.
I	1085.	1092.	1052.	1083.	1090.
Reference	Tava, Pecetti, et al., 2007	Tsokou, Georgopoulos, et al., 2007	Tzakou, Bazos, et al., 2007	Vichi, Riu-Aumatell, et al., 2007	Yassa and Akhani, 2007
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	CP Sil 5 CB	ZB-5	AT-5
Column length (m)	30.	30.	25.	30.	60.
Carrier gas	N2	N2	He		He
Substrate
Column diameter (mm)	0.25	0.25		0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	50.	50.	80.	40.	60.
T_end (C)	280.	280.	270.	300.	200.
Heat rate (K/min)	9.	9.	10.	2.	4.
Initial hold (min)	3.	3.
Final hold (min)	3.	3.			20.
I	1080.	1084.	1082.	1087.	1088.
Reference	Abdelwahed, Hayder, et al., 2006	Abdelwahed, Hayder, et al., 2006	Ayoub, Al-Azizi, et al., 2006	Biondi, Sari, et al., 2006	Borges, Rojas, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	HP-1	HP-1	SPB-1	DB-1
Column length (m)	50.	50.	50.	30.	60.
Carrier gas	He	He	He	Helium	Nitrogen
Substrate
Column diameter (mm)	0.22	0.2	0.2	0.20	0.25
Phase thickness (μm)	0.25	0.5	0.33	0.20
T_start (C)	60.	60.	60.	70.	40.
T_end (C)	220.	250.	250.	220.	200.
Heat rate (K/min)	2.	2.	2.	3.	2.
Initial hold (min)			4.		1.
Final hold (min)	20.	120.	30.	15.	9.
I	1076.	1079.	1079.	1076.	1077.
Reference	Boti, Muselli, et al., 2006	Castel, Fernandez, et al., 2006	Castel, Fernandez, et al., 2006	Cavaleiro, Pinto, et al., 2006	Chen, Sheu, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	DB-5	HP-5MS	DB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He			Helium
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.26
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	70.	60.	60.	60.	60.
T_end (C)	230.	246.	230.	280.	290.
Heat rate (K/min)	2.	3.	3.	4.	3.
Initial hold (min)	2.
Final hold (min)	20.		15.
I	1086.	1087.	1077.	1091.	1083.
Reference	Choi, 2006	Coronel, Cerda-Garcia-Rojas, et al., 2006	Damjanovic, Skala, et al., 2006	Ebrahim Sajjadi and Mehregan, 2006	Elfami, Komar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	BP-1	HP-5	HP-1	DB-5
Column length (m)	50.	50.	30.	50.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.22	0.22	0.25	0.2	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.25
T_start (C)	60.	60.	50.	60.	50.
T_end (C)	220.	220.	300.	250.	250.
Heat rate (K/min)	2.	2.	5.	2.	3.
Initial hold (min)			5.
Final hold (min)	20.	20.	5.	40.	10.
I	1078.	1078.	1085.	1079.	1084.
Reference	Fanciullino, Tomi, et al., 2006	Fanciullino, Tomi, et al., 2006	Figuérédo, Cabassu, et al., 2006	Filippi, Lanfranchi, et al., 2006	Havlik, Kokoska, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	HP-5	DB-5	DB-1	CP Sil 8 CB
Column length (m)	30.	30.	30.	60.	30.
Carrier gas		He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	60.	70.	40.
T_end (C)	220.	240.	260.	230.	250.
Heat rate (K/min)	3.	4.	3.	2.	3.
Initial hold (min)				2.	5.
Final hold (min)	3.			20.	20.
I	1089.	1088.	1089.	1080.	1087.
Reference	Hymete, Rohloff, et al., 2006	Ibañez and Usubillaga, 2006	Javidnia, Miri, et al., 2006	Lan Phi N.T., Nishiyama C., et al., 2006	Li, Lee, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	CP Sil 5 CB	HP-5 MS	HP-5	5 % Phenyl methyl siloxane
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	N2	Nitrogen	N2	Helium
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.52	0.25
T_start (C)	50.	50.	50.	50.	60.
T_end (C)	300.	200.	280.	280.	280.
Heat rate (K/min)	4.	5.	5.	5.	3.
Initial hold (min)
Final hold (min)			5.	5.	30.
I	1082.	1077.	1088.	1088.	1054.
Reference	Lis and Milczarek, 2006	Martin, Joseph, et al., 2006	Marzouk, Mansour, et al., 2006	Marzouk, Neffati, et al., 2006	Marongiu, Piras, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BP-1	DB-5	DB-5	NB-30
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	Helium	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.3	0.25	0.25	0.2
Phase thickness (μm)	0.25		0.25	0.25	0.25
T_start (C)	50.	70.	60.	60.	50.
T_end (C)	250.	220.	220.	220.	250.
Heat rate (K/min)	3.	4.	4.	4.	2.
Initial hold (min)	5.	2.		5.
Final hold (min)		10.
I	1086.	1081.	1091.	1092.	1080.
Reference	Mirza, Navaei, et al., 2006	Moody, Gundidza, et al., 2006	Morteza-Semnani, Akbarzadeh, et al., 2006	Morteza-Semnani K., Saeedi M., et al., 2006	Orav, Raal, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-1	HP-5	DB-5
Column length (m)	25.	30.	50.	30.	30.
Carrier gas	N2	He	N2	He	Hydrogen
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.15	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	95.	60.	70.
T_end (C)	200.	280.	240.	220.	280.
Heat rate (K/min)	4.	5.	4.	5.	4.
Initial hold (min)	3.	0.5		10.	4.
Final hold (min)		2.
I	1085.	1088.	1086.	1089.	1089.
Reference	Ouamba, Ouabonzi, et al., 2006	Ozel, Gogus, et al., 2006	Pala-Paul J., Perez-Alonso M.J., et al., 2006	Pintore G., Chessa M., et al., 2006	Pino, Marbot, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5MS	DB-5	DB-5	ZB-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	50.	60.	60.	40.
T_end (C)	280.	250.	200.	260.	300.
Heat rate (K/min)	3.	10.	2.	5.	2.
Initial hold (min)		5.
Final hold (min)			60.
I	1054.	1088.	1088.	1088.	1087.
Reference	Pitarokili, Tzakou, et al., 2006	Robinson, 2006	Rout, Naik, et al., 2006	Sabulal, Dan, et al., 2006	Sari M., Biondi D.M., et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	FSOT-RSL-200	DB-5	DB-1	HP-5
Column length (m)	60.	30.	30.	60.	25.
