2,6-Nonadienal, (E,Z)-


Van Den Dool and Kratz RI, non-polar column, temperature ramp

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Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Data compiled by: NIST Mass Spectrometry Data Center, William E. Wallace, director

Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5MSDB-5MSDB-5HP-5
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHe He
Substrate      
Column diameter (mm) 0.250.250.250.320.25
Phase thickness (μm) 0.50.250.251.0.25
Tstart (C) 35.35.35.40.50.
Tend (C) 225.225.225.260.250.
Heat rate (K/min) 4.10.10.4.4.
Initial hold (min) 5.5.5.2.4.
Final hold (min) 30.25.25.10.10.
I 1156.1162.1155.1159.1158.
ReferenceJarunrattanasri, Theerakulkait, et al., 2007Lozano P.R., Drake M., et al., 2007Lozano P.R., Drake M., et al., 2007Methven L., Tsoukka M., et al., 2007Quijano, Salamanca, et al., 2007
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSSE-54Mega 5MSHP-5DB-5MS
Column length (m) 30.50.60.30.30.
Carrier gas H2HeHeN2He
Substrate      
Column diameter (mm) 0.250.320.250.250.25
Phase thickness (μm) 0.25 0.250.250.25
Tstart (C) 40.40.60.60.40.
Tend (C) 285.240.240.220.200.
Heat rate (K/min) 4.38.3.5.5.
Initial hold (min)  2. 10.5.
Final hold (min)  5.  45.
I 1154.1160.1185.1158.1160.
ReferenceRadulovic, Misic, et al., 2007Schlutt B., Moran N., et al., 2007Condurso, Verzera, et al., 2006Flamini, Tebano, et al., 2006Whetstine M.E.C., Drake M.A., et al., 2006
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5MSHP-5DB-5CP-Sil 8CB-MSHP-5
Column length (m) 30.30.30.0.30.
Carrier gas  N2N2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 40.60.30.40.50.
Tend (C) 200.220.250.280.250.
Heat rate (K/min) 10.5.3.4.4.
Initial hold (min) 3.10.2.2.5.
Final hold (min) 20. 2.5.15.
I 1160.1158.1145.1159.1155.
ReferenceCarunchia Whetstine, Croissant, et al., 2005Celik, Gokturk, et al., 2005Colahan-Sederstrom and Peterson, 2005Elmore, Cooper, et al., 2005Mahattanatawee, Goodner, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5HP-5HP-5MSDB-5MSDB-5MS
Column length (m) 30.30.30.60.30.
Carrier gas HeHeHeHe 
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 50.50.60.40.40.
Tend (C) 250.250.250.200.200.
Heat rate (K/min) 4.4.4.2.10.
Initial hold (min) 5.5.2. 3.
Final hold (min) 15.15.20.20.20.
I 1153.1151.1155.1157.1154.
ReferenceMahattanatawee, Goodner, et al., 2005Mahattanatawee, Goodner, et al., 2005Pino, Mesa, et al., 2005Seo and Baek, 2005Whetstine, Cadwallader, et al., 2005
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5ZB-5ZB-5DB-5SPB-5
Column length (m) 30.30.0.30.30.
Carrier gas  Helium HeHe
Substrate      
Column diameter (mm) 0.250.320.320.320.25
Phase thickness (μm) 0.250.500.51.0.25
Tstart (C) 40.40.40.40.60.
Tend (C) 200.265.265.230.250.
Heat rate (K/min) 10.7.7.5.4.
Initial hold (min) 5.  4.2.
Final hold (min) 15.5.5.10.20.
I 1153.1194.1156.1153.1167.
