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Tetrahydrocannabinol


Gas Chromatography

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Kovats' RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedOV-1250.2490.Berninger and Möller, 1977 

Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
CapillaryDB-12471.Perrigo, Peel, et al., 198515. m/0.32 mm/0.25 «mu»m, He, 8. K/min, 280. C @ 5. min; Tstart: 120. C

Normal alkane RI, non-polar column, isothermal

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Column type Active phase Temperature (C) I Reference Comment
PackedOV-1180.2419.Gizella, Szabolcs, et al., 1995N2, Chromosorb WHP; Column length: 2.6 m
PackedSE-30200.2452.Lebbe, Lafarge, et al., 1972Nitrogen, Chromosorb (80-100 mesh); Column length: 1.2 m

Normal alkane RI, non-polar column, temperature ramp

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Column type Active phase I Reference Comment
PackedOV-12460.Marozzi, Gambaro, et al., 1982Gas Chrom P, 5. K/min; Column length: 2. m; Tstart: 150. C; Tend: 300. C
PackedSE-302475.Marozzi, Gambaro, et al., 1982Gas Chrom P, 5. K/min; Column length: 2. m; Tstart: 150. C; Tend: 300. C

References

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Berninger and Möller, 1977
Berninger, H.; Möller, M.R., Retentionsindices zur gaschromatographischen Identifizierung von Arzneimitteln, Arch. Toxicol., 1977, 37, 4, 295-305, https://doi.org/10.1007/BF00330821 . [all data]

Perrigo, Peel, et al., 1985
Perrigo, B.J.; Peel, H.W.; Ballantyne, D.J., Use of Dual-Column Fused-Silica Capillary Gas Chromatography in Combination with Detector Response Factors for Analytical Toxicology., J. Chromatogr., 1985, 341, 81-88, https://doi.org/10.1016/S0378-4347(00)84011-6 . [all data]

Gizella, Szabolcs, et al., 1995
Gizella, P.; Szabolcs, N.; Peep, V.; György, O.P.T., Kannabinoidok gázkromatográfiás vizsgálata tandem oszlopokon, Acta Pharm. Hung., 1995, 65, 63-67. [all data]

Lebbe, Lafarge, et al., 1972
Lebbe, J.; Lafarge, J.-P.; Laplace, M., Utilization of gas chromatography in toxicological investigations. I. Characterization of Cannabis sativa, Annales des falsifications et de l'expertise chimique, 1972, 65, 705, 410-417. [all data]

Marozzi, Gambaro, et al., 1982
Marozzi, E.; Gambaro, V.; Saligari, E.; Mariani, R.; Lodi, F., Use of the retention index in gas chromatographic studies of drugs, J. Anal. Toxicol., 1982, 6, 4, 185-192, https://doi.org/10.1093/jat/6.4.185 . [all data]


Notes

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