Carrier gas		Hydrogen	He	He	N2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.2
Phase thickness (μm)	0.25	0.25	0.25		0.33
T_start (C)	70.	40.	40.	40.	30.
T_end (C)	230.	280.	240.	250.	280.
Heat rate (K/min)	2.	6.	4.	4.	3.
Initial hold (min)	2.	5.
Final hold (min)	20.	5.
I	1079.	1087.	1087.	1078.	1091.
Reference	Sawamura, Onishi, et al., 2006	Schmidt, Jirovetz, et al., 2006	Sefidkon and Jamzad, 2006	Sefidkon, Jamzad, et al., 2006	Shafi, Jose, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	SPB-5	DB-5	DB-1	HP-5
Column length (m)	25.	60.	30.	50.	25.
Carrier gas		He	N2	N2	H2
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.32
Phase thickness (μm)		1.	0.25	0.25	0.52
T_start (C)	50.	40.	60.	90.	50.
T_end (C)	230.	230.	240.	240.	280.
Heat rate (K/min)	3.	3.	4.	4.	2.5
Initial hold (min)		5.			5.
Final hold (min)		2.
I	1089.	1102.	1089.	1068.	1087.
Reference	Tesso, Kubeczka, et al., 2006	Tornambe, Cornu, et al., 2006	Trilles, Bombarda, et al., 2006	Velasco-Negueruela, Pérez-Alonso, et al., 2006	Wang, Kong, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	SPB-1	SPB-1	DB-5	DB-5
Column length (m)	30.	50.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.25
T_start (C)	60.	50.	50.	40.	40.
T_end (C)	250.	220.	250.	250.	250.
Heat rate (K/min)	10.	4.	4.	4.	4.
Initial hold (min)	2.	1.	1.
Final hold (min)	10.	10.	10.
I	1094.	1077.	1072.	1062.	1082.
Reference	Wang, Yang, et al., 2006	Wong, Lim, et al., 2006	Wong, Sivasothy, et al., 2006	Yadegarinia, Gachkar, et al., 2006	Yadegarinia, Gachkar, et al., 2006
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	DB-5	Methyl Silicone	SPB-5
Column length (m)	30.	30.	50.	60.	60.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25	0.249	0.3	0.3	0.32
Phase thickness (μm)	0.25	0.25	0.25		1.
T_start (C)	60.	60.	60.	50.	40.
T_end (C)	280.	290.	240.	240.	230.
Heat rate (K/min)	3.	3.	2.	3.	3.
Initial hold (min)					5.
Final hold (min)
I	1083.	1085.	1095.	1088.	1098.
Reference	Basta, Tzakou, et al., 2005	Bos, Stojanova, et al., 2005	Chagonda and Chalchat, 2005	Chalchat and Özcan, 2005	Cornu, Kondjoyan, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-1	HP-5	HP-5MS	CP Sil 5 CB
Column length (m)	60.	50.	30.	25.	30.
Carrier gas	He		He	He	N2
Substrate
Column diameter (mm)	0.25	0.2	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	250.	250.	300.	250.	250.
Heat rate (K/min)	5.	2.	5.	3.	5.
Initial hold (min)		60.	5.	3.
Final hold (min)			5.	10.	10.
I	1079.	1077.	1085.	1089.	1086.
Reference	Fakhari, Salehi, et al., 2005	Fernandez, Lizzani-Cuvelier, et al., 2005	Figuérédo, Cabassu, et al., 2005	Ghasemi Y., Faridi P., et al., 2005	Jassbi, Mehrdad, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	DB-1	HP-5	CP Sil 5 CB	CP Sil 5 CB
Column length (m)	30.	30.	60.	25.	25.
Carrier gas		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.15	0.15
T_start (C)	40.	50.	30.	50.	50.
T_end (C)	280.	265.	260.	230.	230.
Heat rate (K/min)	6.	2.5	2.	3.	3.
Initial hold (min)	2.	1.	2.
Final hold (min)	10.	30.	28.
I	1089.	1072.	1086.5	1083.	1083.
Reference	Jirovetz, Buchbauer, et al., 2005	Khalighi-Sigaroodi, Hadijiakhoondi, et al., 2005	Leffingwell and Alford, 2005	Ogunwande, Olawore, et al., 2005	Olawore, Ogunwande, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	RTX-5 MS	HP-5MS	SPB-5	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.32
T_start (C)	70.	50.	60.	60.	60.
T_end (C)	240.	280.	280.	250.	250.
Heat rate (K/min)	5.	8.	3.	4.	5.
Initial hold (min)		2.		2.	3.
Final hold (min)		2.		20.
I	1089.	1091.	1089.	1088.	1091.
Reference	Oyedeji, Yani, et al., 2005	Pellati, Benvenuti, et al., 2005	Petrakis, Roussis, et al., 2005	Pino, Marbot, et al., 2005	Pourmortazavi, Ghadiri, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	CP Sil 5 CB	HP-5	HP-5MS	HP-5MS
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25		0.25	0.25
T_start (C)	40.	40.	60.	60.	60.
T_end (C)	220.	220.	240.	280.	275.
Heat rate (K/min)	4.	4.	5.	4.	4.
Initial hold (min)	1.	1.
Final hold (min)
I	1089.	1089.	1088.	1087.	1087.
Reference	Rohloff and Bones, 2005	Rohloff and Bones, 2005	Saeidnia, Gohari, et al., 2005	Sajjadi S.E. and Eskandari B., 2005	Sajjadi and Ghannadi, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	DB-5	DB-1	DB-5	HP-5MS
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25		0.25
T_start (C)	60.	60.	60.	40.	60.
T_end (C)	280.	220.	250.	240.	280.
Heat rate (K/min)	4.	3.	5.	4.	3.
Initial hold (min)		4.			5.
Final hold (min)			10.
I	1085.	1086.	1064.	1087.	1092.
Reference	Sajjadi, 2005	Salehi, Sefidkon, et al., 2005	Salehi, Sonboli, et al., 2005	Sefidkon and Jamzad, 2005	Setzer, Noletto, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	PE-5	DB-5	HP-5MS	RTX-1	RTX-1
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	60.	60.
T_end (C)	230.	230.	280.	250.	25.