ReferenceAvsar, Karagul-Yuceer, et al., 2004Bell, 2004Gocmen, Gurbuz, et al., 2004Mahajan, Goddik, et al., 2004Pino, Marbot, et al., 2004
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-5DB-5MSDB-5MSDB-5MSSPB-1
Column length (m) 30.30.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.530.250.250.250.25
Phase thickness (μm) 1.50.250.250.250.25
Tstart (C) 100.40.40.40.35.
Tend (C) 250.200.200.200.225.
Heat rate (K/min) 5.4.4.4.4.
Initial hold (min)  5.5.5.5.
Final hold (min)  20.20.20.20.
I 1160.1158.1158.1158.1125.
ReferenceRodríguez-Burruezo, Kollmannsberger, et al., 2004Yu, Kim, et al., 2004Yu, Kim, et al., 2004, 2Zheng, Kim, et al., 2004Chisholm, Jell, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase SPB-1DB-5HP-5DB-5MSHP-5
Column length (m) 30.30.30.30.30.
Carrier gas HeHeN2HeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 35.60.60.35.60.
Tend (C) 225.240.220.200.280.
Heat rate (K/min) 4.3.5.10.4.
Initial hold (min) 5. 10.5.5.
Final hold (min) 20.  30. 
I 1125.1158.1158.1154.1151.
ReferenceChisholm, Jell, et al., 2003Flamini, Cioni, et al., 2003Flamini, Luigi Cioni, et al., 2003Karagül-Yüceer, Vlahovich, et al., 2003Skaltsa, Demetzos, et al., 2003
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase DB-5DB-5DB-5DB-5DB-5
Column length (m) 30.30.30.30.30.
Carrier gas He HeHe 
Substrate      
Column diameter (mm) 0.250.320.320.320.32
Phase thickness (μm) 0.250.250.250.250.25
Tstart (C) 60.35.40.40.35.
Tend (C) 240.200.220.220.200.
Heat rate (K/min) 3.10.10.10.10.
Initial hold (min)  5.5.5.5.
Final hold (min)  30.30.30.30.
I 1158.1148.1150.1150.1153.
ReferenceFlamini, Cioni, et al., 2002Karagül-Yüceer, Cadwallader, et al., 2002Wu and Cadwallader, 2002Wu and Cadwallader, 2002Karagül-Yüceer, Drake, et al., 2001
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-5MSDB-5MSHP-5HP-5MSHP-5
Column length (m) 30.60.30.30.30.
Carrier gas HeHeHeHeHe
Substrate      
Column diameter (mm) 0.250.250.250.250.25
Phase thickness (μm) 0.250.25 0.250.25
Tstart (C) 40.40.50.60.50.
Tend (C) 200.200.200.280.280.
Heat rate (K/min) 2.2.4.4.4.
Initial hold (min) 5.5.1.5.5.
Final hold (min) 20.30.   
I 1162.1153.1170.1151.1151.
ReferenceKim, Shin, et al., 2001Lee, Suriyaphan, et al., 2001Shalit, Katzir, et al., 2001Skaltsa, Mavrommati, et al., 2001Lazari, Skaltsa, et al., 2000
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI
Column type CapillaryCapillaryCapillaryCapillaryCapillary
Active phase HP-1HP-5DB-5MSSE-30OV-1
Column length (m) 25.30.30.50.50.
Carrier gas     H2
Substrate      
Column diameter (mm) 0.20.250.320.320.2
Phase thickness (μm) 0.330.250.250.25 
Tstart (C) 35.35.40.50.50.
Tend (C) 250.250.200.250.200.
Heat rate (K/min) 4.5.36.4.2.
Initial hold (min)   5.  
Final hold (min) 2.2.30. 55.
I 1132.11153.21156.1125.1185.
ReferenceSiegmund and Pfannhauser, 1999Siegmund and Pfannhauser, 1999Cha and Cadwallader, 1998Misharina and Golovnya, 1996Wu and Liou, 1986
Comment MSDC-RI MSDC-RI MSDC-RI MSDC-RI MSDC-RI

