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Meperidine


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase BP-1BP-1BP-1BP-1BP-1
Column length (m) 12.12.12.12.12.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.220.220.220.220.22
Phase thickness (mum) 0.250.250.250.250.25
Program 120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)
I 1731.1731.1733.1734.1733.
ReferenceStowell and Wilson, 1985Stowell and Wilson, 1985Stowell and Wilson, 1985Stowell and Wilson, 1985Stowell and Wilson, 1985
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryPackedOther
Active phase BP-1OV-1, SE-30, Methyl silicone, SP-2100, OV-101, DB-1, etc.CP Sil 5 CBSE-30Methyl Silicone
Column length (m) 12.50.25.  
Carrier gas HeHydrogenHelium  
Substrate      
Column diameter (mm) 0.220.320.32  
Phase thickness (mum) 0.25 0.48  
Program not specifiednot specified60 0C (2.5 min) 30 0C/min -> 190 0C 7 0C/min -> 295 9C (7 min)not specifiednot specified
I 1740.1720.1736.1765.1751.
ReferenceStowell and Wilson, 1985Waggott and Davies, 1984Bogusz, Wijsbeek, et al., 1983Bogusz, Wijsbeek, et al., 1983Ardrey and Moffat, 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type Other
Active phase Methyl Silicone
Column length (m)  
Carrier gas  
Substrate  
Column diameter (mm)  
Phase thickness (mum)  
Program not specified
I 1759.
ReferenceArdrey and Moffat, 1981
Comment MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Stowell and Wilson, 1985
Stowell, A.; Wilson, L., Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]

Waggott and Davies, 1984
Waggott, A.; Davies, I.W., Identification of organic pollutants using linear temperature programmed retention indices (LTPRIs) - Part II, 1984, retrieved from http://dwi.defra.gov.uk/research/completed-research/reports/dwi0383.pdf. [all data]

Bogusz, Wijsbeek, et al., 1983
Bogusz, M.; Wijsbeek, J.; Franke, J.P.; de Zeeuw, R.A., Applicability of capillary gas chromatography to systematic toxicological analysis: occurence of concentration-dependent retention behavior, J. Analyt. Toxicol., 1983, 7, 4, 188-192, https://doi.org/10.1093/jat/7.4.188 . [all data]

Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C., Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase, J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1 . [all data]


Notes

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