Heat rate (K/min)	5.	3.	3.	5.	5.
Initial hold (min)	2.
Final hold (min)	4.	20.		10.	10.
I	1078.	1089.	1089.	1083.	1082.
Reference	Singh, Raina, et al., 2005	Skoula and Grayer, 2005	Slavkovska, Couladis, et al., 2005	Sonboli A., Fakhari A.R., et al., 2005	Sonboli, Salehi, et al., 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5	HP-5MS	HP-5MS	DB-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He		He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	50.	60.	60.
T_end (C)	250.	210.	240.	280.	280.
Heat rate (K/min)	5.	2.	3.	3.	3.
Initial hold (min)		2.	3.
Final hold (min)	10.	33.
I	1081.	1099.	1095.	1052.	1058.
Reference	Sonboli, Salehi, et al., 2005, 2	Stevanovic, Garneau, et al., 2005	Tepe B., Sokmen M., et al., 2005	Tzakou, Bazos, et al., 2005	Tzakou and Constantinidis, 2005
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	HP-5MS	SPB-1	BP-1
Column length (m)	50.	50.	30.	50.	50.
Carrier gas	N2			He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.2	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.33	0.25
T_start (C)	90.	60.	40.	50.	60.
T_end (C)	240.	240.	220.	220.	220.
Heat rate (K/min)	4.	3.	3.	4.	2.
Initial hold (min)			5.	3.
Final hold (min)			10.	30.	20.
I	1068.	1066.	1083.	1076.	1078.
Reference	Velasco-Negueruela, Pérez-Alonso, et al., 2005	Velasco-Negueruela, Pérez-Alonso, et al., 2005, 2	Vichi, Riu-Aumatell, et al., 2005	Wong, Lee, et al., 2005	Blanc, Muselli, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-52	SPB-5	DB-1	DB-5	ZB-5
Column length (m)	25.	60.	25.	25.	60.
Carrier gas	N2	He		Nitrogen	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.25	0.25
Phase thickness (μm)	0.15	1.	0.25	0.25	0.25
T_start (C)	45.	60.	60.	60.	40.
T_end (C)	200.	200.	180.	240.	260.
Heat rate (K/min)	3.	4.	3.	3.	6.
Initial hold (min)	5.		10.		4.6
Final hold (min)	30.	30.	10.		1.
I	1079.	1092.	1089.	1088.	1099.
Reference	Cakir, Kordali, et al., 2004	Gauvin, Ravaomanarivo, et al., 2004	bin Jantan, Ayop, et al., 2004	JAvidnia, Mojab, et al., 2004	Jürgens and Dötterl, 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	SE-54	HP-5MS	RTX-1	DB-5
Column length (m)	60.	30.	30.	30.	30.
Carrier gas	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	60.	40.
T_end (C)	280.	260.	230.	300.	210.
Heat rate (K/min)	4.	2.	5.	4.	2.
Initial hold (min)	4.	5.	2.		2.
Final hold (min)			10.		33.
I	1086.	1086.	1088.	1080.	1098.
Reference	Kalvandi, Sefidkon, et al., 2004	Kilic, Hafizoglu, et al., 2004	Li and Jiang, 2004	Lis, Boczek, et al., 2004	Lopez Arze, Collin, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-5MS	NB-30	NB-30	DB-1
Column length (m)	30.	30.	50.	50.	50.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.2	0.22
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	70.
T_end (C)	280.	280.	250.	250.	220.
Heat rate (K/min)	3.	3.	2.	2.	4.
Initial hold (min)
Final hold (min)	30.	30.
I	1051.	1050.	1080.	1080.	1082.
Reference	Marongiu, Piras, et al., 2004	Marongiu, Porcedda, et al., 2004	Orav, Stulova, et al., 2004	Orav, Stulova, et al., 2004	Palá-Paúl, García-Jiménez, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	NB-30	NB-30	DB-5	Methyl Silicone
Column length (m)	50.	50.	50.	30.	60.
Carrier gas	N2	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.2	0.20	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	95.	50.	50.	35.	60.
T_end (C)	240.	250.	250.	220.	200.
Heat rate (K/min)	4.	2.	2.	2.5	4.
Initial hold (min)					1.
Final hold (min)				6.	20.
I	1074.	1080.	1080.	1089.	1080.
Reference	Palá-Paúl, Velasco-Negueruela, et al., 2004	Raal, Arak, et al., 2004	Raal, Paaver, et al., 2004	Rohloff, Mordal, et al., 2004	Rojas, Usubillaga, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5 MS	HP-5MS	HP-5MS	DB-1	DB-1
Column length (m)	30.	30.	30.	60.	60.
Carrier gas	Helium	He	He		Nitrogen
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	60.	70.	70.
T_end (C)	200.	280.	280.	230.	230.
Heat rate (K/min)	4.	4.	4.	2.	2.
Initial hold (min)	1.			2.	2.
Final hold (min)	20.			20.
I	1080.	1084.	1090.	1086.	1086.
Reference	Royas, Usubillaga, et al., 2004	Sadeghpour, Asghari, et al., 2004	Sajjadi and Shahpiri, 2004	Sawamura, Son, et al., 2004	Sawamura, Sou, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-1	DB-5	DB-5	CP Sil 5 CB
Column length (m)	30.	30.	30.	30.	20.
Carrier gas		He		He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.33	0.25	0.25	0.25
T_start (C)	50.	40.	60.	60.	100.
T_end (C)	250.	260.	300.	240.	270.
Heat rate (K/min)	3.	2.	3.	3.	8.
Initial hold (min)	5.	5.			2.
Final hold (min)		20.
I	1088.	1061.	1079.	1087.	1074.
Reference	Sefidkon, Jamzad, et al., 2004	Senatore, Napolitano, et al., 2004	Suyenaga, Apel, et al., 2004	Tellez, Khan, et al., 2004	Thappa, Bakshi, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	BPX-5	CP Sil 8 CB	CP Sil 8 CB	DB-5
Column length (m)	30.	25.	30.	30.	30.
Carrier gas	He	He	He		He
Substrate
Column diameter (mm)	0.25	0.22	0.25	0.32	0.249
Phase thickness (μm)	0.25	1.	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	300.	250.	200.	200.	300.
Heat rate (K/min)	3.	3.	10.	5.	3.
Initial hold (min)		5.	3.	5.
Final hold (min)		10.	2.
