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Morphine


Normal alkane RI, non-polar column, custom temperature program

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryOther
Active phase CP Sil 5 CBCP Sil 5 CBBP-1BP-1Methyl Silicone
Column length (m) 10.10.12.12. 
Carrier gas   HeHe 
Substrate      
Column diameter (mm) 0.530.530.220.22 
Phase thickness (mum) 5.25.20.250.25 
Program 100 0C (2 min) 20 0C/min -> 180 0C 7.5 0C/min -> 280 0C (6 min)not specified120 0X 8 0C/min -> 270 0C 25 0C/min -> 300 0C (5 min)not specifiednot specified
I 2440.2454.2399.2435.2390.
ReferenceBogusz, Bialka, et al., 1986Bogusz, Bialka, et al., 1986Stowell and Wilson, 1985Stowell and Wilson, 1985Ardrey and Moffat, 1981
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type OtherOther
Active phase Methyl SiliconeMethyl Silicone
Column length (m)   
Carrier gas   
Substrate   
Column diameter (mm)   
Phase thickness (mum)   
Program not specifiednot specified
I 2400.2454.
ReferenceArdrey and Moffat, 1981Ardrey and Moffat, 1981
Comment MSDC-RI MSDC-RI

References

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Bogusz, Bialka, et al., 1986
Bogusz, M.; Bialka, J.; Gierz, J.; Klys, M., Use of short, wide-bore capillary columns in GC toxicological screening, J. Anal. Toxicol., 1986, 10, 4, 135-138, https://doi.org/10.1093/jat/10.4.135 . [all data]

Stowell and Wilson, 1985
Stowell, A.; Wilson, L., Use of retention indices in drug screening by capillary gas chromatography, Rep. # CD 2362, Department of Scientific and Industrial Reseach, Chemistry Division, Lower Hutt, NZ, 1985, 32. [all data]

Ardrey and Moffat, 1981
Ardrey, R.E.; Moffat, A.C., Gas-liquid chromatographic retention indices of 1318 substances of toxicological interest on SE-30 or OV-1 stationary phase, J. Chromatogr., 1981, 220, 3, 195-252, https://doi.org/10.1016/S0021-9673(00)81925-1 . [all data]


Notes

Go To: Top, Normal alkane RI, non-polar column, custom temperature program, References