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Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SLB-5 MSSLB-5MSPolymethylsiloxane, (PMS-20000)Polymethylsiloxane, (PMS-20000)CP Sil 5 CB
Column length (m) 30.10.12.12.10.
Carrier gas HeliumHeliumHeHe 
Substrate      
Column diameter (mm) 0.250.180.200.200.53
Phase thickness (mum) 0.250.180.330.335.2
Program not specifiednot specifiednot specifiednot specified100 0C (2 min) 20 0C/min -> 180 0C 7.5 0C/min -> 280 0C (6 min)
I 1841.1837.1760.1771.1820.
ReferenceMondello, 2012Risticevic, Carasek, et al., 2008Gambaro, Saligari, et al., 1997Gambaro, Saligari, et al., 1997Bogusz, Bialka, et al., 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase CP Sil 5 CBBP-1BP-1OV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.OV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.
Column length (m) 10.12.12.50.50.
Carrier gas  HeHeHydrogenHydrogen
Substrate      
Column diameter (mm) 0.530.220.220.320.32
Phase thickness (mum) 5.20.250.25  
Program not specified120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)not specifiednot specifiednot specified
I 1810.1775.1810.1776.1777.
ReferenceBogusz, Bialka, et al., 1986Stowell and Wilson, 1985Stowell and Wilson, 1985Waggott and Davies, 1984Waggott and Davies, 1984
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type OtherPackedPacked
Active phase Methyl SiliconeOV-101OV-101
Column length (m)  2.2.
Carrier gas  NitrogenNitrogen
Substrate  Chromosorb G (100-120 mesh)Chromosorb G (100-120 mesh)
Column diameter (mm)    
Phase thickness (mum)    
Program not specifiednot specifiednot specified
I 1810.1801.1810.
ReferenceArdrey and Moffat, 1981Dubsky, Hána, et al., 1978Dubsky, Hána, et al., 1978
Comment MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Mondello, 2012
Mondello, L., HS-SPME-GCxGC-MS analysis of Yerba Mate (Ilex paraguariensis) in Shimadzu GC-GC application compendium of comprehensive 2D GC, Vol. 1-5, Shimadzu Corp., 2012, 1-29. [all data]

Risticevic, Carasek, et al., 2008
Risticevic, S.; Carasek, E.; Pawliszyn, J., Headspace solid-phase microextraction-gas chromatographic-time-of-flight mass spectrometric methodology for geographical origin verification of coffee, Anal. Chim. Acta, 2008, 617, 1-2, 72-84, https://doi.org/10.1016/j.aca.2008.04.009 . [all data]

Gambaro, Saligari, et al., 1997
Gambaro, V.; Saligari, E.; Froldi, R.; Bianchi, L., Analysis of street drugs by means of HRGC, Bollettino Chimico Farmaceutica, 1997, 36, 4, 359-367. [all data]

Bogusz, Bialka, et al., 1986
Bogusz, M.; Bialka, J.; Gierz, J.; Klys, M., Use of short, wide-bore capillary columns in GC toxicological screening, J. Anal. Toxicol., 1986, 10, 4, 135-138, https://doi.org/10.1093/jat/10.4.135 . [all data]

Stowell and Wilson, 1985
Stowell, A.; Wilson, L., Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]

Waggott and Davies, 1984
Waggott, A.; Davies, I.W., Identification of organic pollutants using linear temperature programmed retention indices (LTPRIs) - Part II, 1984, retrieved from http://dwi.defra.gov.uk/research/completed-research/reports/dwi0383.pdf. [all data]

Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C., Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase, J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1 . [all data]

Dubsky, Hána, et al., 1978
Dubsky, H.; Hána, K.; Komárková, M.; Rittich, B., Pouzití kovatsovych indexu pri toxikologickych analysách, Chem. Listy, 1978, 72, 980-984. [all data]


Notes

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