I	1089.	1096.	1086.	1088.	1086.
Reference	Tirillini, Pellegrino, et al., 2004	Vilaseca, Guy, et al., 2004	Wang and Guo-Y. -L., 2004	Wang, Guo, et al., 2004	Woerdenbag, Windono, et al., 2004
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5MS	HP-5	DB-1	HP-5MS	RTX-5Sil
Column length (m)	30.	30.	60.	30.	30.
Carrier gas	He	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	60.	70.	60.	70.
T_end (C)	275.	220.	230.	280.	200.
Heat rate (K/min)	4.	5.	2.	3.	4.
Initial hold (min)		10.	2.
Final hold (min)			20.		10.
I	1088.	1082.	1086.	1086.	1086.
Reference	Afsharypuor and Jahromy, 2003	Bertoli, Menichini, et al., 2003	Choi, 2003	Couladis, Özcan, et al., 2003	Dudai, Larkov, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-5	DB-5	HP-5MS	HP-1
Column length (m)	60.	60.	60.	30.	30.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.32	0.25	0.25
Phase thickness (μm)				0.25	0.25
T_start (C)	50.	50.	50.	60.	70.
T_end (C)	220.	220.	200.	220.	200.
Heat rate (K/min)	3.	3.	3.	5.	10.
Initial hold (min)				20.
Final hold (min)				20.
I	1090.	1090.	1090.	1094.	1079.
Reference	Edris and Farrag, 2003	Edris and Farrag, 2003	Edris, Shalaby, et al., 2003	Feizbaksh, Saber Tehrani, et al., 2003	Fekam Boyom, Amvam Zollo, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-5MS	HP-5	HP-5MS	RSL-200
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	N2	He	He	He	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	40.
T_end (C)	200.	280.	275.	275.	280.
Heat rate (K/min)	5.	4.	4.	4.	6.
Initial hold (min)					5.
Final hold (min)					5.
I	1068.	1088.	1086.	1087.	1079.
Reference	Fekam Boyom, Ngouana, et al., 2003	Ghasemi, Asghari, et al., 2003	Ghannadi and Zolfaghari, 2003	Hajhashemi, Ghannadi, et al., 2003	Jirovetz, Buchbauer, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	SE-30	CP Sil 5 CB	DB-5MS	DB-5
Column length (m)	30.	12.	25.	30.	30.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.22	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.3	0.25	0.25	0.25
T_start (C)	40.	70.	35.	60.	60.
T_end (C)	280.	220.	280.	240.	280.
Heat rate (K/min)	6.	3.	5.	3.	3.
Initial hold (min)	5.		2.5
Final hold (min)	5.				30.
I	1084.	1076.	1077.	1087.	1070.
Reference	Jirovetz, Buchbauer, et al., 2003, 2	Kambouche and El-Abed, 2003	Kanjilal, Kotoky, et al., 2003	Maia, Taveira, et al., 2003	Marongiu, Porcedda, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	ZB-1	DB-1	HP-5	OV-101
Column length (m)	50.	30.	60.	30.	50.
Carrier gas	He	N2	He	Helium	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.32	0.2
Phase thickness (μm)	0.25	0.25	0.25		0.5
T_start (C)	50.	45.	50.	70.	50.
T_end (C)	220.	230.	270.	210.	250.
Heat rate (K/min)	3.	3.	4.	2.	2.
Initial hold (min)	2.
Final hold (min)				60.
I	1088.	1072.	1087.	1086.	1077.
Reference	Masotti, Juteau, et al., 2003	Mierendorff, Stahl-Biskup, et al., 2003	Mirza, Nik, et al., 2003	Mookdasanit, Tamura, et al., 2003	Orav, Kailas, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	DB-1	DB-5	HP-5	DB-1
Column length (m)	25.	50.	30.	30.	60.
Carrier gas	H2	N2	H2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.15	0.25	0.25	0.25	0.25
T_start (C)	50.	95.	60.	60.	50.
T_end (C)	230.	240.	280.	280.	250.
Heat rate (K/min)	3.	4.	4.	3.	4.
Initial hold (min)			10.
Final hold (min)			40.
I	1081.	1081.	1088.	1072.	1076.
Reference	Oyedeji, Ekundayo, et al., 2003	Perez-Alonso, Velasco-Negueruela, et al., 2003	Pino, Marbot, et al., 2003	Pitarokili, Tzakou, et al., 2003	Pourmortazavi, Sefidkon, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-5	DB-1	DB-5	HP-5
Column length (m)	30.	30.	60.	30.	60.
Carrier gas	N2	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	60.	40.
T_end (C)	230.	280.	280.	240.	250.
Heat rate (K/min)	2.	4.	4.	3.	5.
Initial hold (min)					15.
Final hold (min)
I	1082.	1089.	1084.	1087.	1088.
Reference	Rotman, Ahumada, et al., 2003	Sajjadi and Mehregan, 2003	Shahmir, Ahmadi, et al., 2003	da Silva, Luz, et al., 2003	Stashenko, Jaramillo, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	Cross-Linked Methylsilicone	HP-5	HP-5	HP-5
Column length (m)	50.	25.	25.	25.	25.
Carrier gas	N2	He	H2	H2	Helium
Substrate
Column diameter (mm)	0.25	0.2	0.32	0.32	0.32
Phase thickness (μm)	0.25	0.33	0.53	0.53	0.53
T_start (C)	90.	70.	40.	40.	40.
T_end (C)	240.	250.	280.	280.	280.
Heat rate (K/min)	4.	4.	4.	4.	4.
Initial hold (min)
Final hold (min)
I	1069.	1068.	1088.	1089.	1084.
Reference	Velasco-Negueruela, Pérez-Alonso, et al., 2003	Velasco-Negueruela, Pérez-Alonso, et al., 2003, 2	Velickovic, Randjelovic, et al., 2003	Velickovic, Randjelovic, et al., 2003	Velickovic, Ristic, et al., 2003
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	HP-5	HP-5	DB-5	DB-5	DB-5
Column length (m)	25.	30.	30.	25.	30.
Carrier gas	Helium	He	He	N2	He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.249
Phase thickness (μm)	0.53	0.32	0.25	0.25	0.25
T_start (C)	40.	60.	60.	50.	60.
T_end (C)	280.	250.	240.	250.	300.
Heat rate (K/min)	4.	5.	3.	4.	3.
Initial hold (min)		30.