References

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, Notes

Data compilation copyright by the U.S. Secretary of Commerce on behalf of the U.S.A. All rights reserved.

Jarunrattanasri, Theerakulkait, et al., 2007
Jarunrattanasri, A.; Theerakulkait, C.; Cadwallader, K.R., Aroma Components of Acid-Hydrolyzed Vegetable Protein Made by Partial Hydrolysis of Rice Bran Protein, J. Agric. Food Chem., 2007, 55, 8, 3044-3050, https://doi.org/10.1021/jf0631474 . [all data]

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Carunchia Whetstine, Croissant, et al., 2005
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Colahan-Sederstrom and Peterson, 2005
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Pino, Mesa, et al., 2005
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Seo and Baek, 2005
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Gocmen, D.; Gurbuz, O.; Rouseff, R.L.; Smoot, J.M.; Dagdelen, A.F., Gas chromatographic-olfactometric characterization of aroma active compounds in sun-dried and vacuum-dried tarhana, Eur. Food Res. Technol., 2004, 218, 6, 573-578, https://doi.org/10.1007/s00217-004-0913-6 . [all data]

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Wu and Cadwallader, 2002
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Kim, Shin, et al., 2001
Kim, T.H.; Shin, J.H.; Baek, H.H.; Lee, H.J., Volatile flavour compounds in suspension culture of Agastache rugosa Kuntze (Korean mint), J. Sci. Food Agric., 2001, 81, 6, 569-575, https://doi.org/10.1002/jsfa.845 . [all data]

Lee, Suriyaphan, et al., 2001
Lee, G.-H.; Suriyaphan, O.; Cadwallader, K.R., Aroma components of cooked tail meat of American lobster (Homarus americanus), J. Agric. Food Chem., 2001, 49, 9, 4324-4332, https://doi.org/10.1021/jf001523t . [all data]

Shalit, Katzir, et al., 2001
Shalit, M.; Katzir, N.; Tadmor, Y.; Larkov, O.; Burger, Y.; Shalekhet, F.; Lastochkin, E.; Ravid, U.; Amar, O.; Edelstein, M.; Karchi, Z.; Lewinsohn, E., Acetyl-CoA: alcohol acetyltransferase activity and aroma formation in ripening melon fruits, J. Agric. Food Chem., 2001, 49, 2, 794-799, https://doi.org/10.1021/jf001075p . [all data]

Skaltsa, Mavrommati, et al., 2001
Skaltsa, H.D.; Mavrommati, A.; Constantinidis, T., A chemotaxonomic investigation of volatile constituents in Stachys subsect. Swainsonianeae (Labiatae), Phytochemistry, 2001, 57, 2, 235-244, https://doi.org/10.1016/S0031-9422(01)00003-6 . [all data]

Lazari, Skaltsa, et al., 2000
Lazari, D.M.; Skaltsa, H.D.; Constantinidis, T., Volatile constituents of Cerastium candidissimum, a Greek endemic species, Flavour Fragr. J., 2000, 15, 3, 174-176, https://doi.org/10.1002/1099-1026(200005/06)15:3<174::AID-FFJ886>3.0.CO;2-Y . [all data]

Siegmund and Pfannhauser, 1999
Siegmund, B.; Pfannhauser, W., Changes of the volatile fraction of cooked chicken meat during chill storing: results obtained by the electronic nose in comparison to GC-MS and GC olfactometry, Z. Lebensm. Unters. Forsch. A, 1999, 208, 5-6, 336-341, https://doi.org/10.1007/s002170050426 . [all data]

Cha and Cadwallader, 1998
Cha, Y.J.; Cadwallader, K.R., Aroma-active compounds in skipjack tuna sauce, J. Agric. Food Chem., 1998, 46, 3, 1123-1128, https://doi.org/10.1021/jf970380g . [all data]

Misharina and Golovnya, 1996
Misharina, T.A.; Golovnya, R.V., Study of the composition of volatiles in raw and processed sardine by gas chromatography and gas chromatography-mass spectrometry, Zh. Anal. Khim., 1996, 51, 7, 791-795. [all data]

Wu and Liou, 1986
Wu, C.-M.; Liou, S.-E., Effect of tissue disruption of volatile constituents of bell peppers, J. Agric. Food Chem., 1986, 34, 4, 770-772, https://doi.org/10.1021/jf00070a044 . [all data]


Notes

Go To: Top, Van Den Dool and Kratz RI, non-polar column, temperature ramp, References