Final hold (min)				10.	5.
I	1089.	1097.	1085.	1089.	1087.
Reference	Velickovic, Ristic, et al., 2003	Yassa, Akhani, et al., 2003	Zoghbi, Andrade, et al., 2003	Zrira, Elamrani, et al., 2003	Bos, Koulman, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-1	5 % Phenyl methyl siloxane	DB-5MS	HP-5
Column length (m)	30.	30.	30.	30.	30.
Carrier gas	He	He	He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	70.	75.	60.	50.
T_end (C)	280.	220.	200.	280.	250.
Heat rate (K/min)	3.	3.	3.	3.	4.
Initial hold (min)			4.		5.
Final hold (min)	30.	15.	8.
I	1070.	1077.	1089.	1079.	1089.
Reference	Caredda, Marongiu, et al., 2002	Cavaleiro, Salgueiro, et al., 2002	Cicció and Gómez-Laurito, 2002	Congiu, Falconieri, et al., 2002	Farah, Fechtal. M., et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	PTE-5	SE-30	RSL-200
Column length (m)	30.	30.	60.	50.	30.
Carrier gas	He	H2	H2	He	H2
Substrate
Column diameter (mm)	0.25	0.32	0.32	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.30	0.25	0.25
T_start (C)	60.	40.	60.	70.	40.
T_end (C)	240.	245.	285.	240.	280.
Heat rate (K/min)	3.	3.	4.3	4.	6.
Initial hold (min)		20.			5.
Final hold (min)					5.
I	1089.	1067.	1088.	1086.	1078.
Reference	Flamini, Ertugrul, et al., 2002	Gancel, Ollé, et al., 2002	Gudzic, Djokovic, et al., 2002	Iñigo, Palá-Paúl, et al., 2002	Jirovetz, Buchbauer, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	CP Sil 8 CB	DB-1	DB-5	DB-5
Column length (m)	30.	30.	25.	30.	30.
Carrier gas	H2	He	He	He	He
Substrate
Column diameter (mm)	0.32	0.25	0.23	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.20	0.25	0.25
T_start (C)	50.	50.	50.	60.	35.
T_end (C)	280.	220.	200.	240.	280.
Heat rate (K/min)	6.	3.	3.	3.	3.
Initial hold (min)	5.	2.	3.		2.
Final hold (min)	5.		30.		15.
I	1074.	1087.	1089.	1090.	1089.
Reference	Jirovetz, Ngassoum, et al., 2002	Juteau, Masotti, et al., 2002	Khallouki, Younos, et al., 2002	Kobaisy, Tellez, et al., 2002	Krauze-Baranowska, Mardarowicz, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	OV-101	DB-5	DB-5MS	OV-101
Column length (m)	30.	25.	30.	30.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.32	0.25	0.25	0.32
Phase thickness (μm)	0.25		0.25	0.25
T_start (C)	35.	50.	60.	60.	50.
T_end (C)	280.	200.	240.	240.	200.
Heat rate (K/min)	4.	5.	3.	3.	5.
Initial hold (min)	2.
Final hold (min)	15.
I	1090.	1082.	1086.	1089.	1080.
Reference	Krauze-Baranowska, Mardarowicz, et al., 2002, 2	Kuiate, Bessière, et al., 2002	Maia, da Silva, et al., 2002	Maia, Zoghbi, et al., 2002	Menut, Bessière, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	CP Sil 5 CB	HP-5	OV-101	ZEBRON-5	DB-1
Column length (m)	25.	30.	50.	6.	50.
Carrier gas	He		He	He	N2
Substrate
Column diameter (mm)	0.25	0.25	0.2	0.25	0.25
Phase thickness (μm)	0.39	0.25	0.5	0.25	0.25
T_start (C)	60.	60.	50.	40.	80.
T_end (C)	220.	240.	250.	200.	225.
Heat rate (K/min)	5.	3.	2.	3.	4.
Initial hold (min)				5.
Final hold (min)				15.
I	1080.	1091.	1078.	1053.	1068.
Reference	Mojab, Rustaiyan, et al., 2002	Novak, Langbehn, et al., 2002	Orav, Kailas, et al., 2002	Öztürk, Akay, et al., 2002	Palá-Paúl, Pérez-Alonso, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-5	DB-1	DB-1	DB-1	HP-5
Column length (m)	30.	60.	50.	50.	30.
Carrier gas	Helium	He	N2	N2	H2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	60.	40.	95.	60.	40.
T_end (C)	250.	280.	240.	240.	280.
Heat rate (K/min)	4.	4.	4.	3.	4.
Initial hold (min)	2.	5.
Final hold (min)	20.
I	1088.	1077.	1068.	1066.	1088.
Reference	Pino, Marbot, et al., 2002	Sefidkon, 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002	Velasco-Negueruela, Pérez-Alonso, et al., 2002, 2	Velickovic, Randjelovic, et al., 2002
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-5MS	DB-5	DB-5MS	SPB-5
Column length (m)	60.	30.	30.	30.	60.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.32
Phase thickness (μm)	0.25	0.25	0.25	0.25
T_start (C)	50.	60.	60.	60.	40.
T_end (C)	250.	270.	240.	240.	220.
Heat rate (K/min)	4.	3.	3.	3.	3.
Initial hold (min)	5.				5.
Final hold (min)					15.
I	1077.	1088.	1089.	1075.	1089.
Reference	Yamini, Sefidkon, et al., 2002	Zoghbi, Andrade, et al., 2002	Zoghbi, Andrade, et al., 2002, 2	Cherchi, Deidda, et al., 2001	Cornu, Carnat, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	DB-1	HP-5	OV-1	HP-5
Column length (m)	60.	60.	30.	30.	30.
Carrier gas	He	He	N2	H2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.3	0.25
T_start (C)	40.	40.	60.	50.	60.
T_end (C)	280.	280.	220.	250.	220.
Heat rate (K/min)	4.	4.	5.	3.	5.
Initial hold (min)	5.	5.	10.	1.	10.
Final hold (min)				20.
I	1070.	1078.	1089.	1076.	1089.
Reference	Dabiri and Sefidkon, 2001	Dabiri and Sefidkon, 2001	Flamini, Cioni, et al., 2001	Gallori, Bilia, et al., 2001	Gallori, Flamini, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	RTX-1	SPB-5	BP-1	CBP-1
Column length (m)	30.	30.	60.	50.	25.
Carrier gas	H2	N2	Helium	He	Nitrogen
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.22	0.25
Phase thickness (μm)	0.25	0.25	0.25	0.25	0.25
T_start (C)	40.	60.	50.	60.	50.
T_end (C)	280.	300.	240.	230.	210.
Heat rate (K/min)	6.	4.	3.	2.	3.
Initial hold (min)	5.		3.		2.
Final hold (min)	5.		10.	35.
I	1079.	1083.	1097.	1078.	1076.
Reference	Jirovetz L., Buchbauer G., et al., 2001	Kalemba, Marschall, et al., 2001	Kim and Lee, 2001	Lota, de Rocca Serra, et al., 2001	Ly, Yamauchi, et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5MS	DB-1	RSL-200	OV-101	OV-101
Column length (m)	30.	60.	30.	50.	50.
Carrier gas	He	He	H2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.32	0.2	0.2
Phase thickness (μm)	0.25	0.25	0.25	0.5
T_start (C)	60.	50.	40.	50.	50.
T_end (C)	240.	270.	280.	250.	250.
Heat rate (K/min)	3.	4.	6.	2.	2.
Initial hold (min)			5.
Final hold (min)	30.		5.
I	1088.	1076.	1077.	1073.	1076.
Reference	Marongiu, Porcedda, et al., 2001	Mirza, Ahmadi, et al., 2001	Ngassoum, Jirovetz, et al., 2001	Orav, Kailas, et al., 2001	Orav and Kann, 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-1	DB-5	DB-5	DB-5
Column length (m)	50.	30.	60.	30.	30.
Carrier gas	He	N2	He	H2	He
Substrate
Column diameter (mm)	0.2	0.25	0.25	0.25	0.25
Phase thickness (μm)		0.25		0.25	0.25
T_start (C)	50.	80.	50.	60.	60.
T_end (C)	250.	225.	250.	285.	240.
Heat rate (K/min)	2.	4.	3.	3.	3.
Initial hold (min)			5.
Final hold (min)
I	1076.	1045.	1090.	1086.	1089.
Reference	Orav and Kann, 2001	Palá-Paúl, Pérez-Alonso, et al., 2001	Rousis, Papadogianni, et al., 2001	Santos-Gomes and Fernandes-Ferreira, 2001	Tellez M., Estell R., et al., 2001
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SPB-1	OV-101	OV-101	CP Sil 5 CB	CP Sil 5 CB
Column length (m)	30.	50.	50.	25.	25.
Carrier gas	He	N2	N2		He
Substrate
Column diameter (mm)	0.32	0.25	0.25	0.25	0.25
Phase thickness (μm)	0.25			0.15	0.4
T_start (C)	50.	80.	80.	50.	60.
T_end (C)	250.	200.	200.	230.	260.
Heat rate (K/min)	2.	2.	2.	3.	5.
Initial hold (min)					40.
Final hold (min)
I	1083.	1082.	1082.	1078.	1074.
Reference	Vijayanand, Rao, et al., 2001	Yang, 2001	Yang, 2001, 2	Asekun and Ekundayo, 2000	Baser, Özek, et al., 2000
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	RSL-200	DB-1	DB-5	BP-1	HP-5
Column length (m)	60.	25.	30.	25.	30.
Carrier gas	H2	Nitrogen	N2	N2	He
Substrate
Column diameter (mm)	0.32	0.50	0.22	0.33	0.25
Phase thickness (μm)	0.25	0.25	0.25	1.0	0.25
T_start (C)	40.	60.	70.	60.	60.
T_end (C)	250.	220.	230.	275.	275.
Heat rate (K/min)	6.	5.	4.	4.	4.
Initial hold (min)			2.
Final hold (min)			20.
I	1077.	1081.	1092.	1087.	1087.
Reference	Jirovetz, Puschmann, et al., 2000	Mallavarapu, Rao, et al., 2000	Mitiku, Sawamura, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000	Mohagheghzadeh, Shams-Ardakani, et al., 2000, 2
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-101	DB-5	Methyl Silicone	SPB-1
Column length (m)	30.	50.	30.	60.	50.
Carrier gas	He	Nitrogen	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.25	0.2
Phase thickness (μm)	0.25		0.25	0.25	0.33
T_start (C)	40.	40.	60.	40.	60.
T_end (C)	260.	200.	240.	220.	260.
Heat rate (K/min)	2.	2.	3.	5.	4.
Initial hold (min)	5.	10.		10.
Final hold (min)	2.
I	1077.	1082.	1090.	1080.40	1080.
Reference	Senatore, Napolitano, et al., 2000	Tamura, Boonbumrung, et al., 2000	Tellez, Dayan, et al., 2000	Baraldi, Rapparini, et al., 1999	Choo, Wong, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	SE-30	RTX-1	DB-1	OV-101	CBP-1
Column length (m)	30.	30.	25.	25.	25.
Carrier gas	N2	N2	He		He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.32	0.3
Phase thickness (μm)	0.25	0.25	0.25
T_start (C)	60.	60.	50.	50.	60.
T_end (C)	220.	300.	290.	200.	240.
Heat rate (K/min)	4.	4.	4.	5.	4.
Initial hold (min)	10.
Final hold (min)
I	1075.	1082.	1087.	1082.	1082.
Reference	Jassbi, Ahmad, et al., 1999	Kalemba, 1999	Koulman, 1999	Kuiate, Zollo, et al., 1999	Labuckas, Zygadlo, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	OV-1	OV-1	OV-101	CP Sil 5 CB
Column length (m)	30.	25.		50.	25.
Carrier gas		H2		Helium	He
Substrate
Column diameter (mm)	0.32	0.25		0.20	0.25
Phase thickness (μm)	1.	0.25		0.50
T_start (C)	40.	40.	50.	30.	50.
T_end (C)	200.	220.	160.	100.	230.
Heat rate (K/min)	3.	3.	2.	1.	3.
Initial hold (min)	5.	5.		6.
Final hold (min)		5.
I	1090.	1075.	1080.	1075.	1077.
Reference	Meynier, Novelli, et al., 1999	Oberhofer, Nikiforov, et al., 1999	Orav, Kailas, et al., 1999	Orav, Kailas, et al., 1999, 2	Oyedeji, Olawore, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	SE-30	BP-1	CP Sil 5 CB	DB-1
Column length (m)	50.	30.	25.	25.	60.
Carrier gas	He	Helium	N2	He	He
Substrate
Column diameter (mm)	0.25	0.25	0.5	0.25	0.25
Phase thickness (μm)	0.25	0.20		0.39	0.25
T_start (C)	70.	60.	60.	60.	40.
T_end (C)	220.	200.	220.	220.	280.
Heat rate (K/min)	2.	3.	5.	5.	4.
Initial hold (min)	5.	4.		5.	5.
Final hold (min)			10.	20.
I	1079.	1080.	1081.	1083.	1080.
Reference	Pateira, Nogueira, et al., 1999	Prikhod'ko, Klyuev, et al., 1999	Rao, Bhattacharya, et al., 1999	Rustaiyan, Masoudi, et al., 1999	Sefidkon, Dabiri, et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	OV-101	SPB-5
Column length (m)	30.	60.	30.	25.	60.
Carrier gas	He	He	He	Nitrogen	He
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.20	0.32
Phase thickness (μm)	0.25	0.25	0.25		1.
T_start (C)	40.	50.	60.	60.	40.
T_end (C)	220.	220.	240.	220.	200.
Heat rate (K/min)	4.	4.	3.	4.	3.
Initial hold (min)	5.			0.	5.
Final hold (min)				0.	2.
I	1087.	1087.	1090.	1083.	1097.
Reference	Sefidkon and Khajavi, 1999	Sefidkon and Mirza, 1999	Tellez, Canel, et al., 1999	Tropnikova, Zenkevich, et al., 1999	Viallon C., Verdier-Metz I., et al., 1999
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	DB-5MS	SPB-5	DB-5	SE-30
Column length (m)	25.	30.	50.	30.	25.
Carrier gas	He	He	He	He	He
Substrate
Column diameter (mm)	0.20	0.25	0.32	0.25	0.2
Phase thickness (μm)		0.25	0.25	0.25
T_start (C)	80.	60.	60.	60.	60.
T_end (C)	240.	240.	240.	240.	180.
Heat rate (K/min)	6.	3.	3.	3.	3.
Initial hold (min)					10.
Final hold (min)			20.
I	1079.	1085.	1090.	1082.	1081.
Reference	Zenkevich, Kosman, et al., 1999	Zoghbi, Andrade, et al., 1999	Doneanu and Anitescu, 1998	El-Sakhawy, El-Tantawy, et al., 1998	Jantan, Ahmad, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	HP-101	HP-1	HP-5	HP-1
Column length (m)	30.	25.	25.	25.	60.
Carrier gas	He	He		He	He
Substrate
Column diameter (mm)	0.25	0.2	0.32	0.2	0.25
Phase thickness (μm)	0.25	0.2		0.33	0.25
T_start (C)	60.	70.	35.	70.	50.
T_end (C)	240.	200.	250.	290.	280.
Heat rate (K/min)	3.	3.	4.	3.	4.
Initial hold (min)		2.		8.	5.
Final hold (min)		10.		20.
I	1087.	1081.	1077.	1088.	1077.
Reference	Maia, Zohhbi, et al., 1998	Milso, Mastelic, et al., 1998	Ong and Acree, 1998	Poiana, Sicari, et al., 1998	Stashenko, Cervantes, et al., 1998
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	CP Sil 5 CB	CP Sil 5 CB	SPB-Sulfur	SPB-Sulfur
Column length (m)	25.	25.	25.	30.	30.
Carrier gas		N2	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.25	0.32	0.32
Phase thickness (μm)		0.25	0.25	4.	4.
T_start (C)	50.	50.	60.	45.	45.
T_end (C)	200.	290.	300.	240.	240.
Heat rate (K/min)	5.	4.	6.	5.	5.
Initial hold (min)				13.	13.
Final hold (min)				5.	5.
I	1082.	1075.	1075.	1095.	1096.
Reference	Zollo, Biyiti, et al., 1998	Bos, Woerdenbag, et al., 1997	Bos, Woerdenbag, et al., 1997, 2	Mariaca, Berger, et al., 1997	Mariaca, Berger, et al., 1997
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-5	DB-1	DB-5	CBP-1	HP-1
Column length (m)	30.		30.	25.	23.
Carrier gas	He		Helium	He	He
Substrate
Column diameter (mm)	0.25		0.25	0.22	0.32
Phase thickness (μm)	0.25		0.25		0.17
T_start (C)	50.	80.	60.	60.	60.
T_end (C)	250.	220.	240.	240.	250.
Heat rate (K/min)	2.	6.	3.	5.	5.
Initial hold (min)	5.				3.
Final hold (min)					30.
I	1059.	1064.	1089.	1072.	1077.
Reference	Reverchon, Porta, et al., 1997	Salgueiro, Vila, et al., 1997	Tellez, Estell, et al., 1997	Zygadlo, Ariza-Espinar, et al., 1997	Ayedoun, Adeoti, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	BP-1	BP-1	BP-1
Column length (m)	50.	50.	25.	25.	25.
Carrier gas	N2	He	N2	N2	N2
Substrate
Column diameter (mm)	0.25	0.25	0.50	0.50	0.50
Phase thickness (μm)	0.17
T_start (C)	50.	50.	60.	60.	60.
T_end (C)	220.	250.	220.	220.	220.
Heat rate (K/min)	5.	2.	5.	5.	5.
Initial hold (min)
Final hold (min)
I	1069.	1077.	1081.	1082.	1083.
Reference	Chacko, Jayalekshmy, et al., 1996	Orav, Kailas, et al., 1996	Rajeswara, Kaul, et al., 1996	Rajeswara, Kaul, et al., 1996	Rajeswara, Kaul, et al., 1996
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	HP-1	SPB-1	OV-101	DB-1
Column length (m)	60.	25.	50.	50.	60.
Carrier gas	He	Helium	He	He	He
Substrate
Column diameter (mm)	0.32	0.32	0.2	0.2	0.25
Phase thickness (μm)	0.50	0.25	0.33	0.5	0.25
T_start (C)	50.	60.	40.	70.	70.
T_end (C)	250.	220.	200.	180.	270.
Heat rate (K/min)	8.	4.	3.	1.	2.5
Initial hold (min)	1.	2.	3.		5.
Final hold (min)	6.	20.	30.
I	1072.	1077.	1084.	1076.	1080.
Reference	Sagrero-Nieves and Bartley, 1996	Thanh, Dung, et al., 1996	Wong and Lai, 1996	Orav, Kuningas, et al., 1995	Tirado, Stashenko, et al., 1995
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	DB-1	OV-1	HP-5	HP-101	Methyl Silicone
Column length (m)	60.	50.		50.	50.
Carrier gas	He	N2		H2	N2
Substrate
Column diameter (mm)	0.25	0.27		0.32	0.25
Phase thickness (μm)	0.25	0.2		0.3	0.17
T_start (C)	70.	80.	40.	65.	80.
T_end (C)	270.	240.	210.	300.	200.
Heat rate (K/min)	2.5	3.	2.	2.	2.
Initial hold (min)	5.			5.
Final hold (min)
I	1080.	1081.	1098.	1076.	1074.
Reference	Tirado, Stashenko, et al., 1995	Ramanoelina, Viano, et al., 1994	Collin, Deslauriers, et al., 1993	Demarne and van der Walt, 1993	Gopalakrishnan, Menon, et al., 1993
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	Methyl Silicone	CP Sil 5 CB	Methyl Silicone	SE-54	DB-1
Column length (m)	50.	25.	25.	30.	30.
Carrier gas	N2			Hydrogen	N2
Substrate
Column diameter (mm)	0.25	0.25	0.50	0.25
Phase thickness (μm)	0.17			0.25
T_start (C)	80.	60.	60.	60.	80.
T_end (C)	200.	280.	220.	250.	220.
Heat rate (K/min)	3.	5.	5.	2.	4.
Initial hold (min)				5.
Final hold (min)				2.
I	1066.	1082.	1080.	1087.	1053.
Reference	Gopalakrishnan, Menon, et al., 1993	Kaul, Singh, et al., 1993	Mallavarapu, Ramesh, et al., 1993	Kollmannsberger, Nitz, et al., 1992	Velasco-Negueruela, Pérez Alonso, et al., 1991
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	BP-1	OV-101	OV-101	BP-1	SE-30
Column length (m)	25.	50.	50.	50.	40.
Carrier gas		N2	N2	H2	He
Substrate
Column diameter (mm)	0.33	0.25	0.25	0.30	0.50
Phase thickness (μm)					0.75
T_start (C)	45.	80.	80.	40.	30.
T_end (C)	180.	200.	200.	250.	220.
Heat rate (K/min)	3.	2.	2.	10.	3.
Initial hold (min)	3.			1.
Final hold (min)
I	1080.	1081.	1084.	1081.	1077.
Reference	Wyllie, Brophy, et al., 1990	Yang and Sugisawa, 1990	Yang and Sugisawa, 1990	Brophy, Davies, et al., 1989	de Pooter, de Buyck, et al., 1989
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	OV-101	DB-1	OV-1
Column length (m)	50.	50.	50.	60.	60.
Carrier gas	N2	N2	N2	He	Helium
Substrate
Column diameter (mm)	0.25	0.25	0.25	0.315	0.50
Phase thickness (μm)				0.25	1.2
T_start (C)	80.	80.	80.	50.	40.
T_end (C)	200.	200.	200.	250.	220.
Heat rate (K/min)	2.	2.	2.	4.	2.
Initial hold (min)
Final hold (min)
I	1081.	1081.	1084.	1077.	1077.
Reference	Sugisawa, Yamamoto, et al., 1989	Sugisawa, Yang, et al., 1989	Sugisawa, Yang, et al., 1989	Engel, Flath, et al., 1988	Wahab, Aboutabl, et al., 1987
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary	Capillary	Capillary
Active phase	OV-101	OV-101	OV-1	OV-1	OV-101
Column length (m)	50.	50.	40.		30.
Carrier gas			He	He	He
Substrate
Column diameter (mm)	0.30	0.30	0.5		0.5
Phase thickness (μm)			0.75		0.8
T_start (C)	40.	40.	30.	40.	40.
T_end (C)	230.	230.	220.	220.	220.
Heat rate (K/min)	3.5	3.5	3.	2.	2.
Initial hold (min)	5.	5.
Final hold (min)
I	1078.	1091.	1077.	1077.	1077.
Reference	Nykanen, 1986	Nykanen, 1986	de Pooter, de Buyck, et al., 1986	De Pooter, De Buyck, et al., 1986	De Pooter and Schamp, 1986
Comment	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI	MSDC-RI

Column type	Capillary	Capillary	Capillary
Active phase	OV-101	SE-30+Igepal	SE-30+Igepal
Column length (m)	50.	100.	100.
Carrier gas	He
Substrate
Column diameter (mm)	0.31	0.25	0.25
Phase thickness (μm)
T_start (C)	0.	70.	70.
T_end (C)	225.	170.	170.
Heat rate (K/min)	3.	1.	1.
Initial hold (min)	1.
Final hold (min)
I	1072.	1082.	1085.
Reference	del Rosario, de Lumen, et al., 1984	Shibamoto and Jennings, 1977	Shibamoto and Jennings, 1977
Comment	MSDC-RI	MSDC-RI	MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, Notes

Bertuzzi, Tirillini, et al., 2013
Bertuzzi, G.; Tirillini, B.; Angelini, P.; Venanzoni, R., Antioxidative action of Citrus limonum essential oil on scin, Eur. J. Medicinal Plants, 2013, 3, 1, 1-9, https://doi.org/10.9734/EJMP/2013/1987 . [all data]

Sardashti, Valizadeh, et al., 2013
Sardashti, A.R.; Valizadeh, J.; Adhami, Y., Variations in the essential oil composition of Peroskia abrotonolides of different growth stage in Baluchestan, Middle-East J. Sci. Res., 2013, 13, 6, 781-784. [all data]

Bendiabdellah, El Amine Dib, et al., 2012
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Gopalakrishnan, M.; Menon, N.; Padmakumari, K.P.; Jayalekshmy, A.; Narayanan, C.S., GC Analysis and Odor Profiles of Four New Indian Genotypes of Piper nigrum L., J. Essent. Oil Res., 1993, 5, 3, 247-253, https://doi.org/10.1080/10412905.1993.9698217 . [all data]

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Notes

Go To: Top, Normal alkane RI, non-polar column, temperature ramp, References

Symbols used in this document:

T_end Final temperature

T_start Initial temperature
Data from NIST Standard Reference Database 69: NIST Chemistry WebBook
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